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5-iodopyrimidin-4-amine

Product Name
5-iodopyrimidin-4-amine
CAS No.
91416-96-5
Chemical Name
5-iodopyrimidin-4-amine
Synonyms
5-iodopyrimidin-4-amine;4-Amino-5-iodopyrimidine;4-Pyrimidinamine,5-iodo-;5-Iodo-pyrimidin-4-ylamine;5-iodopyrimidin-4-amine ISO 9001:2015 REACH
CBNumber
CB91516109
Molecular Formula
C4H4IN3
Formula Weight
221
MOL File
91416-96-5.mol
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5-iodopyrimidin-4-amine Property

Melting point:
188-189 °C
Boiling point:
322.7±27.0 °C(Predicted)
Density 
2.204±0.06 g/cm3(Predicted)
storage temp. 
Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
pka
3.86±0.10(Predicted)
Appearance
Light yellow to green yellow Solid
InChI
InChI=1S/C4H4IN3/c5-3-1-7-2-8-4(3)6/h1-2H,(H2,6,7,8)
InChIKey
HTBFTDHEWCRQPJ-UHFFFAOYSA-N
SMILES
C1=NC=C(I)C(N)=N1
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Biosynth Carbosynth
Product number
FA153866
Product name
4-Amino-5-iodopyrimidine
Packaging
100mg
Price
$69
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA153866
Product name
4-Amino-5-iodopyrimidine
Packaging
250mg
Price
$137.5
Updated
2021/12/16
Biosynth Carbosynth
Product number
FA153866
Product name
4-Amino-5-iodopyrimidine
Packaging
500mg
Price
$240
Updated
2021/12/16
AK Scientific
Product number
W9386
Product name
4-Amino-5-iodopyrimidine
Packaging
1g
Price
$290
Updated
2021/12/16
Matrix Scientific
Product number
072486
Product name
4-Amino-5-iodopyrimidine
Purity
95+%
Packaging
250mg
Price
$324
Updated
2021/12/16
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5-iodopyrimidin-4-amine Chemical Properties,Usage,Production

Synthesis

163133-86-6

91416-96-5

The general procedure for the synthesis of 4-amino-5-iodopyrimidine from the compound (CAS:163133-86-6) is as follows: 4-aminopyridine (0.970 g, 10.3 mmol) was dissolved in 20 mL of acetic acid, and iodine monochloride (1.67 g, 10.3 mmol, 1.01 eq.) was added to produce a large amount of N-iodine-substituted intermediates precipitate immediately in the reaction system. The reaction mixture was refluxed for 3 hours under argon protection. Upon completion of the reaction, the mixture was cooled to about 10 °C with a water bath to induce complete precipitation of the product. The precipitate was collected by filtration and dried to give 4-amino-5-iodopyrimidine as a pale yellow solid (1.4 g, 62% yield).

References

[1] Heterocycles, 1984, vol. 22, # 5, p. 1195 - 1210
[2] Synthesis (Germany), 2012, vol. 44, # 22, p. 3496 - 3504
[3] Patent: WO2005/30213, 2005, A1. Location in patent: Page/Page column 177
[4] Journal of the Society of Chemical Industry, London, 1950, vol. 69, p. 353
[5] Patent: US6541505, 2003, B1

5-iodopyrimidin-4-amine Preparation Products And Raw materials

Raw materials

Preparation Products

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5-iodopyrimidin-4-amine Suppliers

Shanghai Jiezhen Pharmaceutical Technology Co., Ltd.
Tel
15995055116
Fax
815229059
Email
815229059@qq.com
Country
China
ProdList
142
Advantage
58
PharmaBlock Sciences (Nanjing),Inc.
Tel
025-86918202 4000255188
Fax
86-025-86918232
Email
sales@pharmablock.com
Country
China
ProdList
5000
Advantage
55
Pure Chemistry Scientific Inc.
Tel
001-857-928-2050 or 1-888-588-9418
Fax
001-617-206-9595
Email
sales@chemreagents.com
Country
United States
ProdList
10186
Advantage
62
Shandong Xiya Chemical Co., Ltd
Tel
4009903999 13355009207
Fax
0539-6365991
Email
3007715519@qq.com
Country
China
ProdList
18729
Advantage
57
Shanghai yirong biology science and technology co., ltd
Tel
18049974220
Fax
+86 (21) 51062076
Email
3060526242@qq.com
Country
China
ProdList
995
Advantage
60
NovoChemy Ltd.
Tel
021-31261262/ 49 (0)17662837245
Fax
(0)21-33250524
Email
sales@novochemy.com
Country
Germany
ProdList
6328
Advantage
58
Shanghai Keepontech Co.,Ltd
Tel
021-54849683 13601642561
Fax
+86-21-54375689
Email
sales@keepontech.com
Country
China
ProdList
998
Advantage
59
Bide Pharmatech Ltd.
Tel
400-164-7117 13681763483
Fax
+86-21-61629029
Email
product02@bidepharm.com
Country
China
ProdList
39966
Advantage
60
Shanghai Worldyang Chemical Co.,Ltd.
Tel
021-021-56795766
Fax
+86-21-56795266
Email
sales@worldyachem.com
Country
China
ProdList
9476
Advantage
58
Hunan HuaTeng Pharmaceutical Co., Ltd.,
Tel
400-8592883
Fax
0731-82251112
Email
sales@huatengsci.com
Country
China
ProdList
5872
Advantage
58
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View Lastest Price from 5-iodopyrimidin-4-amine manufacturers

Dideu Industries Group Limited
Product
5-iodopyrimidin-4-amine 91416-96-5
Price
US $1.10/g
Min. Order
1g
Purity
99.00%
Supply Ability
100 Tons Min
Release date
2021-12-06
Career Henan Chemical Co
Product
5-iodopyrimidin-4-amine 91416-96-5
Price
US $6.00/KG
Min. Order
1KG
Purity
98%
Supply Ability
1kg, 5kg, 50kg
Release date
2020-01-09