Ethanone,1-(2-amino-5-chlorophenyl)-
- Product Name
- Ethanone,1-(2-amino-5-chlorophenyl)-
- CAS No.
- 1685-19-4
- Chemical Name
- Ethanone,1-(2-amino-5-chlorophenyl)-
- Synonyms
- 2'-Amino-5'-chloroacetophenone;(2-AMino-5-chlorophenyl)ethanone;Ethanone,1-(2-amino-5-chlorophenyl)-;1-(2-aMino-5-chlorophenyl)ethan-1-one
- CBNumber
- CB92077366
- Molecular Formula
- C8H8ClNO
- Formula Weight
- 169.61
- MOL File
- 1685-19-4.mol
Ethanone,1-(2-amino-5-chlorophenyl)- Property
- Melting point:
- 65-66 °C
- Boiling point:
- 305.1±27.0 °C(Predicted)
- Density
- 1.254±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C(protect from light)
- pka
- 1.67±0.10(Predicted)
- Appearance
- Light yellow to brown Solid
Safety
- HS Code
- 2922390090
N-Bromosuccinimide Price
- Product number
- A617723
- Product name
- 1-(2-Amino-5-chlorophenyl)ethanone
- Packaging
- 500mg
- Price
- $155
- Updated
- 2021/12/16
- Product number
- Y7779
- Product name
- 1-(2-Amino-5-chlorophenyl)ethanone
- Packaging
- 250mg
- Price
- $67
- Updated
- 2021/12/16
- Product number
- FA140484
- Product name
- 1-(2-Amino-5-chlorophenyl)ethanone
- Packaging
- 500mg
- Price
- $85
- Updated
- 2021/12/16
- Product number
- OR918402
- Product name
- 1-(2-Amino-5-chlorophenyl)ethanone
- Purity
- 98%
- Packaging
- 250mg
- Price
- $145
- Updated
- 2021/12/16
- Product number
- FA140484
- Product name
- 1-(2-Amino-5-chlorophenyl)ethanone
- Packaging
- 1g
- Price
- $149
- Updated
- 2021/12/16
Ethanone,1-(2-amino-5-chlorophenyl)- Chemical Properties,Usage,Production
Synthesis
18640-60-3
1685-19-4
(b) A mixture of 1-(5-chloro-2-nitrophenyl)ethanone (4.40 g, 22.05 mmol), PtO2 (40 mg), and activated charcoal (400 mg) in ethanol (80 mL) was subjected to a hydrogen atmosphere with rapid stirring at room temperature for 4.5 hours. Upon completion of the reaction, the mixture was filtered through a diatomaceous earth pad (the residue was washed with dichloromethane) and subsequently concentrated under reduced pressure. The concentrated residue was filtered through a pad of silica gel (eluent was dichloromethane/petroleum ether, 4:1) to give a light green oily substance. The oily substance was recrystallized by ethyl ether/petroleum ether to give 1-(2-amino-5-chlorophenyl)ethanone (3.30 g, 88% yield) as light green crystals.
References
[1] Patent: US2007/238700, 2007, A1. Location in patent: Page/Page column 26
[2] Patent: US2006/63841, 2006, A1. Location in patent: Page/Page column 24; 4/12
[3] Patent: CN102898374, 2016, B. Location in patent: Paragraph 0039; 0040
[4] Journal of Fluorine Chemistry, 2010, vol. 131, # 5, p. 597 - 605
[5] Journal of Organic Chemistry, 2007, vol. 72, # 18, p. 6873 - 6877
Ethanone,1-(2-amino-5-chlorophenyl)- Preparation Products And Raw materials
Raw materials
Preparation Products
Ethanone,1-(2-amino-5-chlorophenyl)- Suppliers
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View Lastest Price from Ethanone,1-(2-amino-5-chlorophenyl)- manufacturers
- Product
- 2-Amino-5-chloroacetophenone 1685-19-4
- Price
- US $1.10-9.90/KG
- Min. Order
- 1KG
- Purity
- 99% min
- Supply Ability
- 100kg
- Release date
- 2025-08-18
- Product
- Ethanone,1-(2-amino-5-chlorophenyl)- 1685-19-4
- Price
- US $1.00/g
- Min. Order
- 1g
- Purity
- 99%
- Supply Ability
- 10000KGS
- Release date
- 2020-01-14