ChemicalBook > Product Catalog > Organic Chemistry > Amides > Naphthenic amines derivatives > 2-Bromo-3-methylaniline
2-Bromo-3-methylaniline
2-Bromo-3-methylaniline Basic information
- Product Name:
- 2-Bromo-3-methylaniline
- Synonyms:
-
- 3-Amino-2-bromotoluene
- 2-broMo-3-MethylbenzenaMine
- BenzenaMine, 2-broMo-3-Methyl-
- 2-BROMO-3-METHYLANILINE 98
- 2-BroMo-3-Methylaniline, 97+%
- 2-BROMO-3-METHYLANILIN
- 2-Bromo-3-methylaniline, 98%, for synthesis
- 2-BROMO-3-METHYLANILINE 98 ISO 9001:2015 REACH
- CAS:
- 54879-20-8
- MF:
- C7H8BrN
- MW:
- 186.05
- Product Categories:
-
- Anilines, Amides & Amines
- Bromine Compounds
- Amines
- C7
- Nitrogen Compounds
- Mol File:
- 54879-20-8.mol
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2-Bromo-3-methylaniline Chemical Properties
- Boiling point:
- 48 °C/0.03 mmHg (lit.)
- Density
- 1.489 g/mL at 25 °C (lit.)
- refractive index
- n20/D 1.605(lit.)
- Flash point:
- >230 °F
- storage temp.
- Keep in dark place,Sealed in dry,Room Temperature
- form
- Liquid
- pka
- 2.66±0.10(Predicted)
- color
- Pale brown
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Safety Information
- Hazard Codes
- Xn
- Risk Statements
- 22-43-36/37/38-20/21/22
- Safety Statements
- 36/37-60-26-23-9
- RIDADR
- 2810
- WGK Germany
- 3
- HazardClass
- 6.1
- HS Code
- 29214300
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2-Bromo-3-methylaniline Usage And Synthesis
Synthesis
Add iron powder (3.86 g, 69 mmol), water (5 mL) and concentrated HCL (0.5 mL) sequentially to a solution of commercially available 2-bromo-3-nitrotoluene (5 g, 23 mmol) in methanol (100 mL) at room temperature and heat the mixture at reflux for 125 h. Remove the solvents under reduced pressure, suspend the residue in water (400 mL) and extract with chloroform (3 x 250 mL). Dry the combined organic extracts over MGS04 and remove the solvents under reduced pressure to afford 2-bromo-3-methylphenylamine as an amber oil (4.45 g, 100percent): 1H NMR (CDC13) 5 2.30 (s, 3H), 4.00 (br s, 2H), 7.60 (m, 2H), 7.00 (t, 1H).
2-Bromo-3-methylanilineSupplier
FUXIN QINGJISHENG SCIENCE AND TECHNOLOGY CO.,LID Gold
- Tel
- 13365798276
- hxy696128@126.com
Alfa Aesar
- Tel
- 400-6106006
- saleschina@alfa-asia.com
Energy Chemical
- Tel
- 021-021-58432009 400-005-6266
- sales8178@energy-chemical.com
Shanghai Sinch Parmaceuticals Tech. Co. Ltd.
- Tel
- +86-21-54098501
- sales@sinch.com.cn
Jia Xing Isenchem Co.,Ltd
- Tel
- 0573-85285100 18627885956
- isenchem@163.com
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2-Bromo-3-methylaniline(54879-20-8)Related Product Information
- 2-bromo-3-methyl-phenol
- Broxitalamic acid
- 2-Bromo-3-nitrotoluene
- Ethyl 2-bromo-3-nitrobenzoate
- 2-Bromo-3-nitrobenzoic acid
- 3-METHYL-2,4,6-TRIBROMOANILINE
- 2,4-Dibromo-6-methylaniline
- 3-BROMO-2-METHYLANILINE, 98+%
- 3,5-DIBROMO-4-METHYLANILINE
- 2-BROMO-4-METHYLANILINE HYDROCHLORIDE
- 4-BROMO-2-METHYLANILINE
- 4-Bromo-N,N-dimethylaniline
- 2,6-Dibromo-4-methylaniline
- 5-(BENZYLOXY)-2-BROMO-4-METHYLANILINE
- 4-Bromo-3-methylaniline
- 4-Bromo-3-methylaniline hydrochloride
- 3-BROMO-N-METHYLANILINE
- 4-BROMO-2-METHYLANILINE HYDROCHLORIDE