3-Iodo-N-phenylcarbazole

Product Name: 3-Iodo-N-phenylcarbazole
CAS No.: 502161-03-7
Chemical Name: 3-Iodo-N-phenylcarbazole
Synonyms: 3-iodo-9-phenyl-9H-carbazole;3-Iodo-N-phenyL;3-Iodo-N-phenylcarba;3-iodo-N-phenylcarbazol;3-Iodo-9-phenylcarbazole;3-Iodo-N-phenylcarbazole;3-Iodo-9-phenylcarbazole>3- iodine-9- phenylcarbazole;3-Iodinated-N-phenylcarbazole;9H-Carbazole, 3-iodo-9-phenyl-
CBNumber: CB01073966
Molecular Formula: C18H12IN
Formula Weight: 369.2
MOL File: 502161-03-7.mol

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3-Iodo-N-phenylcarbazole Property

Melting point:: 103.0 to 107.0 °C
Boiling point:: 480.6±27.0 °C(Predicted)
Density: 1.55±0.1 g/cm3(Predicted)
storage temp.: Keep in dark place,Sealed in dry,Room Temperature
form: powder to crystal
color: White to Light yellow
CAS DataBase Reference: 502161-03-7

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Safety

HS Code: 2933998090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

Precautionary statements

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

P332+P313IF SKIN irritation occurs: Get medical advice/attention.

P337+P313IF eye irritation persists: Get medical advice/attention.

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N-Bromosuccinimide Price

TCI Chemical

Product number: I0913
Product name: 3-Iodo-9-phenylcarbazole
Purity: >98.0%(GC)
Packaging: 1g
Price: $36
Updated: 2025/07/31

TCI Chemical

Product number: I0913
Product name: 3-Iodo-9-phenylcarbazole
Purity: >98.0%(GC)
Packaging: 5g
Price: $50
Updated: 2025/07/31

AK Scientific

Product number: J97724
Product name: 3-Iodo-N-phenylcarbazole
Packaging: 5g
Price: $25
Updated: 2021/12/16

ChemScene

Product number: CS-W021948
Product name: 3-Iodo-N-phenylcarbazole
Purity: 98.72%
Packaging: 25g
Price: $50
Updated: 2021/12/16

Chem-Impex

Product number: 30934
Product name: 3-Iodo-9-phenylcarbazole,≥98%(GC)
Purity: ≥98%(GC)
Packaging: 5G
Price: $61.17
Updated: 2021/12/16

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3-Iodo-N-phenylcarbazole Chemical Properties,Usage,Production

Chemical Properties

White crystalline powder

Synthesis

1150-62-5

502161-03-7

General procedure for the synthesis of 3-iodo-9-phenylcarbazole from N-phenylcarbazole: 2.433 g (10 mmol) of intermediate compound A (N-phenylcarbazole) was dissolved in 100 mL of 80% acetic acid solution, followed by the sequential addition of 1.357 g (5.35 mmol) of iodine monomers (I2) and 0.333 g (1.46 mmol) of o-n-octanoic acid ( H5IO6). The reaction mixture was stirred at 80 °C for 2 h under nitrogen protection. After completion of the reaction, the reaction mixture was extracted three times with ether (50 mL). The organic layers were combined and dried with anhydrous magnesium sulfate, followed by evaporation under reduced pressure to remove the solvent. The resulting crude product was purified by silica gel column chromatography to afford 3.23 g of intermediate compound B (3-iodo-9phenylcarbazole) as a white solid in 87% yield.1H NMR (CDCl3, 300 MHz) δ (ppm): 8.43 (d, 1H), 8.05 (d, 1H), 7.62 (dd, 1H), 7.61-7.75 (m, 2H) , 7.51-7.43 (m, 3H), 7.41-7.35 (m, 2H), 7.27 (dd, 1H), 7.14 (d, 1H).

References

[1] Patent: EP1661888, 2006, A1. Location in patent: Page/Page column 11
[2] Patent: US2008/174237, 2008, A1. Location in patent: Page/Page column 13-14
[3] Patent: EP2149555, 2010, A1. Location in patent: Page/Page column 19
[4] Patent: KR101791161, 2017, B1. Location in patent: Paragraph 0116; 0123-0128
[5] Patent: EP2738166, 2014, A1. Location in patent: Paragraph 0162

3-Iodo-N-phenylcarbazole Preparation Products And Raw materials

Raw materials

Preparation Products

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3-Iodo-N-phenylcarbazole Suppliers

Americas 1 Belgium 1 China 231 Europe 1 Germany 5 India 15 Japan 3 Lithuania 1 Switzerland 1 United Kingdom 4 United States 18 Global 281

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View Lastest Price from 3-Iodo-N-phenylcarbazole manufacturers

Hebei Fengjia New Material Co., Ltd

Product: 3-Iodo-N-phenylcarbazole 502161-03-7
Price: US $2.00/kg
Min. Order: 1kg
Purity: 0.99
Supply Ability: 10000
Release date: 2024-08-08

Hebei Chuanghai Biotechnology Co., Ltd

Product: 3-Iodo-N-phenylcarbazole 502161-03-7
Price: US $10.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 5tons
Release date: 2024-12-04

Shanghai Daken Advanced Materials Co.,Ltd

Product: 9H-Carbazole, 3-iodo-9-phenyl- 502161-03-7
Price: US $0.00/KG
Min. Order: 1KG
Purity: 98.00%
Supply Ability: 150KG /month
Release date: 2021-11-17

502161-03-7, 3-Iodo-N-phenylcarbazoleRelated Search:

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502161-03-7

C18H12IN

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