4-FLUORO-3-METHOXYBENZYL ALCOHOL Chemical Properties

Melting point:

48-49℃

Boiling point:

260℃

Density 

1.187

Flash point:

126℃

storage temp. 

2-8°C

pka

13.98±0.10(Predicted)

form 

crystalline solid

color 

White

InChI

1S/C8H9FO2/c1-11-8-4-6(5-10)2-3-7(8)9/h2-4,10H,5H2,1H3

InChIKey

FZEDGSMVRLKUOQ-UHFFFAOYSA-N

SMILES

COc1cc(CO)ccc1F

CAS DataBase Reference

128495-45-4(CAS DataBase Reference)

Safety Information

Hazard Codes 

C,Xn

Risk Statements 

36/37/38-22

Safety Statements 

26-36

WGK Germany 

WGK 3

HS Code 

2909498090

Storage Class

11 - Combustible Solids

Hazard Classifications

Acute Tox. 4 Oral
Eye Dam. 1

4-FLUORO-3-METHOXYBENZYL ALCOHOL Usage And Synthesis

Synthesis Reference(s)

Journal of Medicinal Chemistry, 33, p. 2408, 1990 DOI: 10.1021/jm00171a014

Synthesis

A solution of borane tetrahydrofuran complex (11.1 mL of 11.0 mmol added dropwise) of 4-fluoro-3-methoxybenzaldehyde (1.54 g, 10.0 mmol) was added to tetrahydrofuran (30 mL) under ice-cold, and the mixture was stirred at room temperature overnight. Methanol was added and the solvent was removed by distillation to give 4 -fluoro- 3 -methoxybenzyl alcohol crystals (1.56 g, quantitatively).

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