(2-BROMOBENZYL)METHYLAMINE
- Product Name
- (2-BROMOBENZYL)METHYLAMINE
- CAS No.
- 698-19-1
- Chemical Name
- (2-BROMOBENZYL)METHYLAMINE
- Synonyms
- SKL295;(2-BROMOBENZYL)METHY;(2-BROMOBENZYL)METHYLAMINE;2-BROMO-N-METHYLBENZYLAMINE;N-Methyl-2-bromobenzylamine;(2-Bromobenzyl)methylamine95%;2-(2-broMophenyl)ethan-1-aMine;2-Bromo-N-methylbenzylamine 97%;2-Bromo-N-methylbenzylamine;2-Bromo-N-methyl-Benzenemethanamine
- CBNumber
- CB9313802
- Molecular Formula
- C8H10BrN
- Formula Weight
- 200.08
- MOL File
- 698-19-1.mol
(2-BROMOBENZYL)METHYLAMINE Property
- Boiling point:
- 71-74 °C2 mm Hg(lit.)
- Density
- 1.358 g/mL at 25 °C(lit.)
- refractive index
- n20/D 1.5670(lit.)
- Flash point:
- 220 °F
- storage temp.
- Keep in dark place,Inert atmosphere,Room temperature
- form
- Viscous Liquid
- pka
- 9.14±0.10(Predicted)
- Appearance
- Colorless to light yellow Liquid
- Sensitive
- Air Sensitive
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H412Harmful to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 631167
- Product name
- 2-Bromo-N-methylbenzylamine
- Purity
- 97%
- Packaging
- 1g
- Price
- $97
- Updated
- 2023/01/07
- Product number
- 631167
- Product name
- 2-Bromo-N-methylbenzylamine
- Purity
- 97%
- Packaging
- 5g
- Price
- $241
- Updated
- 2023/01/07
- Product number
- M296623
- Product name
- N-Methyl-2-bromobenzylamine
- Packaging
- 50mg
- Price
- $45
- Updated
- 2021/12/16
- Product number
- FB153661
- Product name
- (2-Bromobenzyl)methylamine
- Packaging
- 1g
- Price
- $54
- Updated
- 2021/12/16
- Product number
- FB153661
- Product name
- (2-Bromobenzyl)methylamine
- Packaging
- 5G
- Price
- $187.5
- Updated
- 2021/12/16
(2-BROMOBENZYL)METHYLAMINE Chemical Properties,Usage,Production
Synthesis
6630-33-7
698-19-1
Preparation of Example (Compound 22a): 29.4 g of o-bromobenzaldehyde and 81 mL of 40% aqueous methylamine were mixed with 238 mL of tetrahydrofuran (THF). At room temperature, 19 g of sodium borohydride (NaBH4) was added in batches over 25 minutes. The reaction mixture was stirred overnight at room temperature and then concentrated using a rotary evaporator. The residue was stirred into ice water and the aqueous phase was extracted twice with ether. The combined ether phases were concentrated by evaporation under reduced pressure. The product was purified by silica gel column chromatography using ethyl acetate or ethyl acetate/methanol (4:1) as eluent to give 18.5 g of N-methyl-2-bromobenzylamine (22a) in yellow liquid form. Yield: 58%.
References
[1] Patent: US6232468, 2001, B1
[2] Tetrahedron, 2003, vol. 59, # 40, p. 8049 - 8056
(2-BROMOBENZYL)METHYLAMINE Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (2-BROMOBENZYL)METHYLAMINE manufacturers
- Product
- (2-BROMOBENZYL)METHYLAMINE 698-19-1
- Price
- US $0.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 150KG
- Release date
- 2019-07-01