5-iodopyrimidin-4-amine
- Product Name
- 5-iodopyrimidin-4-amine
- CAS No.
- 91416-96-5
- Chemical Name
- 5-iodopyrimidin-4-amine
- Synonyms
- 5-iodopyrimidin-4-amine;4-Amino-5-iodopyrimidine;4-Pyrimidinamine,5-iodo-;5-Iodo-pyrimidin-4-ylamine;5-iodopyrimidin-4-amine ISO 9001:2015 REACH
- CBNumber
- CB91516109
- Molecular Formula
- C4H4IN3
- Formula Weight
- 221
- MOL File
- 91416-96-5.mol
5-iodopyrimidin-4-amine Property
- Melting point:
- 188-189 °C
- Boiling point:
- 322.7±27.0 °C(Predicted)
- Density
- 2.204±0.06 g/cm3(Predicted)
- storage temp.
- Keep in dark place,Inert atmosphere,Store in freezer, under -20°C
- pka
- 3.86±0.10(Predicted)
- Appearance
- Light yellow to green yellow Solid
- InChI
- InChI=1S/C4H4IN3/c5-3-1-7-2-8-4(3)6/h1-2H,(H2,6,7,8)
- InChIKey
- HTBFTDHEWCRQPJ-UHFFFAOYSA-N
- SMILES
- C1=NC=C(I)C(N)=N1
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- FA153866
- Product name
- 4-Amino-5-iodopyrimidine
- Packaging
- 100mg
- Price
- $69
- Updated
- 2021/12/16
- Product number
- FA153866
- Product name
- 4-Amino-5-iodopyrimidine
- Packaging
- 250mg
- Price
- $137.5
- Updated
- 2021/12/16
- Product number
- FA153866
- Product name
- 4-Amino-5-iodopyrimidine
- Packaging
- 500mg
- Price
- $240
- Updated
- 2021/12/16
- Product number
- W9386
- Product name
- 4-Amino-5-iodopyrimidine
- Packaging
- 1g
- Price
- $290
- Updated
- 2021/12/16
- Product number
- 072486
- Product name
- 4-Amino-5-iodopyrimidine
- Purity
- 95+%
- Packaging
- 250mg
- Price
- $324
- Updated
- 2021/12/16
5-iodopyrimidin-4-amine Chemical Properties,Usage,Production
Synthesis
163133-86-6
91416-96-5
The general procedure for the synthesis of 4-amino-5-iodopyrimidine from the compound (CAS:163133-86-6) is as follows: 4-aminopyridine (0.970 g, 10.3 mmol) was dissolved in 20 mL of acetic acid, and iodine monochloride (1.67 g, 10.3 mmol, 1.01 eq.) was added to produce a large amount of N-iodine-substituted intermediates precipitate immediately in the reaction system. The reaction mixture was refluxed for 3 hours under argon protection. Upon completion of the reaction, the mixture was cooled to about 10 °C with a water bath to induce complete precipitation of the product. The precipitate was collected by filtration and dried to give 4-amino-5-iodopyrimidine as a pale yellow solid (1.4 g, 62% yield).
References
[1] Heterocycles, 1984, vol. 22, # 5, p. 1195 - 1210
[2] Synthesis (Germany), 2012, vol. 44, # 22, p. 3496 - 3504
[3] Patent: WO2005/30213, 2005, A1. Location in patent: Page/Page column 177
[4] Journal of the Society of Chemical Industry, London, 1950, vol. 69, p. 353
[5] Patent: US6541505, 2003, B1
5-iodopyrimidin-4-amine Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-iodopyrimidin-4-amine manufacturers
- Product
- 5-iodopyrimidin-4-amine 91416-96-5
- Price
- US $1.10/g
- Min. Order
- 1g
- Purity
- 99.00%
- Supply Ability
- 100 Tons Min
- Release date
- 2021-12-06
- Product
- 5-iodopyrimidin-4-amine 91416-96-5
- Price
- US $6.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 1kg, 5kg, 50kg
- Release date
- 2020-01-09