SALOR-INT L164526-1EA
- Product Name
- SALOR-INT L164526-1EA
- CAS No.
- 33515-62-7
- Chemical Name
- SALOR-INT L164526-1EA
- Synonyms
- SALOR-INT L164526-1EA;4-Iodopyrrole-2-carbaldehyde;4-Iodopyrrole-2-carboxaldehyde;4-IODO-1H-PYRROLE-2-CARBALDEHYDE;4-iodo-1H-Pyrrole-2-carboxaldehyde;1H-Pyrrole-2-carboxaldehyde, 4-iodo-
- CBNumber
- CB9341403
- Molecular Formula
- C5H4INO
- Formula Weight
- 221
- MOL File
- 33515-62-7.mol
SALOR-INT L164526-1EA Property
- Melting point:
- 117-118 °C(Solv: dichloromethane (75-09-2); hexane (110-54-3))
- Boiling point:
- 319.3±27.0 °C(Predicted)
- Density
- 2.177±0.06 g/cm3(Predicted)
- storage temp.
- under inert gas (nitrogen or Argon) at 2–8 °C
- pka
- 13.70±0.50(Predicted)
- Appearance
- White to off-white Solid
- InChI
- InChI=1S/C5H4INO/c6-4-1-5(3-8)7-2-4/h1-3,7H
- InChIKey
- AEYJSULNKPFTAP-UHFFFAOYSA-N
- SMILES
- N1C=C(I)C=C1C=O
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
N-Bromosuccinimide Price
- Product number
- I719493
- Product name
- 4-Iodo-1H-pyrrole-2-carbaldehyde
- Packaging
- 100mg
- Price
- $60
- Updated
- 2021/12/16
- Product number
- I719493
- Product name
- 4-Iodo-1H-pyrrole-2-carbaldehyde
- Packaging
- 500mg
- Price
- $110
- Updated
- 2021/12/16
- Product number
- 120051
- Product name
- 4-Iodo-1H-pyrrole-2-carbaldehyde
- Purity
- 95+%
- Packaging
- 1g
- Price
- $270
- Updated
- 2021/12/16
- Product number
- Y8757
- Product name
- 4-Iodo-1H-pyrrole-2-carbaldehyde
- Packaging
- 25g
- Price
- $328
- Updated
- 2021/12/16
- Product number
- HCH0323156
- Product name
- 4-IODO-1H-PYRROLE-2-CARBALDEHYDE
- Purity
- 95.00%
- Packaging
- 5MG
- Price
- $496.44
- Updated
- 2021/12/16
SALOR-INT L164526-1EA Chemical Properties,Usage,Production
Synthesis
1003-29-8
33515-62-7
General procedure for the synthesis of 4-iodo-1H-pyrrole-2-carbaldehyde from 2-pyrrolecarboxaldehyde: 1H-pyrrole-2-carbaldehyde (7.0 g, 73.6 mmol) was dissolved in tetrahydrofuran (45 mL) and the solution was cooled to -75 °C. N-iodosuccinimide (19.8 g, 88.3 mmol) was added in batches over 20 minutes, followed by continuous stirring of the reaction mixture at -75 °C for 2 hours. Upon completion of the reaction, water and petroleum ether were added and the mixture was slowly warmed to room temperature. The organic layer was separated and the aqueous phase was extracted with petroleum ether. All organic layers were combined, washed sequentially with water and brine, dried with anhydrous sodium sulfate, filtered and concentrated under vacuum to afford 4-iodo-1H-pyrrole-2-carbaldehyde (13.2 g, 81% yield) as a black solid.
References
[1] Patent: WO2009/130481, 2009, A1. Location in patent: Page/Page column 107
[2] Bioorganic and Medicinal Chemistry Letters, 2003, vol. 13, # 24, p. 4515 - 4518
SALOR-INT L164526-1EA Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from SALOR-INT L164526-1EA manufacturers
- Product
- SALOR-INT L164526-1EA 33515-62-7
- Price
- US $1.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 20T
- Release date
- 2024-08-14
- Product
- 4-IODO-1H-PYRROLE-2-CARBALDEHYDE 33515-62-7
- Price
- US $6.86/KG
- Min. Order
- 1KG
- Purity
- 95.0%-99.0%
- Supply Ability
- 1kg-100kg
- Release date
- 2020-03-10
- Product
- SALOR-INT L164526-1EA 33515-62-7
- Price
- US $6.68/KG
- Min. Order
- 1KG
- Purity
- 97%-99%
- Supply Ability
- 1kg-1000kg
- Release date
- 2020-01-10