ChemicalBook > CAS DataBase List > 2-Amino-5-bromoisonicotinic acid

2-Amino-5-bromoisonicotinic acid

Product Name
2-Amino-5-bromoisonicotinic acid
CAS No.
1000339-23-0
Chemical Name
2-Amino-5-bromoisonicotinic acid
Synonyms
2-Amino-5-bromoisonicotinic;2-Amino-5-bromoisonicotinicaci;2-Amino-5-bromoisonicotinic acid;2-aMino-5-broMopyridin-4-carboxylic acid;2-Amino-5-bromo-4-pyridinecarboxylic acid;4-Pyridinecarboxylic acid,2-amino-5-bromo-;2-Amino-5-bromoisonicotinic acid ISO 9001：2015 REACH
CBNumber
CB91457068
Molecular Formula
C6H5BrN2O2
Formula Weight
217.02
MOL File
1000339-23-0.mol
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2-Amino-5-bromoisonicotinic acid Property

Boiling point:
464.1±45.0 °C(Predicted)
Density 
1.909
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
1.16±0.10(Predicted)
form 
solid
color 
Yellow
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Safety

HazardClass 
IRRITANT
HS Code 
2933399990
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

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N-Bromosuccinimide Price

TRC
Product number
A594833
Product name
2-Amino-5-bromoisonicotinicAcid
Packaging
100mg
Price
$75
Updated
2021/12/16
Apolloscientific
Product number
OR907528
Product name
2-Amino-5-bromoisonicotinicacid
Purity
98%
Packaging
5g
Price
$93
Updated
2021/12/16
AK Scientific
Product number
Y6748
Product name
2-Amino-5-bromopyridine-4-carboxylicacid
Packaging
5g
Price
$149
Updated
2021/12/16
Apolloscientific
Product number
OR907528
Product name
2-Amino-5-bromoisonicotinicacid
Purity
98%
Packaging
10g
Price
$163
Updated
2021/12/16
Matrix Scientific
Product number
041229
Product name
2-Amino-5-bromopyridine-4-carboxylic acid
Purity
98%
Packaging
25g
Price
$258
Updated
2021/12/16
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2-Amino-5-bromoisonicotinic acid Chemical Properties,Usage,Production

Synthesis

882499-87-8

1000339-23-0

General procedure for the synthesis of 2-amino-5-bromo-4-carboxylic acid pyridine from 2-amino-5-bromoisonicotinic acid methyl ester: 2-amino-5-bromoisonicotinic acid methyl ester (10.0 g, 43.28 mmol) and lithium hydroxide (LiOH, 5.46 g, 129.8 mmol) were reacted with 2-amino-5-bromo-4-carboxylic acid methyl ester (10.0 g, 43.28 mmol) and 2-amino-5-bromoisonicotinic acid methyl ester (10.0 g, 43.28 mmol) and lithium hydroxide (LiOH, 5.46 g, 129.8 mmol) in a water (100 mL) in a solvent mixture of tetrahydrofuran (THF, 400 mL), methanol (MeOH, 200 mL), and water (100 mL), and the reaction was stirred at 70 °C for 2 h under nitrogen (N2) protection. Upon completion of the reaction, the reaction mixture was cooled to 0 °C and the pH was adjusted to 6 by dropwise addition of concentrated aqueous hydrochloric acid (HCl).Subsequently, the resulting suspension was filtered and the solid was dried under vacuum to afford pyridine 2-amino-5-bromo-4-carboxylic acid (7.8 g, 83% yield). The product was analyzed by liquid chromatography-mass spectrometry (LC-MS, ESI) and showed m/z 211 [M + H]+.

References

[1] Patent: WO2012/58125, 2012, A1. Location in patent: Page/Page column 145

2-Amino-5-bromoisonicotinic acid Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 2-Amino-5-bromoisonicotinic acid manufacturers

RongNa Biotechnology Co.,Ltd
Product
2-Amino-5-bromoisonicotinic acid 1000339-23-0
Price
US $10.00/ASSAYS
Min. Order
1ASSAYS
Purity
99%
Supply Ability
1 ton
Release date
2025-08-27
Henan Fengda Chemical Co., Ltd
Product
2-Amino-5-bromopyridine-4-carboxylic acid 1000339-23-0
Price
US $200.00-1.00/KG
Min. Order
1KG
Purity
99%, 99.5% Sublimated
Supply Ability
g-kg-tons, free sample is available
Release date
2023-12-30
Dideu Industries Group Limited
Product
2-Amino-5-bromoisonicotinic acid 1000339-23-0
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons min
Release date
2021-08-23

1000339-23-0, 2-Amino-5-bromoisonicotinic acidRelated Search:

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  • 1000339-23-0