6-Bromonaphthalen-2-amine

Product Name: 6-Bromonaphthalen-2-amine
CAS No.: 7499-66-3
Chemical Name: 6-Bromonaphthalen-2-amine
Synonyms: F0701-0046;NSC 407685;2-Amino-6-bromophthalene;6-Bromonaphthalen-2-amine;6-BroMo-2-naphthalenaMine;2-Amino-6-bromonaphthalene;6-broMo-2-aMinonaphthalene;6-Bromonaphthalene-2-amine;2-Naphthalenamine, 6-bromo-;6-Bromonaphthalen-2-ylamine
CBNumber: CB9958050
Molecular Formula: C10H8BrN
Formula Weight: 222.08
MOL File: 7499-66-3.mol

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6-Bromonaphthalen-2-amine Property

Melting point:: 128 °C
Boiling point:: 155-160 °C(Press: 1 Torr)
Density: 1.563±0.06 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
solubility: DMSO (Slightly), Methanol (Slightly)
form: solid
pka: 3.66±0.10(Predicted)
color: grey
InChI: InChI=1S/C10H8BrN/c11-9-3-1-8-6-10(12)4-2-7(8)5-9/h1-6H,12H2
InChIKey: UBLKHAWYJFEPDX-UHFFFAOYSA-N
SMILES: C1=C2C(C=C(Br)C=C2)=CC=C1N

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Safety

Hazard Note: Irritant
HS Code: 2921450090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B685940
Product name: 6-Bromo-2-naphthylamine
Packaging: 1g
Price: $85
Updated: 2021/12/16

Oakwood

Product number: 047803
Product name: 2-Amino-6-bromonaphthalene
Packaging: 1g
Price: $19
Updated: 2021/12/16

Matrix Scientific

Product number: 068816
Product name: 6-Bromonaphthalen-2-amine
Purity: >95%
Packaging: 1g
Price: $20
Updated: 2021/12/16

ChemScene

Product number: CS-W001636
Product name: 6-Bromonaphthalen-2-amine
Purity: 96.48%
Packaging: 5g
Price: $29
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB13106
Product name: 6-Bromo-naphthalen-2-ylamine
Packaging: 2g
Price: $40
Updated: 2021/12/16

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6-Bromonaphthalen-2-amine Chemical Properties,Usage,Production

Uses

6-Bromonaphthalen-2-amine is used in the new synthesis of alkylsulphanylnaphthalenes and the synthesis and mesomorphic properties of novel naphthylisothiocyanates.

Application

6-Bromonaphthalen-2-amine can be used to prepare light-emitting diode materials, amine compounds, deuterated aromatic compounds and deuterated compositions thereof.

Synthesis

6-Bromo-2-naphthoic acid (5.07g, 20.19mmol) and triethylamine (4.22mL, 3.07g, 30.3mmol) in dry DMF (155mL) were treated with the diphenylphosphoroyl azide (6.55mL, 8.34g, 30.3mmol) followed by stirring at room temperature for 3h. The solution was then treated with water (2OmL) and warming at 1000C for Ih. The solution was cooled in the flask fitted with a short-path distillation head, and the DMF was removed by distillation under a high vacuum. The solid residue was dissolved in EtOAc and washed with a saturated sodium bicarbonate solution. Filtered through celite, the filtrate was washed with water (3x) and brine. Dried over, filtered, and concentrated under vacuum to give 6-Bromonaphthalen-2-amine as a beige solid (4.48g, 100 percent).

References

[1] Patent: WO2009/39127, 2009, A1. Location in patent: Page/Page column 175
[2] Patent: WO2009/39134, 2009, A1. Location in patent: Page/Page column 104
[3] Patent: WO2010/111437, 2010, A1. Location in patent: Page/Page column 74
[4] Bioorganic and Medicinal Chemistry Letters, 2016, vol. 26, # 15, p. 3793 - 3799
[5] Bioorganic and Medicinal Chemistry Letters, 2002, vol. 12, # 12, p. 1651 - 1655

6-Bromonaphthalen-2-amine Preparation Products And Raw materials

Raw materials

Ammonium hydroxide Sodium sulfite 6-Bromo-2-naphthol

Preparation Products

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6-Bromonaphthalen-2-amine Suppliers

Canada 2 China 208 India 2 United Kingdom 2 United States 10 Global 224

Toronto Research Chemicals

Tel: --
Fax: --
Email: info@trc-canada.com
Country: Canada
ProdList: 6038
Advantage: 71

LIFE CHEMICALS, formerly I.F. Lab

Tel: --
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Email: vasily.pinchuk@lifechemicals.com
Country: Canada
ProdList: 6706
Advantage: 69

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View Lastest Price from 6-Bromonaphthalen-2-amine manufacturers

HANGZHOU HAILAN CHEMICAL CO.,LTD.

Product: 6-Bromonaphthalen-2-amine 7499-66-3
Price: US $0.00/kg
Min. Order: 1kg
Purity: 99%min
Supply Ability: 20tons
Release date: 2025-08-21

Taizhou Creating Bio-pharm co., ltd.

Product: 6-bromonaphthalen-2-amine 7499-66-3
Price: US $0.00/KG
Min. Order: 1KG
Purity: 0.99
Supply Ability: 1TONS
Release date: 2025-06-06

Shaanxi Xianhe Biotech Co., Ltd

Product: 6-bromonaphthalen-2-amine 7499-66-3
Price: US $0.00/KG
Min. Order: 1KG
Purity: 0.99
Supply Ability: 1000KG
Release date: 2025-04-22

7499-66-3, 6-Bromonaphthalen-2-amineRelated Search:

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6-BroMo-2-naphthalenaMine

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6-Bromonaphthalen-2-ylamine

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6-Bromonaphthalen-2-amine

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6-Bromonaphthalene-2-amine

7499-66-3

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7499-66-3