2-Acetyl-6-bromonaphthalene

Product Name: 2-Acetyl-6-bromonaphthalene
CAS No.: 1590-25-6
Chemical Name: 2-Acetyl-6-bromonaphthalene
Synonyms: 6-BROMO-2-ACETONAPHTHONE;1-(6-bromo-2-naphthyl)ethanone;(6-bromo-2-naphthalenyl)ethanone;1-(6-Bromonaphthalen-2-yl)ethanone;1-(6-bromonaphthalen-2-yl)ethan-1-one;Ethanone, 1-(6-bromo-2-naphthalenyl)-
CBNumber: CB91451107
Molecular Formula: C12H9BrO
Formula Weight: 249.1
MOL File: 1590-25-6.mol

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2-Acetyl-6-bromonaphthalene Property

Melting point:: 96 °C
Boiling point:: 357.1±15.0 °C(Predicted)
Density: 1.454±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to light brown Solid
InChI: InChI=1S/C12H9BrO/c1-8(14)9-2-3-11-7-12(13)5-4-10(11)6-9/h2-7H,1H3
InChIKey: UZDOTHVVSQOCJO-UHFFFAOYSA-N
SMILES: C(=O)(C1=CC=C2C(=C1)C=CC(Br)=C2)C

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

ChemScene

Product number: CS-0041458
Product name: 1-(6-Bromonaphthalen-2-yl)ethanone
Purity: >97.0%
Packaging: 100mg
Price: $70
Updated: 2021/12/16

ChemScene

Product number: CS-0041458
Product name: 1-(6-Bromonaphthalen-2-yl)ethanone
Purity: >97.0%
Packaging: 250mg
Price: $112
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0108835
Product name: 1-(6-BROMO-2-NAPHTHYL)ETHANONE
Purity: 95.00%
Packaging: 5MG
Price: $504.64
Updated: 2021/12/16

ChemScene

Product number: CS-0041458
Product name: 1-(6-Bromonaphthalen-2-yl)ethanone
Purity: >97.0%
Packaging: 1g
Price: $279
Updated: 2021/12/16

Matrix Scientific

Product number: 171626
Product name: 1-(6-Bromonaphthalen-2-yl)ethanone
Purity: 95%
Packaging: 2.500g
Price: $1650
Updated: 2021/12/16

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2-Acetyl-6-bromonaphthalene Chemical Properties,Usage,Production

Synthesis

861880-64-0

75-16-1

1590-25-6

Under nitrogen protection, 6-bromo-N-methoxy-N-methyl-2-naphthalenecarboxamide (82.9 g, 282 mmol, 1.0 eq.) was dissolved in tetrahydrofuran (600 mL) in a four-necked flask. The reaction mixture was cooled in an ice bath at a controlled temperature in the range of 10-15 °C. Methylmagnesium bromide (3.2 M in methyltetrahydrofuran, 197 mL, 2.2 eq.) was added slowly dropwise over a period of 1 hour. After the dropwise addition was completed, the reaction mixture continued to be stirred in an ice bath for 30 minutes. Subsequently, aqueous 2M hydrochloric acid (100 mL) was carefully added dropwise to quench the reaction under cooling in the ice bath. After the organic solvent was removed by evaporation, the precipitated product was extracted with dichloromethane (500 mL). The organic phases were combined, dried over anhydrous sodium sulfate, filtered and concentrated. The resulting solid residue was dried under vacuum at 40 °C to give 1-(6-bromonaphthalen-2-yl)ethanone (70.6 g, 99% yield).

References

[1] Patent: WO2011/54834, 2011, A1. Location in patent: Page/Page column 39
[2] Patent: WO2011/91446, 2011, A1. Location in patent: Page/Page column 11
[3] Patent: US2017/253614, 2017, A1. Location in patent: Paragraph 0574; 0575
[4] Patent: US2011/64695, 2011, A1. Location in patent: Page/Page column 94
[5] Patent: US2011/64697, 2011, A1. Location in patent: Page/Page column 85

2-Acetyl-6-bromonaphthalene Preparation Products And Raw materials

Raw materials

Preparation Products

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2-Acetyl-6-bromonaphthalene Suppliers

China 71 India 1 United States 3 Global 75

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View Lastest Price from 2-Acetyl-6-bromonaphthalene manufacturers

Nanjing Fred Technology Co., Ltd

Product: 1-(6-Bromonaphthalen-2-yl)ethanone 1590-25-6
Price: US $0.00/kg
Min. Order: 0.1kg
Purity: 98%HPLC
Supply Ability: 100kg
Release date: 2023-11-27

Career Henan Chemical Co

Product: 2-Acetyl-6-bromonaphthalene 1590-25-6
Price: US $2.00/KG
Min. Order: 1KG
Purity: 98%
Supply Ability: 1 ton
Release date: 2018-08-20

1590-25-6, 2-Acetyl-6-bromonaphthaleneRelated Search:

6-BROMO-2-ACETONAPHTHONE

1-(6-Bromonaphthalen-2-yl)ethanone

(6-bromo-2-naphthalenyl)ethanone

Ethanone, 1-(6-bromo-2-naphthalenyl)-

1-(6-bromonaphthalen-2-yl)ethan-1-one

1-(6-bromo-2-naphthyl)ethanone

1590-25-6