AC-ALA-NHME Chemical Properties

Melting point:

181.2-182.0 °C (sublm)

Boiling point:

406.7±28.0 °C(Predicted)

Density 

1.031±0.06 g/cm3(Predicted)

storage temp. 

Store at 0-5°C

pka

14.62±0.46(Predicted)

AC-ALA-NHME Usage And Synthesis

Chemical Properties

White powder

Purification Methods

Crystallise the amide from EtOAc/Et2O, then from EtOH and Et2O. Also recrystallise it twice by dissolving ~2.5g in hot 200mL of toluene and cooling. It sublimes at ~170o , so its m is measured in a sealed tube. [Applewhite & Niemann J Am Chem Soc 81 2212 1959, Beilstein 4 IV 2500.]

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