ChemicalBook > CAS DataBase List > SALOR-INT L164526-1EA

SALOR-INT L164526-1EA

Product Name
SALOR-INT L164526-1EA
CAS No.
33515-62-7
Chemical Name
SALOR-INT L164526-1EA
Synonyms
SALOR-INT L164526-1EA;4-Iodopyrrole-2-carbaldehyde;4-Iodopyrrole-2-carboxaldehyde;4-IODO-1H-PYRROLE-2-CARBALDEHYDE;4-iodo-1H-Pyrrole-2-carboxaldehyde;1H-Pyrrole-2-carboxaldehyde, 4-iodo-
CBNumber
CB9341403
Molecular Formula
C5H4INO
Formula Weight
221
MOL File
33515-62-7.mol
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SALOR-INT L164526-1EA Property

Melting point:
117-118 °C(Solv: dichloromethane (75-09-2); hexane (110-54-3))
Boiling point:
319.3±27.0 °C(Predicted)
Density 
2.177±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
pka
13.70±0.50(Predicted)
Appearance
White to off-white Solid
InChI
InChI=1S/C5H4INO/c6-4-1-5(3-8)7-2-4/h1-3,7H
InChIKey
AEYJSULNKPFTAP-UHFFFAOYSA-N
SMILES
N1C=C(I)C=C1C=O
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC
Product number
I719493
Product name
4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging
100mg
Price
$60
Updated
2021/12/16
TRC
Product number
I719493
Product name
4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging
500mg
Price
$110
Updated
2021/12/16
Matrix Scientific
Product number
120051
Product name
4-Iodo-1H-pyrrole-2-carbaldehyde
Purity
95+%
Packaging
1g
Price
$270
Updated
2021/12/16
AK Scientific
Product number
Y8757
Product name
4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging
25g
Price
$328
Updated
2021/12/16
American Custom Chemicals Corporation
Product number
HCH0323156
Product name
4-IODO-1H-PYRROLE-2-CARBALDEHYDE
Purity
95.00%
Packaging
5MG
Price
$496.44
Updated
2021/12/16
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SALOR-INT L164526-1EA Chemical Properties,Usage,Production

Synthesis

1003-29-8

33515-62-7

General procedure for the synthesis of 4-iodo-1H-pyrrole-2-carbaldehyde from 2-pyrrolecarboxaldehyde: 1H-pyrrole-2-carbaldehyde (7.0 g, 73.6 mmol) was dissolved in tetrahydrofuran (45 mL) and the solution was cooled to -75 °C. N-iodosuccinimide (19.8 g, 88.3 mmol) was added in batches over 20 minutes, followed by continuous stirring of the reaction mixture at -75 °C for 2 hours. Upon completion of the reaction, water and petroleum ether were added and the mixture was slowly warmed to room temperature. The organic layer was separated and the aqueous phase was extracted with petroleum ether. All organic layers were combined, washed sequentially with water and brine, dried with anhydrous sodium sulfate, filtered and concentrated under vacuum to afford 4-iodo-1H-pyrrole-2-carbaldehyde (13.2 g, 81% yield) as a black solid.

References

[1] Patent: WO2009/130481, 2009, A1. Location in patent: Page/Page column 107
[2] Bioorganic and Medicinal Chemistry Letters, 2003, vol. 13, # 24, p. 4515 - 4518

SALOR-INT L164526-1EA Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from SALOR-INT L164526-1EA manufacturers

Shaanxi Dideu Medichem Co. Ltd
Product
SALOR-INT L164526-1EA 33515-62-7
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20T
Release date
2024-08-14
Career Henan Chemical Co
Product
4-IODO-1H-PYRROLE-2-CARBALDEHYDE 33515-62-7
Price
US $6.86/KG
Min. Order
1KG
Purity
95.0%-99.0%
Supply Ability
1kg-100kg
Release date
2020-03-10
Career Henan Chemical Co
Product
SALOR-INT L164526-1EA 33515-62-7
Price
US $6.68/KG
Min. Order
1KG
Purity
97%-99%
Supply Ability
1kg-1000kg
Release date
2020-01-10

33515-62-7, SALOR-INT L164526-1EARelated Search:


  • SALOR-INT L164526-1EA
  • 4-IODO-1H-PYRROLE-2-CARBALDEHYDE
  • 4-iodo-1H-Pyrrole-2-carboxaldehyde
  • 4-Iodopyrrole-2-carboxaldehyde
  • 4-Iodopyrrole-2-carbaldehyde
  • 1H-Pyrrole-2-carboxaldehyde, 4-iodo-
  • 33515-62-7
  • 433515-62-7