METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE

Product Name: METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE
CAS No.: 865887-07-6
Chemical Name: METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE
Synonyms: METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE;Methyl-4-benzyloxy-1H-indazole-3-carboxylate;1H-Indazole-3-carboxylic acid, 4-Methoxy-, Methyl ester
CBNumber: CB9770133
Molecular Formula: C10H10N2O3
Formula Weight: 206.2
MOL File: 865887-07-6.mol

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METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE Property

storage temp.: 2-8°C
Appearance: Off-white to yellow Solid

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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC

Product number: M779708
Product name: Methyl4-methoxy-1H-indazole-3-carboxylate
Packaging: 10mg
Price: $45
Updated: 2021/12/16

TRC

Product number: M779708
Product name: Methyl4-methoxy-1H-indazole-3-carboxylate
Packaging: 50mg
Price: $65
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: CHM0376683
Product name: METHYL-4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE
Purity: 95.00%
Packaging: 5MG
Price: $504.83
Updated: 2021/12/16

AK Scientific

Product number: 3580AC
Product name: Methyl4-methoxy-1H-indazole-3-carboxylate
Packaging: 5g
Price: $1854
Updated: 2021/12/16

Alichem

Product number: 865887076
Product name: Methyl4-methoxy-1H-indazole-3-carboxylate
Packaging: 5g
Price: $1431
Updated: 2021/12/16

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METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE Chemical Properties,Usage,Production

Synthesis

67-56-1

865887-02-1

865887-07-6

Acetyl chloride (18 mL) was slowly added dropwise to methanol (180 mL) at 0 °C and the reaction mixture was kept stirred at this temperature for 1 hour. Subsequently, 4-methoxy-1H-indazole-3-carboxylic acid (21.8 mmol) was added and the reaction mixture was heated to reflux for 3 hours. After completion of the reaction, the solution was concentrated to dryness under reduced pressure. The resulting residue was suspended in water and the pH was adjusted with saturated sodium bicarbonate solution to 7. Next, extraction was carried out with ethyl acetate (3 x 100 mL), the organic layers were combined, dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure. Finally, the crude product was purified by column chromatography (eluent ratio of 2:1 petroleum ether/ethyl acetate) to afford methyl 4-methoxy-1H-indazole-3-carboxylate in 5% yield (two-step reaction) and the product was a yellow solid.

References

[1] Patent: US2007/78147, 2007, A1. Location in patent: Page/Page column 67

METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE Preparation Products And Raw materials

Raw materials

Preparation Products

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METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE Suppliers

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865887-07-6, METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATERelated Search:

ETHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE 4-HYDROXYINDAZOLE 4-HYDROXY-1H-INDAZOLE-3-CARBOXYLIC ACID 4-METHOXY (1H)INDAZOLE 4-Hydroxy-3-methyl-1H-indazole METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE METHYL 4-BENZYLOXY-3-INDAZOLECARBOXYLATE 4-Methoxyindazole-3-carboxylic acid

METHYL 4-METHOXY-1H-INDAZOLE-3-CARBOXYLATE

Methyl-4-benzyloxy-1H-indazole-3-carboxylate

1H-Indazole-3-carboxylic acid, 4-Methoxy-, Methyl ester

865887-07-6