1,10-Phenanthroline, 4,7-dibroMo-
- Product Name
- 1,10-Phenanthroline, 4,7-dibroMo-
- CAS No.
- 156492-30-7
- Chemical Name
- 1,10-Phenanthroline, 4,7-dibroMo-
- Synonyms
- 4,7-dibromo;4,7-DibroMophenanthroline;4,7-dibromo-1,1-phenanthroline;1,10-Phenthroline, 4,7-dibroMo-;1,10-Phenanthroline, 4,7-dibroMo-;4,7-Dibromo-1,10-phenanthroline Hydrate
- CBNumber
- CB92637717
- Molecular Formula
- C12H6Br2N2
- Formula Weight
- 338
- MOL File
- 156492-30-7.mol
1,10-Phenanthroline, 4,7-dibroMo- Property
- Melting point:
- 236℃
- Boiling point:
- 466.6±40.0 °C(Predicted)
- Density
- 1.915±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2-8°C
- form
- powder to crystal
- pka
- 3.29±0.10(Predicted)
- color
- White to Yellow
- InChI
- InChI=1S/C12H6Br2N2/c13-9-3-5-15-11-7(9)1-2-8-10(14)4-6-16-12(8)11/h1-6H
- InChIKey
- AKZAIDYHEKUXBU-UHFFFAOYSA-N
- SMILES
- N1C2C(=CC=C3C=2N=CC=C3Br)C(Br)=CC=1
Safety
- HS Code
- 2933.99.8290
N-Bromosuccinimide Price
- Product number
- D4987
- Product name
- 4,7-Dibromo-1,10-phenanthroline Hydrate
- Purity
- >98.0%(HPLC)
- Packaging
- 200mg
- Price
- $129
- Updated
- 2025/07/31
- Product number
- D4987
- Product name
- 4,7-Dibromo-1,10-phenanthroline Hydrate
- Purity
- >98.0%(HPLC)
- Packaging
- 1g
- Price
- $442
- Updated
- 2025/07/31
- Product number
- D428060
- Product name
- 4,7-Dibromo-1,10-phenanthroline
- Packaging
- 5mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- 40993
- Product name
- 4,7-Dibromo-1,10-phenanthroline,98%(HPLC)
- Purity
- 98%(HPLC)
- Packaging
- 200MG
- Price
- $153.44
- Updated
- 2021/12/16
- Product number
- 40993
- Product name
- 4,7-Dibromo-1,10-phenanthroline,98%(HPLC)
- Purity
- 98%(HPLC)
- Packaging
- 1G
- Price
- $581.28
- Updated
- 2021/12/16
1,10-Phenanthroline, 4,7-dibroMo- Chemical Properties,Usage,Production
Synthesis
87330-27-6
156492-30-7
1,10-Phenanthroline-4,7(1H,10H)-dione (73c, 4.2 g, 20 mmol) was used as a feedstock and mixed with tribromophosphine (14.3 g, 50 mmol) in anhydrous chloroform. The reaction mixture was refluxed for 6 hours under nitrogen protection. Upon completion of the reaction, the reaction solution was washed with water followed by saturated brine three times. The organic layer was dried with anhydrous magnesium sulfate and the solvent was removed by evaporation. Finally, the crude product was purified by silica gel column chromatography to afford 4,7-dibromo-1,10-phenanthroline (73d, 4.7 g, 13.9 mmol) in 70% yield.
References
[1] Patent: CN106831743, 2017, A. Location in patent: Paragraph 0129; 0134; 0135
[2] Journal of Organic Chemistry, 1951, vol. 16, p. 941,945
[3] Tetrahedron, 2002, vol. 58, # 44, p. 9095 - 9100
1,10-Phenanthroline, 4,7-dibroMo- Preparation Products And Raw materials
Raw materials
Preparation Products
1,10-Phenanthroline, 4,7-dibroMo- Suppliers
- Tel
- 320-37350700
- Fax
- +32 (0)37350701
- sales@tcieurope.eu
- Country
- Europe
- ProdList
- 23671
- Advantage
- 75
View Lastest Price from 1,10-Phenanthroline, 4,7-dibroMo- manufacturers
- Product
- 4,7-dibromo-1,10-phenanthroline 156492-30-7
- Price
- US $223.00-746.00/g
- Min. Order
- 1g
- Purity
- 0.98
- Supply Ability
- 20
- Release date
- 2023-09-14
- Product
- 1,10-Phenanthroline, 4,7-dibroMo- 156492-30-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 200kg
- Release date
- 2020-01-08