2-ethoxy-5-methylaniline Chemical Properties

storage temp. 

Keep in dark place,Inert atmosphere,Room temperature

Appearance

Yellow to brown Solid

Safety Information

HS Code 

2921420090

2-ethoxy-5-methylaniline Usage And Synthesis

Synthesis

General procedure for the synthesis of 2-amino-4-methylphenylethyl ether from 4-ethoxy-3-nitrotoluene: A suspension formed by 1-ethoxy-4-methyl-2-nitrobenzene (2.71 g) with 10% palladium-carbon catalyst (0.27 g) in anhydrous tetrahydrofuran (40 mL) was stirred at room temperature. After 25.5 hours of reaction in a hydrogen atmosphere, the reaction mixture was filtered through cellulose powder. The filtrate was concentrated under reduced pressure and dried to give 2.26 g of 2-amino-4-methylphenylethyl ether as a dark brown solid in 100% yield.

References

[1] Patent: EP1764360, 2007, A1. Location in patent: Page/Page column 106
[2] Justus Liebigs Annalen der Chemie, 1883, vol. 217, p. 172
[3] Gazzetta Chimica Italiana, 1969, vol. 99, p. 397 - 410

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