MORPHOLINIUM CHLORIDE Chemical Properties

Melting point:

204℃

storage temp. 

Store below +30°C.

Water Solubility 

Soluble in water

form 

powder to crystal

color 

White to Light yellow

InChI

InChI=1S/C4H9NO.ClH/c1-3-6-4-2-5-1;/h5H,1-4H2;1H

InChIKey

JXYZHMPRERWTPM-UHFFFAOYSA-N

SMILES

C1NCCOC1.Cl

CAS DataBase Reference

10024-89-2

Safety Information

Toxicity

mouse,LD50,intraperitoneal,1350mg/kg (1350mg/kg),BEHAVIORAL: ANTIPSYCHOTICLUNGS, THORAX, OR RESPIRATION: RESPIRATORY DEPRESSION,Japanese Journal of Pharmacology. Vol. 17, Pg. 475, 1967.

MORPHOLINIUM CHLORIDE Usage And Synthesis

Chemical Properties

White Crysstalline

Synthesis

GENERAL PROCEDURE: Ammonium chloride (0.54 g, 10 mmol) and ethanol (3 mL) were added to a 25 mL round bottom flask, followed by morpholine (10 mmol). The reaction mixture was placed on a magnetic stirrer and heated to reflux for 2 hours. After completion of the reaction, the solvent was removed by rotary evaporator to give morpholine hydrochloride as a white solid in quantitative yield.

References

[1] Synthetic Communications, 2015, vol. 45, # 22, p. 2601 - 2607
[2] Main Group Metal Chemistry, 2016, vol. 39, # 5-6, p. 175 - 181
[3] Patent: WO2008/95943, 2008, A1. Location in patent: Page/Page column 50; 122-123
[4] Advanced Synthesis and Catalysis, 2010, vol. 352, # 7, p. 1135 - 1136
[5] Patent: US2010/204235, 2010, A1. Location in patent: Page/Page column 5; 27; 28

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