3-Bromopropylacetate

Product Name: 3-Bromopropylacetate
CAS No.: 592-33-6
Chemical Name: 3-Bromopropylacetate
Synonyms: 1-Propanol, 3-bromo-, 1-acetate
CBNumber: CB9971628
Molecular Formula: C5H9BrO2
Formula Weight: 181.03
MOL File: 592-33-6.mol

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3-Bromopropylacetate Property

Boiling point:: 163°C(lit.)
Density: 1.417±0.06 g/cm3(Predicted)
refractive index: 1.4560 to 1.4600
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: clear liquid
color: Colorless to Light yellow to Light orange

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Safety

HS Code: 2915.39.9000

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TCI Chemical

Product number: B5650
Product name: 3-Bromopropyl Acetate
Purity: >98.0%(GC)
Packaging: 1g
Price: $59
Updated: 2025/07/31

TCI Chemical

Product number: B5650
Product name: 3-Bromopropyl Acetate
Purity: >98.0%(GC)
Packaging: 5g
Price: $204
Updated: 2025/07/31

American Custom Chemicals Corporation

Product number: HCH0257689
Product name: 3-BROMOPROPYL ACETATE
Purity: 95.00%
Packaging: 5MG
Price: $499.76
Updated: 2021/12/16

Crysdot

Product number: CD10000012
Product name: 3-Bromopropyl Acetate
Purity: 95%
Packaging: 10g
Price: $692
Updated: 2021/12/16

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3-Bromopropylacetate Chemical Properties,Usage,Production

Synthesis

108-24-7

627-18-9

592-33-6

General procedure for the synthesis of propyl 3-bromoacetate from ethanoic anhydride and 3-bromo-1-propanol: To a stirred solution of 3-bromo-1-propanol (8.0 g, 57.55 mmol) in anhydrous dichloromethane (40 mL) was added triethylamine (12 mL, 86.32 mmol) and stirred for 1 h at room temperature. Ethanoic anhydride (6.5 mL, 69.06 mmol) dissolved in dichloromethane (5 mL) was added dropwise at 0 °C, followed by stirring for 16 h at room temperature. The reaction process was monitored by thin layer chromatography (TLC). Upon completion of the reaction, the reaction mixture was quenched with 1N hydrochloric acid solution and extracted with dichloromethane. The combined organic layers were washed with brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The residue was purified by column chromatography with 10% ethyl acetate/hexane as eluent to give the target product propyl 3-bromoacetate. Yield: 10.0 g, 96% yield; 1H NMR (400 MHz, CDCl3) δ 4.19-4.17 (m, 2H), 3.47 (t, J=6.5 Hz, 2H), 2.21-2.18 (m, 2H), 2.06 (s, 3H).

References

[1] Patent: WO2017/6283, 2017, A1. Location in patent: Paragraph 0474; 0475
[2] Patent: WO2018/98206, 2018, A1. Location in patent: Paragraph 0940
[3] Patent: WO2008/39999, 2008, A1. Location in patent: Page/Page column 49
[4] Patent: TW2017/8220, 2017, A. Location in patent: Page/Page column 73; 74
[5] Chemistry - A European Journal, 2003, vol. 9, # 14, p. 3353 - 3366

3-Bromopropylacetate Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Bromopropylacetate Suppliers

Americas 1 China 25 Europe 1 India 2 Japan 1 Slovakia 1 United States 3 Global 34

Nanjing Chemlin Chemical Co., Ltd

Tel: 025-83697070
Fax: +86-25-83453306
Email: info@chemlin.com.cn
Country: China
ProdList: 15883
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TOKYO CHEMICAL INDUSTRY CO., LTD.

Tel: 03-36680489
Fax: 03-3668-0520
Email: Sales-JP@TCIchemicals.com
Country: Japan
ProdList: 28387
Advantage: 80

TCI Europe

Tel: 320-37350700
Fax: +32 (0)37350701
Email: sales@tcieurope.eu
Country: Europe
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TCI AMERICA

Tel: 800-4238616
Fax: +1-888-520-1075 / +1-503-283-1987
Email: sales@tciamerica.com
Country: Americas
ProdList: 23653
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Bide Pharmatech Ltd.

Tel: 400-164-7117 13681763483
Fax: +86-21-61629029
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Country: China
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Mashilabs (Shanghai) Co.,Ltd.

Tel: 19916721580
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Country: China
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Taizhou GreenChem Pharmaceutical Co., Ltd.

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Shanghai YuanYe Biotechnology Co., Ltd.

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Zhengzhou Huiju Chemical Co., Ltd.

Tel: 0371-55900031 18137872243
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Country: China
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Aikon International Limited

Tel: 025-58859352 18068836627
Fax: 02557626880
Email: sales01@aikonchem.com
Country: China
ProdList: 16027
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592-33-6, 3-BromopropylacetateRelated Search:

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1-Propanol, 3-bromo-, 1-acetate

592-33-6