ChemicalBook > CAS DataBase List > TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE

TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE

Uses

Product Name: TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE
CAS No.: 57476-50-3
Chemical Name: TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE
Synonyms: 1-Boc-3-formylindole;1-Boc-Indole-3-carboxaldehyde;3-FORMYLINDOLE, N-BOC PROTECTED;tertbutyl 3-formyl-1H-indole-1-formate;TERT-BUTYL 3-FORMYLINDOLE-1-CARBOXYLATE;INDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTED;1H-Indole-3-carboxaldehyde, N-BOC protected;TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE;tert-butyl 2-(3-formyl-1H-indol-1-yl)acetate;3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER
CBNumber: CB9132010
Molecular Formula: C14H15NO3
Formula Weight: 245.27
MOL File: 57476-50-3.mol

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TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE Property

Melting point:: 119-121°C
Boiling point:: 380.0±34.0 °C(Predicted)
Density: 1.13±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: solid
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36/37/39
HazardClass: IRRITANT
HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word: Warning
Hazard statements: H302Harmful if swallowed

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N-Bromosuccinimide Price

Sigma-Aldrich

Product number: KOB0061
Product name: tert-Butyl 3-formyl-1H-indole-1-carboxylate
Packaging: 1G
Price: $179
Updated: 2025/07/31

TCI Chemical

Product number: D6036
Product name: tert-Butyl 3-Formyl-1H-indole-1-carboxylate
Packaging: 5G
Price: $71
Updated: 2025/07/31

TCI Chemical

Product number: D6036
Product name: tert-Butyl 3-Formyl-1H-indole-1-carboxylate
Packaging: 25G
Price: $213
Updated: 2025/07/31

TRC

Product number: B695270
Product name: tert-Butyl3-Formyl-1H-indole-1-carboxylate
Packaging: 50mg
Price: $60
Updated: 2021/12/16

Matrix Scientific

Product number: 045909
Product name: tert-Butyl 3-formyl-1H-indole-1-carboxylate
Purity: >95%
Packaging: 1g
Price: $10
Updated: 2021/12/16

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TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE Chemical Properties,Usage,Production

Uses

3-Formylindole-1-carboxylic acid t-butyl ester is a carboxylic acid ester derivative that can be used as an intermediate in organic synthesis.

Synthesis

487-89-8

24424-99-5

57476-50-3

GENERAL METHOD: 3-indolecarboxaldehyde, triethylamine (1.3 eq.) and 10 mol% DMAP were dissolved in dichloromethane and di-tert-butyl dicarbonate (1.2 eq.) was added slowly. The reaction mixture was stirred at room temperature until complete consumption of the ingredients was shown by thin layer chromatography (TLC) monitoring. Upon completion of the reaction, the reaction mixture was diluted with dichloromethane and subsequently washed with water. The organic layer was separated, washed with saturated brine, dried over anhydrous sodium sulfate, filtered and concentrated under reduced pressure. The crude product was purified by fast column chromatography (eluent ratio: ethyl acetate/hexane = 1:5 for 1a and 1b; ethyl acetate/hexane = 1:9 for 1c) to afford the target compounds tert-butyl 3-formyl-1H-indole-1-carboxylate (1a-1c).

References

[1] Synthetic Communications, 2000, vol. 30, # 12, p. 2143 - 2159
[2] Organic and Biomolecular Chemistry, 2011, vol. 9, # 22, p. 7904 - 7912
[3] Bulletin of the Korean Chemical Society, 2013, vol. 34, # 2, p. 357 - 358
[4] Journal of Organic Chemistry, 2016, vol. 81, # 4, p. 1723 - 1730
[5] Journal of the American Chemical Society, 2018, vol. 140, # 20, p. 6432 - 6440

TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE Suppliers

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View Lastest Price from TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE manufacturers

Career Henan Chemical Co

Product: TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE 57476-50-3
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2019-12-23

57476-50-3, TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATERelated Search:

TERT-BUTYL 3-FLUORO-4-NITROBENZOATE tert-Butyl 3-formylbenzoate 5-METHOXY-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER Indole-3-carboxaldehyde 4-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 3-FORMYL-6-METHOXYINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 3-FORMYL-5-NITROINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 1H-INDOLE-1,3-DICARBOXYLIC ACID, 4-BROMO-, 1-(1,1-DIMETHYLETHYL)ESTER TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE 4-BENZYLOXY-1-BOC-3-INDOLECARBALDEHYDE 3-FORMYL-4-HYDROXYINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 6-BENZYLOXY-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER 5-BROMO-3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER INDOLE-1,3-DICARBOXYLIC ACID 1-TERT-BUTYL ESTER 3-METHYL ESTER tert-butyl 2-formyl-1H-indole-1-carboxylate TERT-BUTYL 7-FORMYL-1H-INDOLE-1-CARBOXYLATE TERT-BUTYL 6-FORMYL-1H-INDOLE-1-CARBOXYLATE TERT-BUTYL 4-FORMYL-1H-INDOLE-1-CARBOXYLATE

TERT-BUTYL 3-FORMYL-1H-INDOLE-1-CARBOXYLATE

TERT-BUTYL 3-FORMYLINDOLE-1-CARBOXYLATE

INDOLE-3-CARBOXALDEHYDE, N-BOC PROTECTED

3-FORMYLINDOLE-1-CARBOXYLIC ACID TERT-BUTYL ESTER

3-FORMYLINDOLE, N-BOC PROTECTED

1-Boc-3-formylindole

3-Formylindole-1-carboxylic acid t-butyl ester

1H-Indole-3-carboxaldehyde, N-BOC protected

3-Formyl-1H-indole, N-BOC protected, tert-Butyl 3-formyl-1H-indole-1-carboxylate

1-Boc-Indole-3-carboxaldehyde

1H-Indole-1-carboxylic acid, 3-formyl-, 1,1-dimethylethyl ester

tert-butyl 2-(3-formyl-1H-indol-1-yl)acetate

tert-Butyl 3-formyl-1H-indole-1-carboxylate, 1-(tert-Butoxycarbonyl)-3-formyl-1H-indole

tertbutyl 3-formyl-1H-indole-1-formate

<i>tert</i>-Butyl 3-formyl-1<i>H</i>-indole-1-carboxylate

57476-50-3