Basic information Safety Supplier Related

1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE

Basic information Safety Supplier Related

1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE Basic information

Product Name:
1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE
Synonyms:
  • 1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE
  • 5,6-Dihydro-1H-cyclopenta[c]furan-1,3(4H)-dione
  • Cyclopentene-1,2-dicarboxylic acid anhydride
  • 4,5,6,6a-Tetrahydro-1H-cyclopenta[c]furan-1,3(3aH)-dione
  • Cyclopentane-1,2-dicarboxylic anhydride
  • 5,6-dihydro-4H-cyclopenta[c]furan-1,3-dione
  • 5,6-dihydro-4H-cyclopenta[c]furan-1,3-quinone
  • NSC 291644
CAS:
3205-94-5
MF:
C7H6O3
MW:
138.12
Product Categories:
  • Carbonyl Compounds
  • Carboxylic Acid Anhydrides
  • Organic Building Blocks
  • Building Blocks
  • Carbonyl Compounds
  • Carboxylic Acid Anhydrides
  • Chemical Synthesis
  • Organic Building Blocks
Mol File:
3205-94-5.mol
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1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE Chemical Properties

Melting point:
42-45 °C (lit.)
Boiling point:
133-135 °C/10 mmHg (lit.)
Density 
1.2667 (rough estimate)
refractive index 
n20/D 1.4978(lit.)
Flash point:
>230 °F
storage temp. 
under inert gas (nitrogen or Argon) at 2-8°C
BRN 
123650
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Safety Information

Hazard Codes 
Xi
Risk Statements 
36/37/38
Safety Statements 
26-36
WGK Germany 
3
21

MSDS

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1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDE Usage And Synthesis

Uses

Valuable Diels-Alder dienophile, for example, in approach to the bicycloundecane system in taxanes.

Purification Methods

If IR has OH peaks, then some hydrolysis to the diacid (m 178o) must have occurred. In this case reflux it with an appropriate volume of Ac2O for 30minutes, evaporate the Ac2O and distil it in vacuo. The distillate solidifies and can be recrystallised from EtOAc/hexane (1:1). The diacid distils without decomposition due to formation of the anhydride. The dimethyl ester has m 120-125o/11mm. [Askain Chem Ber 98 2322 1965, Beilstein 17/11 V 125.]

1-CYCLOPENTENE-1,2-DICARBOXYLIC ANHYDRIDESupplier

Energy Chemical
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Syntechem Co.,Ltd
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