6-METHOXYQUINAZOLIN-4-OL
- Product Name
- 6-METHOXYQUINAZOLIN-4-OL
- CAS No.
- 19181-64-7
- Chemical Name
- 6-METHOXYQUINAZOLIN-4-OL
- Synonyms
- 6-METHOXYQUINAZOLIN-4-OL;6-methoxy-1H-quinazolin-4-one;6-methoxy-3H-quinazolin-4-one;6-Methoxyquinazolin-4(3H)-one;6-Methoxy-4(3H)-quinazolinone;6-METHOXY-4(1H)-QUINAZOLINONE;6-methoxy-4 (1H) - quinazolone;4(1H)-Quinazolinone, 6-methoxy-;4(3H)-Quinazolinone, 6-methoxy-;6-Methoxy-1,4-dihydroquinazolin-4-one
- CBNumber
- CB9278705
- Molecular Formula
- C9H8N2O2
- Formula Weight
- 176.17
- MOL File
- 19181-64-7.mol
6-METHOXYQUINAZOLIN-4-OL Property
- Melting point:
- 242-243℃
- Boiling point:
- 361.8±44.0 °C(Predicted)
- Density
- 1.32
- storage temp.
- Sealed in dry,Room Temperature
- pka
- 1.95±0.20(Predicted)
- Appearance
- Off-white to brown Solid
Safety
- HS Code
- 2933998090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- M269553
- Product name
- 6-Methoxy-1,4-dihydroquinazolin-4-one
- Packaging
- 100mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- M269553
- Product name
- 6-Methoxy-1,4-dihydroquinazolin-4-one
- Packaging
- 500mg
- Price
- $200
- Updated
- 2021/12/16
- Product number
- OR926223
- Product name
- 6-Methoxyquinazolin-4-ol
- Purity
- 98%
- Packaging
- 1g
- Price
- $165
- Updated
- 2021/12/16
- Product number
- W4116
- Product name
- 6-Methoxyquinazolin-4-ol
- Packaging
- 1g
- Price
- $235
- Updated
- 2021/12/16
- Product number
- 126368
- Product name
- 6-Methoxyquinazolin-4-ol
- Purity
- >95%
- Packaging
- 1g
- Price
- $252
- Updated
- 2021/12/16
6-METHOXYQUINAZOLIN-4-OL Chemical Properties,Usage,Production
Synthesis
54413-93-3
6313-33-3
19181-64-7
In a 10 mL glass tube, 2-iodo-5-methoxybenzoic acid (1.0 mmol), formamidine hydrochloride (1.2 mmol), CuCl2 (0.1 mmol), ligand L2 (0.1 mmol), and NaOH (4.0 eq.) were added sequentially, followed by 3.0 mL of water. After sealing the reaction vessel with a septum, it was placed in a microwave reactor. Using a CEM Discover microwave synthesizer, microwave radiation was applied at 120 W for 20 min at room temperature, during which the reaction mixture was kept continuously stirred. After completion of the reaction, the solvent was removed by distillation under reduced pressure. The crude product was purified by silica gel column chromatography to afford 6-methoxy-4(1H)-quinazolinone. All products were analyzed by nuclear magnetic resonance (NMR) and mass spectrometry (MS) to confirm their structures.
References
[1] Synthetic Communications, 2018, vol. 48, # 24, p. 3089 - 3098
6-METHOXYQUINAZOLIN-4-OL Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 6-METHOXYQUINAZOLIN-4-OL manufacturers
- Product
- 6-METHOXYQUINAZOLIN-4-OL 19181-64-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-09