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2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE

Product Name
2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE
CAS No.
73225-15-7
Chemical Name
2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE
Synonyms
1-(4-nitrophenyl)-2-Methylimidazole;2-methyl-1-(4-nitrophenyl)imidazole;2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE;1H-Imidazole, 2-methyl-1-(4-nitrophenyl)-;2-Methyl-1-(4-nitrophenyl)-1H-imidazole95%
CBNumber
CB9255182
Molecular Formula
C10H9N3O2
Formula Weight
203.2
MOL File
73225-15-7.mol
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2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE Property

Melting point:
138-139 °C
Boiling point:
396.5±44.0 °C(Predicted)
Density 
1.29±0.1 g/cm3(Predicted)
storage temp. 
Sealed in dry,Room Temperature
pka
6.17±0.10(Predicted)
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Matrix Scientific
Product number
071884
Product name
2-Methyl-1-(4-nitrophenyl)-1H-imidazole
Purity
95+%
Packaging
1g
Price
$139
Updated
2021/12/16
AK Scientific
Product number
W8149
Product name
2-Methyl-1-(4-nitrophenyl)-1H-imidazole
Packaging
1g
Price
$104
Updated
2021/12/16
Matrix Scientific
Product number
071884
Product name
2-Methyl-1-(4-nitrophenyl)-1H-imidazole
Purity
95+%
Packaging
5g
Price
$360
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
COR0001803
Product name
2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE
Purity
95.00%
Packaging
1G
Price
$440
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
COR0001803
Product name
2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE
Purity
95.00%
Packaging
5G
Price
$520
Updated
2021/12/16
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2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE Chemical Properties,Usage,Production

Synthesis

693-98-1

350-46-9

73225-15-7

General procedure: 1-fluoro-4-nitrobenzene (10 g, 70.9 mmol), 2-methyl-1H-imidazole (5.8 g, 70.9 mmol) and cesium carbonate (Cs2CO3, 34.7 g, 106.4 mmol) were placed in degassed N,N-dimethylformamide (DMF, 200 mL). The mixture was heated to 100 °C and stirred overnight under nitrogen protection. The progress of the reaction was monitored by thin layer chromatography (TLC) and after confirming the complete consumption of 1-fluoro-4-nitrobenzene, the reaction mixture was concentrated under reduced pressure. Water (300 mL) was added to the concentrated residue and a gray precipitate was precipitated, which was separated by filtration to afford the target compound 2-methyl-1-(4-nitrophenyl)-1H-imidazole (12.8 g, 89% yield).

References

[1] Advanced Synthesis and Catalysis, 2016, vol. 358, # 4, p. 597 - 609
[2] Patent: WO2011/75478, 2011, A1. Location in patent: Page/Page column 53
[3] Patent: WO2009/71888, 2009, A1. Location in patent: Page/Page column 83
[4] Patent: US5298520, 1994, A
[5] Journal of Medicinal Chemistry, 1995, vol. 38, # 10, p. 1799 - 1810

2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE Suppliers

Shanghai Litong Chemical Technology Co.,Ltd.
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Aikon International Limited
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View Lastest Price from 2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE manufacturers

Career Henan Chemica Co
Product
2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE 73225-15-7
Price
US $1.00/g
Min. Order
1g
Purity
85.0-99.8%
Supply Ability
20tons
Release date
2020-10-28

73225-15-7, 2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLERelated Search:


  • 2-METHYL-1-(4-NITROPHENYL)-1H-IMIDAZOLE
  • 2-Methyl-1-(4-nitrophenyl)-1H-imidazole95%
  • 1-(4-nitrophenyl)-2-Methylimidazole
  • 1H-Imidazole, 2-methyl-1-(4-nitrophenyl)-
  • 2-methyl-1-(4-nitrophenyl)imidazole
  • 73225-15-7
  • API intermediates