ChemicalBook > CAS DataBase List > 2-Acetyl-6-bromonaphthalene
2-Acetyl-6-bromonaphthalene
- Product Name
- 2-Acetyl-6-bromonaphthalene
- CAS No.
- 1590-25-6
- Chemical Name
- 2-Acetyl-6-bromonaphthalene
- Synonyms
- 6-BROMO-2-ACETONAPHTHONE;1-(6-bromo-2-naphthyl)ethanone;(6-bromo-2-naphthalenyl)ethanone;1-(6-Bromonaphthalen-2-yl)ethanone;1-(6-bromonaphthalen-2-yl)ethan-1-one;Ethanone, 1-(6-bromo-2-naphthalenyl)-
- CBNumber
- CB91451107
- Molecular Formula
- C12H9BrO
- Formula Weight
- 249.1
- MOL File
- 1590-25-6.mol
More
Less
2-Acetyl-6-bromonaphthalene Property
- Melting point:
- 96 °C
- Boiling point:
- 357.1±15.0 °C(Predicted)
- Density
- 1.454±0.06 g/cm3(Predicted)
- storage temp.
- Sealed in dry,Room Temperature
- Appearance
- White to light brown Solid
- InChI
- InChI=1S/C12H9BrO/c1-8(14)9-2-3-11-7-12(13)5-4-10(11)6-9/h2-7H,1H3
- InChIKey
- UZDOTHVVSQOCJO-UHFFFAOYSA-N
- SMILES
- C(=O)(C1=CC=C2C(=C1)C=CC(Br)=C2)C
More
Less
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
More
Less
N-Bromosuccinimide Price
ChemScene
- Product number
- CS-0041458
- Product name
- 1-(6-Bromonaphthalen-2-yl)ethanone
- Purity
- >97.0%
- Packaging
- 100mg
- Price
- $70
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0041458
- Product name
- 1-(6-Bromonaphthalen-2-yl)ethanone
- Purity
- >97.0%
- Packaging
- 250mg
- Price
- $112
- Updated
- 2021/12/16
American Custom Chemicals Corporation
- Product number
- HCH0108835
- Product name
- 1-(6-BROMO-2-NAPHTHYL)ETHANONE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $504.64
- Updated
- 2021/12/16
ChemScene
- Product number
- CS-0041458
- Product name
- 1-(6-Bromonaphthalen-2-yl)ethanone
- Purity
- >97.0%
- Packaging
- 1g
- Price
- $279
- Updated
- 2021/12/16
Matrix Scientific
- Product number
- 171626
- Product name
- 1-(6-Bromonaphthalen-2-yl)ethanone
- Purity
- 95%
- Packaging
- 2.500g
- Price
- $1650
- Updated
- 2021/12/16
More
Less
2-Acetyl-6-bromonaphthalene Chemical Properties,Usage,Production
Synthesis
861880-64-0
75-16-1
1590-25-6
Under nitrogen protection, 6-bromo-N-methoxy-N-methyl-2-naphthalenecarboxamide (82.9 g, 282 mmol, 1.0 eq.) was dissolved in tetrahydrofuran (600 mL) in a four-necked flask. The reaction mixture was cooled in an ice bath at a controlled temperature in the range of 10-15 °C. Methylmagnesium bromide (3.2 M in methyltetrahydrofuran, 197 mL, 2.2 eq.) was added slowly dropwise over a period of 1 hour. After the dropwise addition was completed, the reaction mixture continued to be stirred in an ice bath for 30 minutes. Subsequently, aqueous 2M hydrochloric acid (100 mL) was carefully added dropwise to quench the reaction under cooling in the ice bath. After the organic solvent was removed by evaporation, the precipitated product was extracted with dichloromethane (500 mL). The organic phases were combined, dried over anhydrous sodium sulfate, filtered and concentrated. The resulting solid residue was dried under vacuum at 40 °C to give 1-(6-bromonaphthalen-2-yl)ethanone (70.6 g, 99% yield).
References
[1] Patent: WO2011/54834, 2011, A1. Location in patent: Page/Page column 39
[2] Patent: WO2011/91446, 2011, A1. Location in patent: Page/Page column 11
[3] Patent: US2017/253614, 2017, A1. Location in patent: Paragraph 0574; 0575
[4] Patent: US2011/64695, 2011, A1. Location in patent: Page/Page column 94
[5] Patent: US2011/64697, 2011, A1. Location in patent: Page/Page column 85
2-Acetyl-6-bromonaphthalene Preparation Products And Raw materials
Raw materials
Preparation Products
More
Less
2-Acetyl-6-bromonaphthalene Suppliers
- Tel
- 18515581800 18501085097
- Fax
- 010-89508210
- sales.bj@hwrkchemical.com
- Country
- China
- ProdList
- 9400
- Advantage
- 55
- Tel
- 0573-85285100 18627885956
- Fax
- 0573-85285100
- isenchem@163.com
- Country
- China
- ProdList
- 9310
- Advantage
- 66
- Tel
- 400-164-7117 13681763483
- Fax
- +86-21-61629029
- product02@bidepharm.com
- Country
- China
- ProdList
- 39966
- Advantage
- 60
- Tel
- 021-60345187 13671753212
- Fax
- 021-34702061
- lzz841106@aliyun.com
- Country
- China
- ProdList
- 10263
- Advantage
- 55
- Tel
- 025-0523-86200082 15380713688
- Fax
- 0523-86200991
- Austin@fredchem.cn
- Country
- China
- ProdList
- 151
- Advantage
- 55
- Tel
- 010-56330744 18310155299
- Fax
- 010-56330744
- sales@labter.com.cn
- Country
- China
- ProdList
- 20000
- Advantage
- 55
- Tel
- 027-59207879 1972026995 18140587686
- Fax
- QQ：1972026995
- sales@3600chem.com
- Country
- China
- ProdList
- 4456
- Advantage
- 55
- Tel
- 0512-62910395 17751098781
- Fax
- 0512-62910396
- sales@crstpharma.com
- Country
- China
- ProdList
- 499
- Advantage
- 58
- Tel
- 0371-86658258
- Fax
- 0371-60996044
- info@coreychem.com
- Country
- China
- ProdList
- 10453
- Advantage
- 58
- Tel
- 0931-8235634 13321316780
- Fax
- +86(931) 4873122
- 1455540579@qq.com
- Country
- China
- ProdList
- 958
- Advantage
- 55
- Tel
- 021-31137757-00; 18121466954
- Fax
- 021-64902762
- 28328681@qq.com
- Country
- China
- ProdList
- 180
- Advantage
- 55
- Tel
- 021-61312847; 18021002903
- Fax
- QQ:3008007432
- 3008007409@qq.com
- Country
- China
- ProdList
- 71826
- Advantage
- 60
- Tel
- 400-685-9117
- Fax
- 021-51816740
- market@bepharm.com
- Country
- China
- ProdList
- 15081
- Advantage
- 60
- Tel
- 21-21-31590156 13042155638
- Fax
- +86 21 31590152
- sales@sino-biochemlab.com
- Country
- China
- ProdList
- 293
- Advantage
- 58
- Tel
- 0371-55900031 18137872243
- Fax
- QQ：2853979815
- 2853979815@qq.com
- Country
- China
- ProdList
- 9975
- Advantage
- 55
- Tel
- 025-58859352 18068836627
- Fax
- 02557626880
- sales01@aikonchem.com
- Country
- China
- ProdList
- 15083
- Advantage
- 58
- Tel
- 4009004166/18616739031 18616739031
- 3007523370@qq.com
- Country
- China
- ProdList
- 52687
- Advantage
- 58
- Tel
- 18916696128
- service@snowpharm.com
- Country
- China
- ProdList
- 1369
- Advantage
- 58
- Tel
- 15121162054
- Country
- CHINA
- ProdList
- 635
- Advantage
- 58
- Tel
- +8615255079626
- eric@witopchemical.com
- Country
- China
- ProdList
- 23541
- Advantage
- 58
- Tel
- +86-0571-88938639 +8617705817739
- Fax
- +86-571-88938652，+86-571- 88492614
- info@dycnchem.com
- Country
- China
- ProdList
- 52846
- Advantage
- 58
- Tel
- +8617735180244
- mike_yan@xuanranglobal.com
- Country
- CHINA
- ProdList
- 4017
- Advantage
- 58
- Tel
- +8618660799346
- Fax
- +86 531 8316 6650
- sales@qinmuchem.com
- Country
- China
- ProdList
- 1008
- Advantage
- 58
- Tel
- +86-5922680277 +86-13806087780
- sale@simagchem.com
- Country
- China
- ProdList
- 17346
- Advantage
- 58
- Tel
- 86-21-51086038
- Fax
- 86-21-51861608
- chemwill_asia@126.com
- Country
- CHINA
- ProdList
- 23912
- Advantage
- 58
- Tel
- +86-023-6139-8061 +86-86-13650506873
- sales@chemdad.com
- Country
- China
- ProdList
- 39927
- Advantage
- 58
- Tel
- 15151934985
- sales@yingsapharm.com
- Country
- China
- ProdList
- 5183
- Advantage
- 58
- Tel
- 021-58461859 15821823057
- service@aiviche.com
- Country
- China
- ProdList
- 49312
- Advantage
- 58
- Tel
- 18503026267
- info@antaichem.com
- Country
- CHINA
- ProdList
- 9636
- Advantage
- 58
- Tel
- 021-58432009 400-005-6266
- Fax
- 021-58436166
- marketing@energy-chemical.com
- Country
- China
- ProdList
- 44918
- Advantage
- 58
- Tel
- 021-51816796-820 13611835272
- Fax
- 021-5161 3951
- sales2@sunwaypharm.com
- Country
- China
- ProdList
- 44119
- Advantage
- 58
- Tel
- 0574-87314919 057487319282
- info@nbinno.com
- Country
- China
- ProdList
- 7047
- Advantage
- 58
- Tel
- 400-8210725 4008210725
- malulu@leyan.com
- Country
- China
- ProdList
- 40000
- Advantage
- 58
- Tel
- 18130062233
- 3362556465@qq.com
- Country
- China
- ProdList
- 8100
- Advantage
- 58
- Tel
- 400-6005915
- sales@picasso-e.com
- Country
- China
- ProdList
- 39665
- Advantage
- 58
- Tel
- 18051976595
- 3086187058@qq.com
- Country
- China
- ProdList
- 298
- Advantage
- 58
- Tel
- 15841022315
- sales@affinitytech.cn
- Country
- China
- ProdList
- 3000
- Advantage
- 58
- Tel
- 15811073878
- 2559355526@qq.com
- Country
- China
- ProdList
- 10701
- Advantage
- 58
- Tel
- 13901585132
- 2261760024@qq.com
- Country
- China
- ProdList
- 4900
- Advantage
- 58
- Tel
- 15553348166
- m15553348166@163.com
- Country
- China
- ProdList
- 9967
- Advantage
- 58
- Tel
- +86(21)5895 0110 19945755304
- sales@chemany.com
- Country
- China
- ProdList
- 9984
- Advantage
- 58
- Tel
- 19307246857
- 2687203556@qq.com
- Country
- China
- ProdList
- 786
- Advantage
- 58
- Tel
- 021-021-50706066 15221275939
- shenlinxing@macklin.cn
- Country
- China
- ProdList
- 29784
- Advantage
- 58
- Tel
- 18621169109
- market03@meryer.com
- Country
- China
- ProdList
- 27987
- Advantage
- 58
- Tel
- 010-50973130 17801761073
- Gsiyu@solarbio.com
- Country
- China
- ProdList
- 50751
- Advantage
- 58
- Tel
- 021-57520305 13795461237
- zhuruyan@jskchem.com
- Country
- China
- ProdList
- 49234
- Advantage
- 58
- Tel
- 4000255188
- sales@pharmablock.com
- Country
- China
- ProdList
- 7268
- Advantage
- 58
- Tel
- 400-0628126 18736790110;
- sales-team@aobchem.com.cn
- Country
- China
- ProdList
- 50000
- Advantage
- 58
- Tel
- 029-81145305 17791533577
- 1021@dideu.com
- Country
- China
- ProdList
- 10009
- Advantage
- 58
- Tel
- 400-6206333 13167063860
- anhua.mao@aladdin-e.com
- Country
- China
- ProdList
- 48457
- Advantage
- 58
More
Less
View Lastest Price from 2-Acetyl-6-bromonaphthalene manufacturers
Nanjing Fred Technology Co., Ltd
- Product
- 1-(6-Bromonaphthalen-2-yl)ethanone 1590-25-6
- Price
- US $0.00/kg
- Min. Order
- 0.1kg
- Purity
- 98%HPLC
- Supply Ability
- 100kg
- Release date
- 2023-11-27
Career Henan Chemical Co
- Product
- 2-Acetyl-6-bromonaphthalene 1590-25-6
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1 ton
- Release date
- 2018-08-20