ChemicalBook > CAS DataBase List > 2-BROMO-4-METHYL-6-NITROANILINE

2-BROMO-4-METHYL-6-NITROANILINE

Product Name
2-BROMO-4-METHYL-6-NITROANILINE
CAS No.
827-24-7
Chemical Name
2-BROMO-4-METHYL-6-NITROANILINE
Synonyms
2-BROMO-4-METHYL-6-NITROANILINE;2-BROMO-4-METHYL-6-NITROBENZENAMINE;2-BROMO-4-METHYL-6-NITRO-PHENYLAMINE;Benzenamine, 2-bromo-4-methyl-6-nitro-;4-Amino-3-bromo-5-nitrotoluene, 2-Bromo-6-nitro-p-toluidine
CBNumber
CB9231193
Molecular Formula
C7H7BrN2O2
Formula Weight
231.05
MOL File
827-24-7.mol
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2-BROMO-4-METHYL-6-NITROANILINE Property

Melting point:
64-66
Boiling point:
329.1±37.0 °C(Predicted)
Density 
1.698±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
-1.74±0.25(Predicted)
Appearance
Light brown to orange Solid
InChI
InChI=1S/C7H7BrN2O2/c1-4-2-5(8)7(9)6(3-4)10(11)12/h2-3H,9H2,1H3
InChIKey
VFPKZASVVCBVMG-UHFFFAOYSA-N
SMILES
C1(N)=C([N+]([O-])=O)C=C(C)C=C1Br
CAS DataBase Reference
827-24-7(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
HazardClass 
IRRITANT
HS Code 
2921420090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
B677970
Product name
2-Bromo-4-methyl-6-nitroaniline
Packaging
50mg
Price
$60
Updated
2021/12/16
SynQuest Laboratories
Product number
4755-9-X0
Product name
2-Bromo-4-methyl-6-nitroaniline
Packaging
5G
Price
$52
Updated
2021/12/16
AK Scientific
Product number
V7891
Product name
2-Bromo-4-methyl-6-nitroaniline
Packaging
25g
Price
$94
Updated
2021/12/16
SynQuest Laboratories
Product number
4755-9-X0
Product name
2-Bromo-4-methyl-6-nitroaniline
Packaging
25g
Price
$180
Updated
2021/12/16
Matrix Scientific
Product number
045534
Product name
2-Bromo-4-methyl-6-nitroaniline
Purity
>95%
Packaging
500mg
Price
$181
Updated
2021/12/16
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2-BROMO-4-METHYL-6-NITROANILINE Chemical Properties,Usage,Production

Synthesis

89-62-3

827-24-7

4-Methyl-2-nitroaniline (131.2 g, 862 mmol) was used as a raw material and suspended in glacial acetic acid (1.25 L). Bromine (54 mL, 1.05 mol) was added slowly over 1 h at ambient temperature. After addition, the reaction mixture was continued to be stirred for 1 hour. Subsequently, the reaction solution was poured into water (7.5 L) and the suspension was stirred for 30 minutes. The solid product was collected by filtration, washed thoroughly with water (5 x 1 L) and dried to give 2-bromo-4-methyl-6-nitroaniline (187.2 g, 94%) as an orange solid. Its 1H NMR (CDCl3) data were as follows: δ 7.94 (1H, s), 7.56 (1H, s), 6.47 (2H, br s), 2.27 (3H, s).

References

[1] Organic Letters, 2006, vol. 8, # 22, p. 4989 - 4992
[2] Chemistry - A European Journal, 2015, vol. 21, # 52, p. 18915 - 18920
[3] Journal of Labelled Compounds and Radiopharmaceuticals, 1995, vol. 36, # 3, p. 281 - 288
[4] Journal of Antibiotics, 1994, vol. 47, # 12, p. 1456 - 1465
[5] Bioorganic and Medicinal Chemistry, 2011, vol. 19, # 20, p. 6026 - 6032

2-BROMO-4-METHYL-6-NITROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-4-METHYL-6-NITROANILINE Suppliers

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View Lastest Price from 2-BROMO-4-METHYL-6-NITROANILINE manufacturers

Career Henan Chemical Co
Product
2-BROMO-4-METHYL-6-NITROANILINE 827-24-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
100KG
Release date
2020-01-09

827-24-7, 2-BROMO-4-METHYL-6-NITROANILINERelated Search:

4-bromo-N-methyl-2-nitroaniline 2-bromo-4-methyl-5-nitroaniline 2-bromo-N-methyl-4-nitroaniline 4-Bromo-2-Methyl-6-Nitroaniline98% 3-bromo-4-methyl-5-nitroaniline 4-BROMO-2-METHYL-6-NITROANILINE 2-BROMO-6-METHYL-4-NITROANILINE,2-BROMO-6-METHYL-4-NITROANILINE 98% 2-BROMO-4-TRIFLUOROMETHYL-6-NITROPHENYLISOTHIO-CYANATE METHYL 4-AMINO-3-BROMO-5-NITROBENZENECARBOXYLATE N-(6-BROMO-2,3-DIHYDRO-4-NITRO-1-OXO-1H-INDEN-5-YL)ACETAMIDE BUTTPARK 62\11-04 4-AMINO-3-BROMO-5-NITROBENZOTRIFLUORIDE 2-BROMO-4-METHYL-6-NITROANILINE

  • 2-BROMO-4-METHYL-6-NITRO-PHENYLAMINE
  • 2-BROMO-4-METHYL-6-NITROANILINE
  • 2-BROMO-4-METHYL-6-NITROBENZENAMINE
  • 4-Amino-3-bromo-5-nitrotoluene, 2-Bromo-6-nitro-p-toluidine
  • Benzenamine, 2-bromo-4-methyl-6-nitro-
  • 827-24-7
  • Amines
  • blocks
  • Bromides