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Methyl cyanoformate

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Methyl cyanoformate Basic information

Product Name:
Methyl cyanoformate
Synonyms:
  • Carbonocyanidic acid, methyl ester
  • carbonocyanidicacid,methylester
  • CH3OC(O)CN
  • Cyanoformate methyl ester
  • cyanoformatemethylester
  • Cyanoformicacid,methylester
  • cyano-formicacimethylester
  • Cyklon A
CAS:
17640-15-2
MF:
C3H3NO2
MW:
85.06
EINECS:
241-626-6
Product Categories:
  • C2 to C5
  • Carbonyl Compounds
  • Esters
Mol File:
17640-15-2.mol
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Methyl cyanoformate Chemical Properties

Melting point:
185-186 °C
Boiling point:
100-101 °C (lit.)
Density 
1.072 g/mL at 25 °C (lit.)
refractive index 
n20/D 1.374(lit.)
Flash point:
79 °F
BRN 
1742994
EPA Substance Registry System
Carbonocyanidic acid, methyl ester (17640-15-2)
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Safety Information

Hazard Codes 
T+
Risk Statements 
10-26/27/28-36/38-36/37/38
Safety Statements 
26-28-36/37-45
RIDADR 
UN 3275 6.1/PG 2
WGK Germany 
3
RTECS 
LQ7525000
10-19-21
HazardClass 
3.2
PackingGroup 
III

MSDS

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Methyl cyanoformate Usage And Synthesis

Description

Methyl cyanoformate is the organic compound with the formula CH3OC(O)CN. It is used as a reagent in organic synthesis as a source of the methoxy carbonyl group , in which context it is also known as Mander's reagent. It was also the active ingredient in the pesticide product Zyklon A.

Chemical Properties

Colorless liquid; ethereal odor. Decomposedby alkalies and water. Soluble in alcohol, benzene,ether.

Uses

Selective acylating reagent.

Uses

Organic synthesis.

Purification Methods

Purify the ester by fractionation through a 45cm glass helices packed column or a 30cm spinning band column. [Sheppard J Org Chem 27 3756 1962.] It has been distilled through a short Vigreux column (p 11), and further purified by recrystallisation from Et2O at -40o as white crystals which melt at room temperature. NMR:  4.0 ( C3), and IR: 2250 (CN) and 1750 (CO) cm-1 . [Childes & Weber JOrg Chem 41 3486 1976, Beilstein 2 III 1587.]

Methyl cyanoformateSupplier

Energy Chemical
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Shanghai Hanhong Scientific Co.,Ltd.
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Syntechem Co.,Ltd
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HBCChem, Inc.
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