ChemicalBook > CAS DataBase List > (3-(BROMOMETHYL)PHENYL)METHANOL

(3-(BROMOMETHYL)PHENYL)METHANOL

Uses

Product Name: (3-(BROMOMETHYL)PHENYL)METHANOL
CAS No.: 82072-22-8
Chemical Name: (3-(BROMOMETHYL)PHENYL)METHANOL
Synonyms: 3-BROMO METHYLBENZYL ALCOHOL;3-(Bromomethyl)benzenemethanol;(3-(BROMOMETHYL)PHENYL)METHANOL
CBNumber: CB9708648
Molecular Formula: C8H9BrO
Formula Weight: 201.06
MOL File: 82072-22-8.mol

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(3-(BROMOMETHYL)PHENYL)METHANOL Property

Boiling point:: 286.0±20.0 °C(Predicted)
Density: 1.514±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
pka: 14.23±0.10(Predicted)
Appearance: Light yellow to yellow Powder

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H314Causes severe skin burns and eye damage

H317May cause an allergic skin reaction

H400Very toxic to aquatic life

Precautionary statements

P260Do not breathe dust/fume/gas/mist/vapours/spray.

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P270Do not eat, drink or smoke when using this product.

P272Contaminated work clothing should not be allowed out of the workplace.

P273Avoid release to the environment.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P333+P313IF SKIN irritation or rash occurs: Get medical advice/attention.

P363Wash contaminated clothing before reuse.

P391Collect spillage. Hazardous to the aquatic environment

P405Store locked up.

P501Dispose of contents/container to..…

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N-Bromosuccinimide Price

TRC

Product number: B697108
Product name: 3-Bromomethylbenzylalcohol
Packaging: 1g
Price: $295
Updated: 2021/12/16

AK Scientific

Product number: W8601
Product name: (3-(Bromomethyl)phenyl)methanol
Packaging: 5g
Price: $531
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0030270
Product name: (3-(BROMOMETHYL)PHENYL)METHANOL
Purity: 95.00%
Packaging: 5G
Price: $1584.66
Updated: 2021/12/16

Medical Isotopes, Inc.

Product number: 38284
Product name: 3-(Bromomethyl)benzylalcohol
Purity: 95+%
Packaging: 5G
Price: $680
Updated: 2021/12/16

Matrix Scientific

Product number: 076545
Product name: 3-Bromomethylbenzyl alcohol
Purity: 95+%
Packaging: 5g
Price: $759
Updated: 2021/12/16

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(3-(BROMOMETHYL)PHENYL)METHANOL Chemical Properties,Usage,Production

Uses

3-Bromomethylbenzyl alcohol can be used as a pharmaceutical synthesis intermediate.

Synthesis

1129-28-8

82072-22-8

Step A: To a stirred solution of methyl 3-bromomethylbenzoate (5 g, 21.8 mmol) in toluene (50 mL) was slowly added DABAL-H (43.6 mL, 43.6 mmol) under ice bath conditions. The reaction temperature was maintained at 0 °C with continuous stirring for 2 hours. Upon completion of the reaction, the reaction was quenched with 1N HCl solution and subsequently separated by extraction with ethyl acetate (EtOAc) and water. The organic layer was collected, dried with anhydrous sodium sulfate (Na2SO4) and concentrated under reduced pressure to give 3-bromomethylbenzyl alcohol (4.0 g, 19.9 mmol, 91% yield) as a colorless oil.

References

[1] Organometallics, 2015, vol. 34, # 9, p. 1627 - 1634
[2] Patent: WO2015/142903, 2015, A2. Location in patent: Page/Page column 94
[3] Patent: WO2015/140133, 2015, A1. Location in patent: Page/Page column 106
[4] Patent: WO2017/68064, 2017, A1. Location in patent: Page/Page column 191; 192
[5] Patent: EP2816023, 2014, A1. Location in patent: Paragraph 0488

(3-(BROMOMETHYL)PHENYL)METHANOL Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from (3-(BROMOMETHYL)PHENYL)METHANOL manufacturers

Shanghai Rlavie Technology Co ltd

Product: 3-Bromomethylbenzyl alcohol 82072-22-8
Price: US $0.00/KG
Min. Order: 0.0001KG
Purity: 98%min
Supply Ability: 500kgs/month
Release date: 2022-05-11

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3-BROMO METHYLBENZYL ALCOHOL

(3-(BROMOMETHYL)PHENYL)METHANOL

3-(Bromomethyl)benzenemethanol

82072-22-8