ChemicalBook > CAS DataBase List > 2-AMINO-5-IODOBENZOTRIFLUORIDE

2-AMINO-5-IODOBENZOTRIFLUORIDE

Product Name
2-AMINO-5-IODOBENZOTRIFLUORIDE
CAS No.
97760-97-9
Chemical Name
2-AMINO-5-IODOBENZOTRIFLUORIDE
Synonyms
4-IODO-2-(TRIFLUOROMETHYL)ANILINE;ASISCHEM Z25859;2-AMINO-5-IODOBENZOTRIFLUORIDE;2-Amino-5-iodobenzotrifluoride98%;2-Amino-5-iodobenzotrifluoride 98%;4-Iodo-2-trifluoromethylphenylamine;4-iodo-2-(trifluoromethyl)benzenamine;2-amino-5-iodo-trifluoromethylbenzene;Benzenamine, 4-iodo-2-(trifluoromethyl)-;2-AMino-5-iodobenzotrifluoride[4-iodo-2-(trifluoroMethyl)aniline]
CBNumber
CB9138698
Molecular Formula
C7H5F3IN
Formula Weight
287.02
MOL File
97760-97-9.mol
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2-AMINO-5-IODOBENZOTRIFLUORIDE Property

Boiling point:
262℃
Density 
1.948
Flash point:
112℃
storage temp. 
Keep in dark place,Inert atmosphere,2-8°C
form 
liquid
pka
0.67±0.10(Predicted)
color 
Clear, brown
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Safety

Hazard Codes 
Xi
Risk Statements 
20/21/22-36/37/38
Safety Statements 
26-36/37/39
HazardClass 
IRRITANT
HS Code 
2921420090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC
Product number
I724785
Product name
4-Iodo-2-trifluoromethylaniline
Packaging
100mg
Price
$45
Updated
2021/12/16
TRC
Product number
I724785
Product name
4-Iodo-2-trifluoromethylaniline
Packaging
1g
Price
$75
Updated
2021/12/16
AK Scientific
Product number
J56944
Product name
4-Iodo-2-trifluoromethylaniline
Packaging
10g
Price
$82
Updated
2021/12/16
Matrix Scientific
Product number
066903
Product name
2-Amino-5-iodobenzotrifluoride
Purity
98%
Packaging
25g
Price
$148
Updated
2021/12/16
Apolloscientific
Product number
PC2012
Product name
2-Amino-5-iodobenzotrifluoride
Purity
98%
Packaging
25g
Price
$156
Updated
2021/12/16
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2-AMINO-5-IODOBENZOTRIFLUORIDE Chemical Properties,Usage,Production

Uses

4-Iodo-2-trifluoromethylaniline

Synthesis

887144-94-7

540-37-4

97760-97-9

The general procedure for synthesizing 2-amino-5-iodobenzotrifluoride from 1-(trifluoromethyl)-1,2-phenyliodonyl-3(1H)-one and p-iodoaniline is as follows: in this embodiment, p-iodoaniline was used as the aromatic amine, and the rest of the reaction conditions and post-processing steps were the same as in Example 28. The specific reaction conditions were as follows: 1-(trifluoromethyl)-1,2-phenyliodono-3(1H)-one (0.5 mmol, 1.0 eq.), p-iodoaniline (1.5 mmol, 3.0 eq.), nickel hydroxide (10 μmol), and potassium carbonate (1.5 mmol, 3.0 eq.) were used as bases, and DMSO (2 mL) was used as a solvent, and the temperature of the reaction was 35 °C. The reaction time was 2 hours. After the reaction was completed, post-treatment was carried out according to the method of Example 1.

References

[1] Organic Letters, 2018, vol. 20, # 13, p. 3732 - 3735
[2] Patent: CN108503552, 2018, A. Location in patent: Paragraph 0240-0244
[3] Patent: CN103553857, 2016, B. Location in patent: Paragraph 0021-0022
[4] Organic Letters, 2014, vol. 16, # 6, p. 1768 - 1771

2-AMINO-5-IODOBENZOTRIFLUORIDE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-AMINO-5-IODOBENZOTRIFLUORIDE Suppliers

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97760-97-9, 2-AMINO-5-IODOBENZOTRIFLUORIDERelated Search:


  • 4-IODO-2-(TRIFLUOROMETHYL)ANILINE
  • 2-AMINO-5-IODOBENZOTRIFLUORIDE
  • ASISCHEM Z25859
  • 2-Amino-5-iodobenzotrifluoride 98%
  • 2-Amino-5-iodobenzotrifluoride98%
  • 4-Iodo-2-(trifluoromethyl)aniline, 4-Iodo-alpha,alpha,alpha-trifluoro-o-toluidine
  • 2-AMino-5-iodobenzotrifluoride[4-iodo-2-(trifluoroMethyl)aniline]
  • 2-amino-5-iodo-trifluoromethylbenzene
  • 4-iodo-2-(trifluoromethyl)benzenamine
  • 4-Iodo-2-trifluoromethylphenylamine
  • Benzenamine, 4-iodo-2-(trifluoromethyl)-
  • 97760-97-9
  • C6H5F3IN
  • Phenyls & Phenyl-Het
  • Amines
  • Phenyls & Phenyl-Het