SALOR-INT L164526-1EA

Product Name: SALOR-INT L164526-1EA
CAS No.: 33515-62-7
Chemical Name: SALOR-INT L164526-1EA
Synonyms: SALOR-INT L164526-1EA;4-Iodopyrrole-2-carbaldehyde;4-Iodopyrrole-2-carboxaldehyde;4-IODO-1H-PYRROLE-2-CARBALDEHYDE;4-iodo-1H-Pyrrole-2-carboxaldehyde;1H-Pyrrole-2-carboxaldehyde, 4-iodo-
CBNumber: CB9341403
Molecular Formula: C5H4INO
Formula Weight: 221
MOL File: 33515-62-7.mol

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SALOR-INT L164526-1EA Property

Melting point:: 117-118 °C(Solv: dichloromethane (75-09-2); hexane (110-54-3))
Boiling point:: 319.3±27.0 °C(Predicted)
Density: 2.177±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2–8 °C
pka: 13.70±0.50(Predicted)
Appearance: White to off-white Solid
InChI: InChI=1S/C5H4INO/c6-4-1-5(3-8)7-2-4/h1-3,7H
InChIKey: AEYJSULNKPFTAP-UHFFFAOYSA-N
SMILES: N1C=C(I)C=C1C=O

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TRC

Product number: I719493
Product name: 4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging: 100mg
Price: $60
Updated: 2021/12/16

TRC

Product number: I719493
Product name: 4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging: 500mg
Price: $110
Updated: 2021/12/16

Matrix Scientific

Product number: 120051
Product name: 4-Iodo-1H-pyrrole-2-carbaldehyde
Purity: 95+%
Packaging: 1g
Price: $270
Updated: 2021/12/16

AK Scientific

Product number: Y8757
Product name: 4-Iodo-1H-pyrrole-2-carbaldehyde
Packaging: 25g
Price: $328
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0323156
Product name: 4-IODO-1H-PYRROLE-2-CARBALDEHYDE
Purity: 95.00%
Packaging: 5MG
Price: $496.44
Updated: 2021/12/16

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SALOR-INT L164526-1EA Chemical Properties,Usage,Production

Synthesis

1003-29-8

33515-62-7

General procedure for the synthesis of 4-iodo-1H-pyrrole-2-carbaldehyde from 2-pyrrolecarboxaldehyde: 1H-pyrrole-2-carbaldehyde (7.0 g, 73.6 mmol) was dissolved in tetrahydrofuran (45 mL) and the solution was cooled to -75 °C. N-iodosuccinimide (19.8 g, 88.3 mmol) was added in batches over 20 minutes, followed by continuous stirring of the reaction mixture at -75 °C for 2 hours. Upon completion of the reaction, water and petroleum ether were added and the mixture was slowly warmed to room temperature. The organic layer was separated and the aqueous phase was extracted with petroleum ether. All organic layers were combined, washed sequentially with water and brine, dried with anhydrous sodium sulfate, filtered and concentrated under vacuum to afford 4-iodo-1H-pyrrole-2-carbaldehyde (13.2 g, 81% yield) as a black solid.

References

[1] Patent: WO2009/130481, 2009, A1. Location in patent: Page/Page column 107
[2] Bioorganic and Medicinal Chemistry Letters, 2003, vol. 13, # 24, p. 4515 - 4518

SALOR-INT L164526-1EA Preparation Products And Raw materials

Raw materials

Preparation Products

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SALOR-INT L164526-1EA Suppliers

China 50 India 3 United States 7 Global 60

A.J Chemicals

Tel: --
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Email: sales@ajchem.in
Country: India
ProdList: 6100
Advantage: 58

CHEMSWORTH

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Email: info@chemsworth.com
Country: India
ProdList: 6700
Advantage: 30

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View Lastest Price from SALOR-INT L164526-1EA manufacturers

Shaanxi Dideu Medichem Co. Ltd

Product: SALOR-INT L164526-1EA 33515-62-7
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 20T
Release date: 2024-08-14

Career Henan Chemical Co

Product: 4-IODO-1H-PYRROLE-2-CARBALDEHYDE 33515-62-7
Price: US $6.86/KG
Min. Order: 1KG
Purity: 95.0%-99.0%
Supply Ability: 1kg-100kg
Release date: 2020-03-10

Career Henan Chemical Co

Product: SALOR-INT L164526-1EA 33515-62-7
Price: US $6.68/KG
Min. Order: 1KG
Purity: 97%-99%
Supply Ability: 1kg-1000kg
Release date: 2020-01-10

33515-62-7, SALOR-INT L164526-1EARelated Search:

4-IODO-2-(TRICHLOROACETYL)PYRROLE 4-IODOPYRROLE-2-CARBOXYLIC ACID METHYL ESTER SALOR-INT L164526-1EA 4-iodo-1H-pyrrole-2-carbohydrazide SPECS AQ-776/42801684 2-ACETYL-4-IODOPYRROLE 1-BENZYL-4-IODO-1H-PYRROLE-2-CARBALDEHYDE 4-iodo-1H-pyrrole-2-carboxylic acid

SALOR-INT L164526-1EA

4-IODO-1H-PYRROLE-2-CARBALDEHYDE

4-iodo-1H-Pyrrole-2-carboxaldehyde

4-Iodopyrrole-2-carboxaldehyde

4-Iodopyrrole-2-carbaldehyde

1H-Pyrrole-2-carboxaldehyde, 4-iodo-

33515-62-7

433515-62-7