SodiuM new houttuyfonate
- Product Name
- SodiuM new houttuyfonate
- CAS No.
- 83766-73-8
- Chemical Name
- SodiuM new houttuyfonate
- Synonyms
- Houttuynin Sodium;HOUTTUYFONATE SODIUM;SODIUM HOUTTUYFONATE;Enzastaurin Impurity 3;Sodium neohouttuyfonate;SODIUM NEW HOUTTUYFONATE;Houttuynin sodium bisulfite;Sodium Houttuyfonate (Houttuynin);Sodium Houttuyfonate, 10 mM in DMSO;sodium 1-hydroxy-3-oxododecane-1-sulfonate
- CBNumber
- CB9806678
- Molecular Formula
- C12H25NaO5S
- Formula Weight
- 304.38
- MOL File
- 83766-73-8.mol
SodiuM new houttuyfonate Property
- Melting point:
- 159 - 162°C
- storage temp.
- -20°C Freezer, Under inert atmosphere
- solubility
- DMSO (Sparingly, Heated), Methanol (Slightly, Heated)
- form
- Solid
- color
- White to Off-White
- InChI
- InChI=1S/C12H24O5S.Na.H/c1-2-3-4-5-6-7-8-9-11(13)10-12(14)18(15,16)17;;/h12,14H,2-10H2,1H3,(H,15,16,17);;
- InChIKey
- XTAHMVHCMAPGRY-UHFFFAOYSA-N
- SMILES
- C(=O)(CCCCCCCCC)CC(O)S(O)(=O)=O.[NaH]
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P280Wear protective gloves/protective clothing/eye protection/face protection.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- 300989
- Product name
- Sodium Houttuyfonate
- Packaging
- 20mg
- Price
- $276
- Updated
- 2021/12/16
- Product number
- S634340
- Product name
- SodiumHouttuyfonate
- Packaging
- 25mg
- Price
- $360
- Updated
- 2021/12/16
- Product number
- S634340
- Product name
- SodiumHouttuyfonate
- Packaging
- 50mg
- Price
- $635
- Updated
- 2021/12/16
- Product number
- orb259505
- Product name
- Sodium Houttuyfonate
- Purity
- 98%
- Packaging
- 20mg
- Price
- $238
- Updated
- 2021/12/16
- Product number
- orb259505
- Product name
- Sodium Houttuyfonate
- Purity
- 98%
- Packaging
- 100mg
- Price
- $314.5
- Updated
- 2021/12/16
SodiuM new houttuyfonate Chemical Properties,Usage,Production
Uses
Sodium Houttuyfonate is an inhibitor of inflammatory responses. It also has antibacterial activity. It is also a surfactant.
Synthesis
(1) Preparation of 2-tridecanone:
First, 2.3g of sodium metal was added to the reaction flask, and then 3mL of anhydrous ethanol was added, heated to 2530, and then 13.0g of ethyl acetoacetate, 10mL ethanol and 12.5mL of anhydrous ethyl ether were added dropwise to the solution, and stirred and refluxed for 1 hour; and then 21.85g of Lauryl chloride and 30 mL of ether were added to the reaction flask, and stirred and refluxed for 2-3 hours; after cooling, it was dissolved with dilute sulfuric acid, and the ether layer was separated, and the aqueous layer was extracted twice with ether, and the organic layers were combined and washed with distilled water, and the ether was recovered to obtain 15.7 g of intermediate 2-tridecanone in 92% yield.
(2) dodecanoyl acetaldehyde preparation:
With anhydrous ethanol as solvent, add 1.1g of sodium metal in the reaction vessel, heat and reflux for 1 hour, dropwise addition of 8g of 2-tridecanone, 3g of ethyl formate, stir the reaction for 4-6 hours, leave overnight, then washed with distilled water, and then extracted with ether for several times, the combined ether solution, dried with anhydrous sodium sulfate and filtered. After drying with anhydrous sodium sulfate and filtering, the ether was finally separated to obtain 8.3g of dodecanoyl acetaldehyde in 90.3% yield.
(3) a-hydroxy dodecanoyl ethyl sulfonate sodium preparation:
To the reaction vessel to add 60 ml of saturated sodium bisulfite saturated solution, and then slowly add 6.9 g of dodecanoyl acetaldehyde, 85 ~ 90 C. Reaction for 1.5 hours, cool down, filtration, washing, drying, a-hydroxy dodecanoyl ethyl sulfonate sodium 8.1g. Sodium a-hydroxydodecanoyl ethyl sulfonate 8.1g yield 89.3%, the content was 99.4% by HPLC.SodiuM new houttuyfonate Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from SodiuM new houttuyfonate manufacturers
- Product
- SodiuM new houttuyfonate 83766-73-8
- Price
- US $587.00/Kg/Bag
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 1000KG
- Release date
- 2021-06-04
- Product
- SodiuM new houttuyfonate 83766-73-8
- Price
- US $10.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- 10 mt
- Release date
- 2025-03-11
- Product
- Sodium new houttuyfonate 83766-73-8
- Price
- US $0.00-0.00/Kg
- Min. Order
- 1Kg
- Purity
- 99.9%
- Supply Ability
- 200tons
- Release date
- 2024-04-09