2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER

Product Name: 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
CAS No.: 142896-15-9
Chemical Name: 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
Synonyms: 6-diMethylpyridine-4-carboxylate;Methyl 2,6-diMethylisonicotinate;2,6- DI METHYL PYRIDINE -4-CARBOXYLATE;Methyl 2,6-diMethylpyridine-4-carboxylate;Methyl 2,6-dimethyl-4-pyridinecarboxylate;2,6-Dimethyl-isonicotinic acid methyl ester;2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER;4-Pyridinecarboxylic acid, 2,6-diMethyl-, Methyl ester;Methyl 2,6-dimethylpyridine-4-carboxylate, 2,6-Dimethyl-4-(methoxycarbonyl)pyridine
CBNumber: CB92464803
Molecular Formula: C9H11NO2
Formula Weight: 165.19
MOL File: 142896-15-9.mol

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2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Property

Melting point:: 45 °C
Boiling point:: 238.1±35.0 °C(Predicted)
Density: 1.078±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 4.55±0.10(Predicted)
Appearance: White to off-white Solid

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Safety

HS Code: 2933399990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: M221938
Product name: Methyl2,6-Dimethylisonicotinate
Packaging: 5mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M221938
Product name: Methyl2,6-Dimethylisonicotinate
Packaging: 50mg
Price: $220
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4H23-1-Y2
Product name: Methyl 2,6-dimethylisonicotinate
Packaging: 250mg
Price: $248
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0398447
Product name: 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER
Purity: 95.00%
Packaging: 5MG
Price: $505.8
Updated: 2021/12/16

Matrix Scientific

Product number: 189072
Product name: Methyl 2,6-dimethylpyridine-4-carboxylate
Packaging: 1g
Price: $743
Updated: 2021/12/16

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2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Chemical Properties,Usage,Production

Synthesis

42521-09-5

544-97-8

142896-15-9

A mixture of methyl 2,6-dichloropyridine-4-carboxylate (2.00 g), dimethylzinc (2N toluene solution, 14.6 mL, 3.0 eq.), and PdCl2(dppf)2 (400 mg, 0.05 eq.) in dioxane (50 mL) was heated for 4 hr. at 80 °C under inert atmosphere. Upon completion of the reaction, the reaction mixture was cooled through an ice bath, quenched with water (100 mL) and filtered through a diatomaceous earth pad. The diatomaceous earth pad was rinsed with water and ethyl acetate (EtOAc). The filtrate was extracted with ethyl acetate (250 mL) and the organic layer was washed with brine (100 mL), dried over anhydrous magnesium sulfate (MgSO4) and concentrated. Purification by fast chromatography (methanol gradient in dichloromethane, 0 to 2%) afforded compound 99 (methyl 2,6-dimethylisonicotinate) as an orange oil in 96% yield.1H-NMR (400 MHz, DMSO): δ 2.51 (s, 6H, 2×CH3), 3.88 (s, 3H, O-CH3), 7.51 (s, 2H, Ar). Mass spectrum (M+H)+ m/z = 166.1.

References

[1] Patent: EP2666775, 2013, A1. Location in patent: Paragraph 0390
[2] Patent: WO2013/174822, 2013, A1. Location in patent: Page/Page column 137

2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Preparation Products And Raw materials

Raw materials

Preparation Products

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2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER Suppliers

China 45 Germany 1 India 2 United Kingdom 1 United States 5 Global 54

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Amadis Chemical Company Limited

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View Lastest Price from 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER manufacturers

Career Henan Chemical Co

Product: 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER 142896-15-9
Price: US $1.00/KG
Min. Order: 1KG
Purity: 97%
Supply Ability: 100kg
Release date: 2020-02-01

142896-15-9, 2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTERRelated Search:

2,6-DIMETHYLPIPERIDIN-4-ONE HYDROCHLORIDE 2,6-DIMETHYL-PYRIDINE-3-CARBALDEHYDE

Methyl 2,6-diMethylisonicotinate

6-diMethylpyridine-4-carboxylate

2,6-DIMETHYLPYRIDINE-4-CARBOXYLIC ACID METHYL ESTER

4-Pyridinecarboxylic acid, 2,6-diMethyl-, Methyl ester

Methyl 2,6-dimethylpyridine-4-carboxylate, 2,6-Dimethyl-4-(methoxycarbonyl)pyridine

Methyl 2,6-diMethylpyridine-4-carboxylate

2,6-Dimethyl-isonicotinic acid methyl ester

Methyl 2,6-dimethyl-4-pyridinecarboxylate

2,6- DI METHYL PYRIDINE -4-CARBOXYLATE

142896-15-9