8-Chloro-1-octene
- Product Name
- 8-Chloro-1-octene
- CAS No.
- 871-90-9
- Chemical Name
- 8-Chloro-1-octene
- Synonyms
- 1-Octene, 8-chloro-;Oct-7-en-1-yl chloride;8-CHLORO-1-OCTENE, 97%8-CHLORO-1-OCTENE, 97%8-CHLORO-1-OCTENE, 97%8-CHLORO-1-OCTENE, 97%
- CBNumber
- CB01074105
- Molecular Formula
- C8H15Cl
- Formula Weight
- 146.66
- MOL File
- 871-90-9.mol
8-Chloro-1-octene Property
- Boiling point:
- 180.9±19.0 °C(Predicted)
- Density
- 0.877±0.06 g/cm3(Predicted)
- storage temp.
- 2-8°C
- Appearance
- Colorless to light yellow Liquid
Safety
- HS Code
- 2903290000
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H315Causes skin irritation
H319Causes serious eye irritation
H332Harmful if inhaled
H335May cause respiratory irritation
- Precautionary statements
-
P233Keep container tightly closed.
P260Do not breathe dust/fume/gas/mist/vapours/spray.
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P271Use only outdoors or in a well-ventilated area.
P280Wear protective gloves/protective clothing/eye protection/face protection.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P302+P352IF ON SKIN: wash with plenty of soap and water.
P304IF INHALED:
P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
P312Call a POISON CENTER or doctor/physician if you feel unwell.
P321Specific treatment (see … on this label).
P330Rinse mouth.
P332+P313IF SKIN irritation occurs: Get medical advice/attention.
P337+P313IF eye irritation persists: Get medical advice/attention.
P340Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P362Take off contaminated clothing and wash before reuse.
P403Store in a well-ventilated place.
P403+P233Store in a well-ventilated place. Keep container tightly closed.
P405Store locked up.
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- 23791
- Product name
- 8-CHLORO-1-OCTENE,97%
- Packaging
- 5G
- Price
- $159.78
- Updated
- 2021/12/16
- Product number
- 23792
- Product name
- 8-CHLORO-1-OCTENE,97%
- Packaging
- 25g
- Price
- $609.91
- Updated
- 2021/12/16
- Product number
- 102963
- Product name
- 8-Chloro-1-octene
- Packaging
- 5g
- Price
- $812
- Updated
- 2021/12/16
- Product number
- HCH0006907
- Product name
- 8-CHLOROOCT-1-ENE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $836.8
- Updated
- 2021/12/16
- Product number
- 10001-001f
- Product name
- 8-chloro-1-octene
- Purity
- 97%
- Packaging
- 5g
- Price
- $930
- Updated
- 2021/12/16
8-Chloro-1-octene Chemical Properties,Usage,Production
Synthesis
6294-17-3
75-01-4
871-90-9
1. 2.55 g (105 mmol) of magnesium metal (20-50 mesh) and 75 g of tetrahydrofuran (THF) were added to a 200 mL flask, replaced with a nitrogen atmosphere, and the reaction solution was cooled to 0 °C with stirring. 2. After cooling, the Grignard reagent was prepared by slow dropwise addition of 19.95 g (100 mmol) of 1-bromo-6-chlorohexane (solvent to dihaloalkane weight ratio 3.76) for about 2 hours and aging at the same temperature for 2 hours. 3. The reaction solution was analyzed by gas chromatography (GC) with a yield of 86 area% and a selectivity of 86% for the Grignard reagent. 4. 0.16 g (1.0 mmol) of ferric chloride was added to the Grignard reagent solution, maintained at 0 °C, and 6.25 g (100 mmol) of vinyl chloride was drummed into the solution over a period of 2 hours and aged at that temperature for 1 hour. 5. Upon completion of the reaction, 10% aqueous ammonium chloride and methylene chloride were added to dissolve and separate the resulting salt. 6. After separation of the organic layer, 8-chloro-1-octene was quantified by gas chromatography (GC) to give 8-chloro-1-octene as the target product in 72% yield. The results are shown in Table 4.
References
[1] Patent: JP5885213, 2016, B2. Location in patent: Paragraph 0041; 0042; 0043
8-Chloro-1-octene Preparation Products And Raw materials
Raw materials
Preparation Products
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