4-Methyl-3-(hydroxyMethyl)Morpholine

Product Name: 4-Methyl-3-(hydroxyMethyl)Morpholine
CAS No.: 1159598-86-3
Chemical Name: 4-Methyl-3-(hydroxyMethyl)Morpholine
Synonyms: 4-Methyl-3-morpholinemethanol;3-Morpholinemethanol, 4-methyl-;(4-Methylmorpholin-3-yl)methanol;4-Methyl-3-(hydroxyMethyl)Morpholine
CBNumber: CB92629985
Molecular Formula: C6H13NO2
Formula Weight: 131.17
MOL File: 1159598-86-3.mol

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4-Methyl-3-(hydroxyMethyl)Morpholine Property

Boiling point:: 201.1±15.0 °C(Predicted)
Density: 1.031±0.06 g/cm3(Predicted)
storage temp.: 2-8°C
pka: 14.85±0.10(Predicted)
Appearance: Colorless to light yellow Liquid

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Safety

HS Code: 2934999090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B585958
Product name: 4-Methyl-3-(hydroxymethyl)morpholine
Packaging: 100mg
Price: $240
Updated: 2021/12/16

ChemScene

Product number: CS-0061777
Product name: (4-Methylmorpholin-3-yl)methanol
Packaging: 100mg
Price: $93
Updated: 2021/12/16

ChemScene

Product number: CS-0061777
Product name: (4-Methylmorpholin-3-yl)methanol
Packaging: 250mg
Price: $155
Updated: 2021/12/16

ChemScene

Product number: CS-0061777
Product name: (4-Methylmorpholin-3-yl)methanol
Packaging: 1g
Price: $309
Updated: 2021/12/16

Apolloscientific

Product number: OR55495
Product name: 4-Methyl-3-(hydroxymethyl)morpholine
Purity: 95%
Packaging: 1g
Price: $432
Updated: 2021/12/16

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4-Methyl-3-(hydroxyMethyl)Morpholine Chemical Properties,Usage,Production

Synthesis

50-00-0

106910-83-2

1159598-86-3

Step 2: Preparation of (4-methylmorpholin-3-yl)methanol To a solution of morpholin-3-ylmethanol (0.540 g, 4.6 mmol) in methanol (20 mL) was added formaldehyde (1.86 g, 23 mmol, 37% aqueous solution) and palladium/carbon catalyst (0.200 g). The reaction mixture was stirred overnight at room temperature under hydrogen atmosphere (1.0 atm). Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth pad and the filtrate was concentrated under reduced pressure. The residue was purified by silica gel column chromatography (eluent ratio: methanol:dichloromethane=1:15) to afford (4-methylmorpholin-3-yl)methanol (0.130 g, 22% yield) as a yellow oil.

References

[1] Patent: US2016/168090, 2016, A1. Location in patent: Paragraph 0927-0928

4-Methyl-3-(hydroxyMethyl)Morpholine Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 4-Methyl-3-(hydroxyMethyl)Morpholine manufacturers

Nanjing jinheyou Trading Co., Ltd.

Product: 4-Methyl-3-(hydroxyMethyl)Morpholine 1159598-86-3
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 20kg/month
Release date: 2019-11-19

Nanjing jinheyou Trading Co., Ltd.

Product: 4-Methyl-3-(hydroxyMethyl)Morpholine 1159598-86-3
Price: US $0.00/g
Min. Order: 1g
Purity: 95%min
Supply Ability: 20kg/month
Release date: 2019-11-19

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1159598-86-3