ChemicalBook > CAS DataBase List > 4-METHOXY-3-NITROANILINE

4-METHOXY-3-NITROANILINE

Product Name
4-METHOXY-3-NITROANILINE
CAS No.
577-72-0
Chemical Name
4-METHOXY-3-NITROANILINE
Synonyms
3-NITRO-P-ANISIDINE;4-METHOXY-3-NITROANI;4-METHOXY-3-NITROANILINE;3-Nitro-p-anisidine (NH2=1);4-Methoxy-3-nitrobenzenamine;Benzenamine, 4-methoxy-3-nitro-;3-Nitro-4-methoxybenzene-1-amine;4-METHOXY-3-NITROANILINE ISO 9001：2015 REACH;4-Methoxy-3-nitroaniline@100 μg/mL in Methanol;4-Amino-2-nitroanisole, 5-Amino-2-methoxynitrobenzene
CBNumber
CB9462814
Molecular Formula
C7H8N2O3
Formula Weight
168.15
MOL File
577-72-0.mol
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4-METHOXY-3-NITROANILINE Property

Melting point:
46-47 °C
Boiling point:
356.9±22.0 °C(Predicted)
Density 
1.318±0.06 g/cm3(Predicted)
storage temp. 
under inert gas (nitrogen or Argon) at 2–8 °C
solubility 
Acetonitrile (Slightly), Chloroform (Slightly)
form 
Solid
pka
3.33±0.10(Predicted)
color 
Dark Red
InChI
InChI=1S/C7H8N2O3/c1-12-7-3-2-5(8)4-6(7)9(10)11/h2-4H,8H2,1H3
InChIKey
RUFOHZDEBFYQSV-UHFFFAOYSA-N
SMILES
C1(N)=CC=C(OC)C([N+]([O-])=O)=C1
CAS DataBase Reference
577-72-0(CAS DataBase Reference)
NIST Chemistry Reference
P-anisidine, 3-nitro-,(577-72-0)
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Safety

Hazard Codes 
Xi
Hazard Note 
Irritant
HS Code 
2922290090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H332Harmful if inhaled

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC
Product number
M327203
Product name
4-Methoxy-3-nitroaniline
Packaging
50mg
Price
$45
Updated
2021/12/16
ChemScene
Product number
CS-W002411
Product name
4-Methoxy-3-nitroaniline
Purity
99.71%
Packaging
5g
Price
$50
Updated
2021/12/16
ChemScene
Product number
CS-W002411
Product name
4-Methoxy-3-nitroaniline
Purity
99.71%
Packaging
10g
Price
$79
Updated
2021/12/16
Apolloscientific
Product number
OR0934
Product name
4-Methoxy-3-nitroaniline
Packaging
5g
Price
$105
Updated
2021/12/16
SynQuest Laboratories
Product number
4655-1-W8
Product name
4-Methoxy-3-nitroaniline
Packaging
5G
Price
$116
Updated
2021/12/16
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4-METHOXY-3-NITROANILINE Chemical Properties,Usage,Production

Chemical Properties

orange red solid

Uses

4-Methoxy-3-nitroaniline is a chemical compound that has been shown to have anti-tumor and anti-inflammatory effects. It belongs to the class of amines and can be synthesized by nitrating 4-methoxy aniline.

Synthesis

119-34-6

74-88-4

577-72-0

2-Nitro-4-aminophenol (10.0 g, 64.9 mmol) was used as starting material and mixed with cesium carbonate (21 g, 64 mmol) and iodomethane (9.22 g, 64.9 mmol) in acetonitrile (1500 mL). The reaction mixture was heated to reflux for 5 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble solids. The filtrate was concentrated under reduced pressure to remove the solvent, and the resulting crude product was purified by fast column chromatography (eluent: chloroform) to give 5.03 g of 4-methoxy-3-nitroaniline in 46% yield as a red oil. The structure of the product was confirmed by 1H NMR (DMSO-d6) δ 7.09-7.03 (m, 2H), 6.87 (d, J=3Hz, 1H), 5.21 (bs, 2H), 3.77 (s, 3H) and HRMS (EI) m/z 168.0497 (M+1). Elemental analysis results (C7H8N2O3): calculated values C 50.00, H 4.80, N 16.66; measured values C 50.20, H 5.07, N 16.60.

References

[1] Patent: US2002/26052, 2002, A1

4-METHOXY-3-NITROANILINE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-METHOXY-3-NITROANILINE Suppliers

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View Lastest Price from 4-METHOXY-3-NITROANILINE manufacturers

Career Henan Chemical Co
Product
4-METHOXY-3-NITROANILINE 577-72-0
Price
US $1.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
1ton
Release date
2018-08-09

577-72-0, 4-METHOXY-3-NITROANILINERelated Search:

BINAPACRYL DINOSEB ACETATE N-(4-METHOXY-3-NITROPHENYL)ACETAMIDE DINOCAP MEDINOTERB ACETATE DINOBUTON 2,4-DINITROPHENETOLE 1-Methoxy-2,4-dinitrobenzene O-MONO-2,4-DNP-L-TYROSINE 4-tert-Butyl-2,6-dinitro-3-methoxytoluene 2,4-Dinitro-1-(trifluoromethoxy)benzene 2-nitro-p-anisidine 4-methoxy-2-nitroaniline,4-METHOXY-2-NITROANILINE N-ACETYL-4-METHOXY-2-NITROANILINE 2-METHOXY-5-NITROANILINE HCL,2-Methoxy-5-nitroaniline hydrochloride 3-Methoxy-2-nitroaniline 2-METHOXY-6-NITROANILINE 2,5-Dimethoxy-4-nitroaniline 2-METHOXY-5-NITROANILINE

  • Benzenamine, 4-methoxy-3-nitro-
  • 3-NITRO-P-ANISIDINE
  • 4-METHOXY-3-NITROANILINE
  • 3-Nitro-p-anisidine (NH2=1)
  • 3-Nitro-4-methoxybenzene-1-amine
  • 4-METHOXY-3-NITROANI
  • 4-Amino-2-nitroanisole, 5-Amino-2-methoxynitrobenzene
  • 4-Methoxy-3-nitroaniline@100 μg/mL in Methanol
  • 4-METHOXY-3-NITROANILINE ISO 9001：2015 REACH
  • 4-Methoxy-3-nitrobenzenamine
  • 577-72-0
  • API intermediates
  • Anilines, Aromatic Amines and Nitro Compounds