4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE
4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE Basic information
- Product Name:
- 4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE
- Synonyms:
-
- 4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE
- JRH-01113, 1-(2-Hydroxy-4,5-dimethylphenyl)propan-1-one, 97%
- 1-Propanone, 1-(2-hydroxy-4,5-dimethylphenyl)-
- 1-(2-Hydroxy-4,5-dimethylphenyl)-1-propanone
- CAS:
- 5384-13-4
- MF:
- C11H14O2
- MW:
- 178.23
- Mol File:
- 5384-13-4.mol
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4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE Chemical Properties
- Melting point:
- 60–61°C
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4'5'-DIMETHYL-2'-HYDROXYPROPIOPHENONE Usage And Synthesis
Preparation
Preparation by Fries rearrangement of 3,4-dimethylphenyl propionate with aluminium chloride
without solvent between 120° and 150° (quantitative yield), at 165° for 1 h (93%), at 100° for 2 h (90%), at 110° (85%) and in the presence of sodium chloride ;
in nitromethane at 20° for 7 days (89%).
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