3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid
- Product Name
- 3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid
- CAS No.
- 946152-72-3
- Chemical Name
- 3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid
- Synonyms
- Reaxys ID: 15523810;3-(tert-Butoxycarbonylami...;3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid;3-{[(tert-butoxy)carbonyl]amino}cyclobutane-1-carboxylic acid;3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid - B0234;3-{[(tert-butoxy)carbonyl]amino}cyclobutane-1-carboxylic aci...;3-[[(1,1-Dimethylethoxy)carbonyl]amino]cyclobutanecarboxylic acid;Cyclobutanecarboxylic acid, 3-[[(1,1-dimethylethoxy)carbonyl]amino]-
- CBNumber
- CB92485482
- Molecular Formula
- C10H17NO4
- Formula Weight
- 215.25
- MOL File
- 946152-72-3.mol
3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid Property
- Boiling point:
- 368.3±31.0 °C(Predicted)
- Density
- 1.17±0.1 g/cm3(Predicted)
- storage temp.
- 2-8°C
- pka
- 4.58±0.40(Predicted)
- Appearance
- White to off-white Solid
Safety
- HS Code
- 2924297099
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P321Specific treatment (see … on this label).
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P362Take off contaminated clothing and wash before reuse.
N-Bromosuccinimide Price
- Product number
- 4258-1-35
- Product name
- 3-{[(tert-Butoxy)carbonyl]amino}cyclobutane-1-carboxylic acid
- Purity
- 97.0%
- Packaging
- 250mg
- Price
- $115
- Updated
- 2021/12/16
- Product number
- 4258-1-35
- Product name
- 3-{[(tert-Butoxy)carbonyl]amino}cyclobutane-1-carboxylic acid
- Purity
- 97.0%
- Packaging
- 1g
- Price
- $290
- Updated
- 2021/12/16
- Product number
- 068589
- Product name
- 3-(tert-Butoxycarbonylamino)-cyclobutanecarboxylic acid
- Purity
- >95%
- Packaging
- 500mg
- Price
- $387
- Updated
- 2021/12/16
- Product number
- Y4811
- Product name
- 3-(tert-Butoxycarbonylamino)cyclobutanecarboxylicacid
- Packaging
- 10g
- Price
- $412
- Updated
- 2021/12/16
- Product number
- CHM0382206
- Product name
- 3-(TERT-BUTOXYCARBONYLAMINO)CYCLOBUTANECARBOXYLIC ACID
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $497.06
- Updated
- 2021/12/16
3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid Chemical Properties,Usage,Production
Synthesis
946152-71-2
946152-72-3
Step 2: To a solution of ethyl 3-((tert-butoxycarbonyl)amino)cyclobutanecarboxylate (0.4 g, 1.64 mmol) in tetrahydrofuran (6.5 mL) was added a solution of lithium hydroxide monohydrate (0.138 g, 3.28 mmol) in water (6.5 mL), and the reaction mixture was stirred at room temperature overnight. After completion of the reaction, the reaction mixture was washed with ether (20 mL) and the aqueous phase was acidified with 1 M potassium bisulfate. The product was extracted with ethyl acetate (3×20 mL), the organic phase was dried with anhydrous magnesium sulfate, and concentrated under reduced pressure to give 3-(Boc-amino)cyclobutanecarboxylic acid (0.335 g, 95%) as a white crystalline solid: no molecular ion peaks were observed in the mass spectra.
References
[1] Patent: US2007/191406, 2007, A1. Location in patent: Page/Page column 37
3-(tert-Butoxycarbonylamino)cyclobutanecarboxylic acid Preparation Products And Raw materials
Raw materials
Preparation Products
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