1-BOC-AMINO-BUTYL-3-AMINE Chemical Properties

Boiling point:

282.6±23.0 °C(Predicted)

Density 

0.972±0.06 g/cm3(Predicted)

storage temp. 

Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

pka

12.77±0.46(Predicted)

1-BOC-AMINO-BUTYL-3-AMINE Usage And Synthesis

Synthesis

Under nitrogen protection, 1,3-dimethylethyl phenylmethyl-1,3-butanediyl biscarbamate (0.19 g, 0.59 mmol) was dissolved in 5 mL of ethanol and 30 mg of 10% palladium/carbon catalyst was added. The reaction mixture was placed under hydrogen atmosphere (1 atm) and stirred at room temperature for 5 hours. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated to give 0.10 g of tert-butyl (3-aminobutyl)carbamate in 90% yield.

References

[1] Patent: WO2006/29210, 2006, A2. Location in patent: Page/Page column 125

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