Ethyl N-cyanoethanimideate Chemical Properties

Melting point:

78-81 °C(Solv: ethyl ether (60-29-7))

Boiling point:

133.2±23.0 °C(Predicted)

Density 

0.94

refractive index 

1.45

storage temp. 

2-8°C

pka

-2.94±0.50(Predicted)

CAS DataBase Reference

1558-82-3(CAS DataBase Reference)

Safety Information

HS Code 

2926.90.5050

Ethyl N-cyanoethanimideate Usage And Synthesis

Preparation

To a flask equipped as in Preparation 2-6 is added 162.0 gm (1.0 mole) of ethyl orthoacetate, 42.0 gm (1.0 mole) of cyanamide, and 134.0 gm (2.0 moles) of acetic anhydride. The reaction mixture is heated to 130-140°C and the ethyl acetate and acetic acid are distilled over. The heat is removed until the initial vigorous reaction subsides and then the heat­ing is continued at 135-140°C until most of the remaining ethyl acetate and acetid acid have distilled over (approx. 1 hr). The residue is then distilled under reduced pressure to afford 100.8 gm (90%), b.p. 90-95°C (20 mm Hg).

Ethyl N-cyanoethanimideate(1558-82-3)Related Product Information

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• Ethyl formate
• Ethanol
• ISOXADIFEN-ETHYL
• Methylene dithiocyanate
• Tris(trimethylsilyl)phosphate
• ETHYL 2-CYANOACRYLATE
• Ethyl cyanoformate
• Sodium cyanoborohydride
• Ethyl isocyanoacetate
• Methyl acrylate
• 2-Ethoxyethanol
• 2-Cyanoacetamide
• Ethylparaben
• Ethyl pyruvate
• Trinexapac-ethyl
• Dimethyl succinate
• Methyl 4-cyanobenzoate