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3'-METHOXYPHENACYL BROMIDE

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3'-METHOXYPHENACYL BROMIDE Basic information

Product Name:
3'-METHOXYPHENACYL BROMIDE
Synonyms:
  • 3'-Methoxyphenacyl Bromide [for HPLC Labeling]
  • Ethanone, 2-bromo-1-(3-methoxyphenyl)-
  • bromomethyl 3-methoxyphenyl ketone
  • AKOS BBS-00003869
  • ALPHA-BROMO-M-METHOXYACETOPHENONE
  • ALPHA-BROMO-3'-METHOXYACETOPHENONE
  • M-METHOXYPHENACYL BROMIDE
  • 2-BROMO-3''-METHOXYACETOPHENONE 97%
CAS:
5000-65-7
MF:
C9H9BrO2
MW:
229.07
EINECS:
225-666-1
Product Categories:
  • Aromatics
  • Intermediates
  • Aromatic Halides (substituted)
  • Analytical Chemistry
  • Carboxyl Group Labeling Reagents for HPLC
  • HPLC Labeling Reagents
  • UV Detection (HPLC Labeling Reagents)
Mol File:
5000-65-7.mol
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3'-METHOXYPHENACYL BROMIDE Chemical Properties

Melting point:
60-62 °C(lit.)
Boiling point:
215.8°C (rough estimate)
Density 
1.4921 (rough estimate)
refractive index 
1.5500 (estimate)
storage temp. 
2-8°C
solubility 
soluble in Methanol
form 
Crystalline Powder
color 
White to slightly yellow-green
BRN 
510128
CAS DataBase Reference
5000-65-7(CAS DataBase Reference)
NIST Chemistry Reference
2-Bromo-3'-methoxyacetophenone(5000-65-7)
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Safety Information

Hazard Codes 
C
Risk Statements 
34-36/37-22
Safety Statements 
26-27-28-36/37/39-45-34
RIDADR 
UN 3261 8/PG 2
WGK Germany 
3
HazardClass 
8
PackingGroup 
III
HS Code 
29147000

MSDS

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3'-METHOXYPHENACYL BROMIDE Usage And Synthesis

Chemical Properties

WHITE TO SLIGHTLY YELLOW-GREEN CRYST. POWDER

Uses

Derivatizing reagent.

Uses

2-bromo-3′-methoxyacetophenone, an alkylating agent, has been used to stabilize clopidogrel active metabolite (AM) in human plasma. It has also been used in the derivatisation of active metabolites in blood to ensure its stability during sample processing and storage.

Preparation

Obtained by reaction of bromine with 3-methoxyacetophenone in chloroform at 0° for 3 h (88%).

3'-METHOXYPHENACYL BROMIDESupplier

Guangdong Fangxin Biotechnology Co., Ltd. Gold
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Shanghai Boyle Chemical Co., Ltd.
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J & K SCIENTIFIC LTD.
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Meryer (Shanghai) Chemical Technology Co., Ltd.
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Alfa Aesar
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