Dimethyl nitroterephthalate

Product Name: Dimethyl nitroterephthalate
CAS No.: 5292-45-5
Chemical Name: Dimethyl nitroterephthalate
Synonyms: 2-Nitro;RARECHEM AL BF 0920;Dimethyl nitroterephthalate;DIMETHYL2-NITROTEREPHTALATE;Dithyl 2-Nitroterephthalate;Dimethyl-2-nitroterephthalat;DIMETHYL 2-NITROTEREPHTHALATE;DimethylNitroterephthalate>2-Nitro dimethyl terphthalate;2-NITRO DIMETHYL TEREPHTHALATE
CBNumber: CB9728811
Molecular Formula: C10H9NO6
Formula Weight: 239.18
MOL File: 5292-45-5.mol

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Dimethyl nitroterephthalate Property

Melting point:: 73-76 °C(lit.)
Boiling point:: 381.83°C (rough estimate)
Density: 1.272
vapor pressure: 0.014Pa at 20℃
refractive index: 1.5310 (estimate)
storage temp.: Sealed in dry,Room Temperature
form: Powder
color: White to Almost white
Water Solubility: INSOLUBLE
BRN: 1993064
LogP: 1.78 at 23℃ and pH3.6
CAS DataBase Reference: 5292-45-5(CAS DataBase Reference)
EPA Substance Registry System: 1,4-Benzenedicarboxylic acid, 2-nitro-, dimethyl ester (5292-45-5)

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Safety

Hazard Codes: Xi
Risk Statements: 36/37/38
Safety Statements: 37/39-26-24/25
WGK Germany: 2
TSCA: Yes
HS Code: 29173990

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H411Toxic to aquatic life with long lasting effects

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: N0501
Product name: Dimethyl Nitroterephthalate
Purity: >97.0%(GC)
Packaging: 25g
Price: $23
Updated: 2025/07/31

TCI Chemical

Product number: N0501
Product name: Dimethyl Nitroterephthalate
Purity: >97.0%(GC)
Packaging: 250g
Price: $124
Updated: 2025/07/31

TRC

Product number: D480418
Product name: Dimethyl Nitroterephthalate
Packaging: 1g
Price: $55
Updated: 2021/12/16

TRC

Product number: D480418
Product name: Dimethyl Nitroterephthalate
Packaging: 2.5g
Price: $65
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FD33944
Product name: Dimethyl 2-nitroterephthalate
Packaging: 250g
Price: $80
Updated: 2021/12/16

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Dimethyl nitroterephthalate Chemical Properties,Usage,Production

Chemical Properties

white powder

Synthesis

120-61-6

5292-45-5

In a 1000 ml four-necked flask, 926.97 g of 98% concentrated sulfuric acid was added with stirring and the temperature was maintained at 10 to 15°C. 200.72 g of 97.7% nitric acid was added slowly and dropwise. After the nitric acid was added, 300.0 g of dimethyl terephthalate was added and the reaction temperature was maintained at 10 to 15°C for about 30 minutes. Subsequently, the reaction temperature was controlled at 15 to 20°C and the reaction was continued for 30 minutes before the endpoint of the reaction was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was stirred for 15 minutes, filtered, and the filter cake was sequentially washed to neutrality with 900 mL of 5% aqueous sodium hydroxide and 500 mL of water. The filter cake was suspended in 3000 ml of water and stirred for 30 min at room temperature. Next, the mixture is transferred to a recrystallization unit and 1500 g of ethanol is added for recrystallization: the solid is first heated to 50 to 55°C to dissolve completely, then slowly cooled to below 5°C to promote full precipitation of the product. The precipitate was collected by filtration and dried to give 382.5 g of crude product. Further vacuum drying at 60°C gave 351.2 g of the white crystalline product, dimethyl 2-nitroterephthalate, in 95% yield (as dimethyl terephthalate). The product was analyzed by gas chromatography and showed a purity of greater than 99% with a melting point of 73.8 to 75.5°C (literature value: 73 to 76°C).

References

[1] Journal of Organic Chemistry, 2001, vol. 66, # 12, p. 4356 - 4360
[2] Patent: CN103524386, 2016, B. Location in patent: Paragraph 0029; 0030; 0031
[3] Patent: CN104072403, 2016, B. Location in patent: Paragraph 0031-0033
[4] Liebigs Annalen der Chemie, 1987, p. 833 - 838
[5] Justus Liebigs Annalen der Chemie, 1912, vol. 393, p. 25

Dimethyl nitroterephthalate Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from Dimethyl nitroterephthalate manufacturers

Asia Chem I and E (Jiangsu) Co Ltd

Product: Dimethyl nitroterephthalate 5292-45-5
Price: US $41.86/Kg/Drum
Min. Order: 25Kg/Drum
Purity: 99.00%HPLC
Supply Ability: 15tons/month
Release date: 2021-09-24

Career Henan Chemical Co

Product: Dimethyl nitroterephthalate 5292-45-5
Price: US $1.00/g
Min. Order: 1g
Purity: 99%
Supply Ability: 10000KGS
Release date: 2020-01-09

5292-45-5, Dimethyl nitroterephthalateRelated Search:

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2-Nitro

2-nitrobenzene-1,4-dicarboxylic acid dimethyl ester

DIMETHYL2-NITROTEREPHTALATE

Dimethyl-2-nitroterephthalat

Dimethyl nitroterephthalate, 98+%

1,4-Benzenedicarboxylic acid, 2-nitro-, dimethyl ester

Dimethyl nitroterephthalate,99%

Dimethyl nitroterephthalate

DIMETHYL 2-NITRO-1,4-BENZENEDICARBOXYLATE

Terephthalic acid, nitro-, dimethyl ester

RARECHEM AL BF 0920

NITROTEREPHTHALIC ACID DIMETHYL ESTER

4-benzenedicarboxylicacid,2-nitro-dimethylester

Dimethyl 2-nitrobenzene-1,4-dicarboxylate

DIMETHYL 2-NITROTEREPHTHALATE

2-Nitrobenzene-1,4-dicarboxylic acid dimethyl ester~Nitroterephthalic acid dimethyl ester

Dimethyl 2-nitroterephthalate, 98+%

Nitroterephthalatedimethylester

Dithyl 2-Nitroterephthalate

DimethylNitroterephthalate&gt

1,4-Benzenedicarboxylic acid, 2-nitro-, 1,4-dimethyl ester

2-NITRO DIMETHYL TEREPHTHALATE

2 – Nitro Dimethyl terephthalate/ NDMT

2-nitro-1,4-benzenedicarboxylic acid dimethyl ester

2-NITRO TEREPHTHALIC ACID DIMETHYL ESTER

2-Nitro dimethyl terphthalate

5292-45-5

5952-45-5

5292-45-4

O2NC6H314CO2CH32

Esters

Organic Building Blocks

Building Blocks

C10 to C11

Carbonyl Compounds

Derivatives of phthalic acid