ChemicalBook > CAS DataBase List > 3-CHLORO-4-FLUOROCINNAMIC ACID

3-CHLORO-4-FLUOROCINNAMIC ACID

Product Name: 3-CHLORO-4-FLUOROCINNAMIC ACID
CAS No.: 155814-22-5
Chemical Name: 3-CHLORO-4-FLUOROCINNAMIC ACID
Synonyms: RARECHEM BK HW 0061;3-Chloro-4-fluorocinnamicaci;3-CHLORO-4-FLUOROCINNAMIC ACID;3-(3-chloro-4-fluorophenyl)acrylic acid;3-CHLORO-4-FLUOROCINNAMIC ACID USP/EP/BP;(E)-3-(3-Chloro-4-fluorophenyl)-2-propenoic acid;(2E)-3-(3-chloro-4-fluorophenyl)prop-2-enoic acid;trans-3-(3-Chloro-4-fluorophenyl)-2-propenoic acid;(2E)- 3-(3-chloro-4-fluorophenyl)-2-propenoic acid;3-Chloro-4-fluorocinnamic Acid, Predominantly trans
CBNumber: CB9172254
Molecular Formula: C9H6ClFO2
Formula Weight: 200.59
MOL File: 155814-22-5.mol

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3-CHLORO-4-FLUOROCINNAMIC ACID Property

Melting point:: 173-175°C
Boiling point:: 326℃
Density: 1.420
Flash point:: 151℃
storage temp.: 2-8°C
Appearance: White to off-white Solid

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 26-36
Hazard Note: Harmful
HazardClass: IRRITANT

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Oakwood

Product number: 005637
Product name: 3-Chloro-4-fluorocinnamicacid
Purity: 98%
Packaging: 1g
Price: $20
Updated: 2021/12/16

Oakwood

Product number: 005637
Product name: 3-Chloro-4-fluorocinnamicacid
Purity: 98%
Packaging: 5g
Price: $67
Updated: 2021/12/16

AK Scientific

Product number: 9967AL
Product name: (E)-3-(3-Chloro-4-fluorophenyl)-2-propenoicacid
Packaging: 5g
Price: $126
Updated: 2021/12/16

Oakwood

Product number: 005637
Product name: 3-Chloro-4-fluorocinnamicacid
Purity: 98%
Packaging: 25g
Price: $204
Updated: 2021/12/16

Crysdot

Product number: CD12137940
Product name: 3-Chloro-4-fluorocinnamicacid
Purity: 95+%
Packaging: 100g
Price: $546
Updated: 2021/12/16

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3-CHLORO-4-FLUOROCINNAMIC ACID Chemical Properties,Usage,Production

Uses

3-Chloro-4-fluorocinnamic Acid (CAS# 58537-11-4) can be used to prepare chemokine receptor modulators.

Synthesis

141-82-2

34328-61-5

155814-22-5

GENERAL METHOD: 3-chloro-4-fluorobenzaldehyde (10 mmol), malonic acid (30 mmol, 3.12 g), and piperidine (0.5 mL) were dissolved in pyridine (20 mL), and the reaction mixture was heated under reflux conditions for 4 hours. Upon completion of the reaction, the solution was cooled to room temperature and slowly poured into pre-cooled aqueous 3M HCl solution (100 mL). The precipitated white solid precipitate was collected by filtration and washed sequentially with deionized water (350 mL), 5% w/v NaHCO3 aqueous solution (20 mL) and deionized water (250 mL). The resulting solid was dried in an oven at 60 °C to constant weight. If necessary, the crude product was purified by recrystallization through EtOH/H2O mixed solvent.

References

[1] Tetrahedron, 2016, vol. 72, # 46, p. 7256 - 7262
[2] Journal of Medicinal Chemistry, 2003, vol. 46, # 3, p. 409 - 416

3-CHLORO-4-FLUOROCINNAMIC ACID Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 3-CHLORO-4-FLUOROCINNAMIC ACID manufacturers

Career Henan Chemical Co

Product: 3-CHLORO-4-FLUOROCINNAMIC ACID 155814-22-5
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100KG
Release date: 2020-01-10

155814-22-5, 3-CHLORO-4-FLUOROCINNAMIC ACIDRelated Search:

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RARECHEM BK HW 0061

(E)-3-(3-Chloro-4-fluorophenyl)-2-propenoic acid

trans-3-(3-Chloro-4-fluorophenyl)-2-propenoic acid

3-(3-chloro-4-fluorophenyl)acrylic acid

3-CHLORO-4-FLUOROCINNAMIC ACID

(2E)-3-(3-chloro-4-fluorophenyl)prop-2-enoic acid

2-Propenoic acid, 3-(3-chloro-4-fluorophenyl)-, (2E)-

3-Chloro-4-fluorocinnamicaci

3-CHLORO-4-FLUOROCINNAMIC ACID USP/EP/BP

(2E)- 3-(3-chloro-4-fluorophenyl)-2-propenoic acid

3-Chloro-4-fluorocinnamic Acid, Predominantly trans

155814-22-5

Fluorine series

Cinnamic acid