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(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE

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(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE Basic information

Product Name:
(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE
Synonyms:
  • (chloromethyl)triphenylphosphonium chliride
  • Chloromethyl triphenylphosphonium chloride, 98+%
  • (Chloromethyl)triphenylphosphoniumchloridetech
  • (CHLOROMETHYL)-TRIPHENYLPHOSPHONIUM CHLORIDE TECH 95%
  • (Chloromethly)triphenylphosphonium chloride
  • (Chloromethyl)-triphenylphosphonium chloride, 95%, tech
  • (Chloromethyl)triphenylphosphonium chloride purum
  • NSC 93980
CAS:
5293-84-5
MF:
C19H17Cl2P
MW:
347.22
EINECS:
226-139-9
Product Categories:
  • Phosphonium Compounds
  • Synthetic Organic Chemistry
  • Wittig & Horner-Emmons Reaction
  • Wittig Reaction
  • C-C Bond Formation
  • Olefination
  • Wittig Reagents
Mol File:
5293-84-5.mol
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(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE Chemical Properties

Melting point:
262-264 °C (lit.)
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
form 
Fine Crystalline Powder
color 
White to almost white
Water Solubility 
almost transparency
BRN 
3599784
InChIKey
SXYFAZGVNNYGJQ-UHFFFAOYSA-M
CAS DataBase Reference
5293-84-5(CAS DataBase Reference)
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-37/39
WGK Germany 
3
RTECS 
TA1882000
HS Code 
29310099

MSDS

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(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDE Usage And Synthesis

Chemical Properties

white to almost white fine crystalline powder

Uses

(Chloromethyl)triphenylphosphonium Chloride is a Wittig reagent.

Uses

Used for corrosion inhibition of iron

Reactant involved in:

  • Acting as a potential electrophile
  • Elimination reactions for the synthesis of linear alkynes
  • Intramolecular nucleophilic vinylic substitution
  • Homologation of aldehydes
  • Endo-selective alkynol cycloisomerization

Preparation

(Chloromethyl)triphenylphosphonium chliride is available commercially (chloride or iodide salt) or synthetically from Triphenylphosphine and Chloroiodomethane.

Reactivity Profile

(Chloromethyl)triphenylphosphonium chliride is a precursor to the chloro-substituted ylide for Wittig reactions with aldehydes and ketones to form 1-chloroalkenes and, after elimination of HCl, terminal alkynes.

Precautions

For best results the anhydrous salt should be used. The ylide, formed from the salt and strong base, will react with air, water, or other acidic protons

(CHLOROMETHYL)TRIPHENYLPHOSPHONIUM CHLORIDESupplier

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