ChemicalBook > CAS DataBase List > 4-NITROBENZO-15-CROWN-5

4-NITROBENZO-15-CROWN-5

Product Name
4-NITROBENZO-15-CROWN-5
CAS No.
60835-69-0
Chemical Name
4-NITROBENZO-15-CROWN-5
Synonyms
NITROBENZO-15-CROWN-5;4-NITROBENZO-15-CROWN-5;4'-NITROBENZO-15-CROWN-5;4'-Nitrobenzo-15-crown-5;Nitrobenzo-15-crown-5,99%;4-nitryl-benzo-15-crown-5;4-Nitrobenzo-15-crown-5,99%;4'-NITROBENZO-15-CROWN 5-ETHER;4'-Nitrobenzo-15-crown 5-Ether;4'-Nitrobenzo-15-crown5-Ether>
CBNumber
CB9439728
Molecular Formula
C14H19NO7
Formula Weight
313.3
MOL File
60835-69-0.mol
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4-NITROBENZO-15-CROWN-5 Property

Melting point:
93-97 °C(lit.)
Boiling point:
453.11°C (rough estimate)
Density 
1.191
refractive index 
1.5230 (estimate)
storage temp. 
Store below +30°C.
solubility 
It is soluble in non-polar solvents.
form 
powder to crystal
color 
Light orange to Yellow to Green
BRN 
1598970
CAS DataBase Reference
60835-69-0(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29329985
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P405Store locked up.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
341878
Product name
4′-Nitrobenzo-15-crown-5
Purity
99%
Packaging
1g
Price
$50.9
Updated
2023/01/07
TCI Chemical
Product number
N0561
Product name
4'-Nitrobenzo-15-crown 5-Ether
Purity
>99.0%(GC)
Packaging
1g
Price
$67
Updated
2024/03/01
TCI Chemical
Product number
N0561
Product name
4'-Nitrobenzo-15-crown 5-Ether
Purity
>99.0%(GC)
Packaging
5g
Price
$202
Updated
2024/03/01
Alfa Aesar
Product number
A16225
Product name
4-Nitrobenzo-15-crown-5, 99%
Packaging
5g
Price
$170
Updated
2024/03/01
Alfa Aesar
Product number
A16225
Product name
4-Nitrobenzo-15-crown-5, 99%
Packaging
1g
Price
$35.3
Updated
2021/12/16
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4-NITROBENZO-15-CROWN-5 Chemical Properties,Usage,Production

Chemical Properties

LIGHT YELLOW GRANULAR POWDER

Uses

4-Nitrobenzo-15-crown-5 is a raw material used in synthesis as well as an intemediate in chemical syntheis and pharmaceutica intemediate. It is also used to separate cations, dissolve inorganic salts into organic solvents to perform naked anion chemistry, serve as phase transfer catalysts, and chiral crown ethers have been used to resolve racemic mixtures or separate isomers by chiral chromatography.

Purification Methods

Recrystallise the crown ether from EtOH, MeOH or *C6H6/hexane as for the 18-crown-6 compound below. It complexes with Na+, K+, NH4+, Ca2+, Mg2+ and Cd2+. The 1HNMR spectrum (CDCl3) has (ppm): 3.6-4.4 (m 16CH2), 6.8 (d 1H arom), 7.65 (d 1H arom), 7.80 (dd 1H arom Jab 9Hz and Jbc 3Hz) [Schmid et al. J Am Chem Soc 98 5198 1976, Kikukawa et al. Bull Chem Soc Jpn 50 2207 1977, Toke et al. Justus Liebigs Ann Chem 349 349, 761 1988, Lindner et al. Z Anal Chem 322 157 1985].

4-NITROBENZO-15-CROWN-5 Preparation Products And Raw materials

Raw materials

Preparation Products

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4-NITROBENZO-15-CROWN-5 Suppliers

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60835-69-0, 4-NITROBENZO-15-CROWN-5Related Search:

3,4-Dimethoxynitrobenzene O,O'-BIS(2-HYDROXYETHOXY)BENZENE 3-NITROPHENETOLE 3,4-DIETHOXY NITROBENZENE 2-(2-HYDROXYETHOXY)PHENOL Benzo-15-crown-5 4-NITROPHENYL-2-METHOXYETHYL ETHER 3,4-Diethoxyaniline 4'-Aminobenzo-15-crown-5-ether 2-[2-[2-(2-phenoxyethoxy)ethoxy]ethoxy]ethanol 4-NITROBENZO-15-CROWN-5 15-Crown-5 2-DODECYL-2-METHYL-1,3-PROPANEDIYL BIS[N-[5'-NITRO(BENZO-15-CROWN-5)-4'-YL]CARBAMATE] CHEMBRDG-BB 4024087 4-(2-METHOXYETHOXY)ANILINE 4'-AMINO-5'-NITROBENZO-15-CROWN-5 4-(2-ETHOXYETHOXY)ANILINE 2-(3-aminophenoxy)-1-ethanol

  • 2,3,5,6,8,9,11,12-Octahydro-15-nitro-1,4,7,10,13-benzopentaoxacyclopentadecin
  • CROWN ETHER/4'-NITROBENZO-15-CROWN-5 FOR
  • Crown ether/4'-Nitrobenzo-15-crown-5 for synthesis
  • 15-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecine
  • 17-Nitro-2,3-benzo-1,4,7,10,13-pentaoxacyclopentadecen-2
  • NITROBENZO-15-CROWN-5
  • CROWN ETHER/4'-NITROBENZO-15-CROWN-5
  • 4'-NITROBENZO-15-CROWN-5
  • 4-NITROBENZO-15-CROWN-5
  • 4'-NITROBENZO-15-CROWN 5-ETHER
  • 2,3-(4-NITROBENZO)-1,4,7,10,13-PENTAOXACYCLOPENTADEC-2-ENE
  • CARBON DISULFIDE, REAGENTPLUS, >=99.9%, LOW BENZENE
  • 4-Nitrobenzo-15-crown-5,99%
  • 1,4,7,10,13-Benzopentaoxacyclopentadecin, 2,3,5,6,8,9,11,12-octahydro-15-nitro-
  • 1,13-(4-Nitro-1,2-phenylene)-1,4,7,10,13-pentaoxatridecane
  • 1,2-(1,4,7,10,13-Pentaoxatridecane-1,13-diyl)-4-nitrobenzene
  • 15-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin
  • 16-Nitro-2,3,5,6,8,9,11,12-octahydro-1,4,7,10,13-benzopentaoxacyclopentadecin
  • Nitrobenzo-15-crown-5,99%
  • 4-nitryl-benzo-15-crown-5
  • 17-nitro-2,5,8,11,14-pentaoxabicyclo[13.4.0]nonadeca-1(15),16,18-triene
  • 4'-Nitrobenzo-15-crown5-Ether&gt
  • 4- Nitrobenzene -15- crown ether -5
  • 4'-Nitrobenzo-15-crown 5-Ether
  • 4'-Nitrobenzo-15-crown-5
  • 60835-69-0
  • 33408-96-1
  • C14H19NO7
  • Chelation/Complexation Compounds
  • Synthetic Reagents
  • Crown Ethers
  • Macrocycles for Host-Guest Chemistry
  • Crown Ethers
  • Functional Materials
  • Macrocycles for Host-Guest Chemistry
  • Chelation/Complexation Compounds
  • Crown Ethers
  • Synthetic Reagents