3-Bromo-4-nitrophenol

Product Name: 3-Bromo-4-nitrophenol
CAS No.: 5470-65-5
Chemical Name: 3-Bromo-4-nitrophenol
Synonyms: NSC 2796;NSC 27960;4-Nitro-3-bromophenol;3-Bromo-4-nitrophenol;3-Bromo-4-nitro-phenol;Phenol, 3-broMo-4-nitro-
CBNumber: CB91175735
Molecular Formula: C6H4BrNO3
Formula Weight: 218
MOL File: 5470-65-5.mol

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3-Bromo-4-nitrophenol Property

Melting point:: 125-1270C
Boiling point:: 306.7±27.0 °C(Predicted)
Density: 1.881±0.06 g/cm3(Predicted)
storage temp.: Inert atmosphere,Room Temperature
solubility: DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form: Solid
pka: 6.32±0.10(Predicted)
color: Yellow to Brown

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H317May cause an allergic skin reaction

H318Causes serious eye damage

H410Very toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P391Collect spillage. Hazardous to the aquatic environment

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B686255
Product name: 3-Bromo-4-nitrophenol
Packaging: 10g
Price: $225
Updated: 2021/12/16

ChemScene

Product number: CS-W003684
Product name: 3-Bromo-4-nitrophenol
Purity: 98.97%
Packaging: 10g
Price: $159
Updated: 2021/12/16

AK Scientific

Product number: Z4867
Product name: 3-Bromo-4-nitrophenol
Packaging: 250mg
Price: $73
Updated: 2021/12/16

ChemScene

Product number: CS-W003684
Product name: 3-Bromo-4-nitrophenol
Purity: 98.97%
Packaging: 5g
Price: $89
Updated: 2021/12/16

AK Scientific

Product number: Z4867
Product name: 3-Bromo-4-nitrophenol
Packaging: 1g
Price: $91
Updated: 2021/12/16

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3-Bromo-4-nitrophenol Chemical Properties,Usage,Production

Chemical Properties

Brown Solid

Synthesis

591-20-8

5470-65-5

Example 1 Synthesis of 3-bromo-4-nitrophenol (Compound 4): concentrated sulfuric acid (98%, 10.0 mL, 187.4 mmol) was slowly added dropwise to a solution of NaNO3 (13.5 g, 159.6 mmol) in water (30 mL), and the reaction temperature was maintained at 0-5°C. Subsequently, a solution of 3-bromophenol (12.0 g, 69.4 mmol) dissolved in ethanol (25 mL). The reaction mixture was stirred overnight at room temperature before being poured into ice water (300 mL) and extracted with dichloromethane (3 × 100 mL). The combined organic layers were dried over anhydrous Na2SO4, filtered and concentrated, and purified by silica gel column chromatography (eluent: hexane solution of 30% ethyl acetate) to afford the target product, compound 4, in 37.1% yield (5.59 g) as a yellow solid. The structure of the product was confirmed by 1H-NMR (DMSO-d6, 400 MHz), 13C-NMR (CDCl3, 100 MHz) and mass spectrometry (ESI).

References

[1] Organic Letters, 2013, vol. 15, # 13, p. 3234 - 3237
[2] Patent: US2014/256817, 2014, A1. Location in patent: Page/Page column
[3] Patent: WO2007/30366, 2007, A1. Location in patent: Page/Page column 91-92
[4] Journal of Organic Chemistry, 2009, vol. 74, # 1, p. 212 - 221
[5] Journal of the Chemical Society, 1926, p. 159

3-Bromo-4-nitrophenol Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromo-4-nitrophenol Suppliers

Canada 1 China 96 India 5 The Netherlands 1 United Kingdom 1 United States 9 Global 113

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View Lastest Price from 3-Bromo-4-nitrophenol manufacturers

Career Henan Chemical Co

Product: 3-Bromo-4-nitrophenol 5470-65-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-25

5470-65-5, 3-Bromo-4-nitrophenolRelated Search:

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3-Bromo-4-nitrophenol

3-Bromo-4-nitro-phenol

Phenol, 3-broMo-4-nitro-

NSC 2796

NSC 27960

4-Nitro-3-bromophenol

5470-65-5

5470-65-6

Aromatics Compounds

Aromatics