ChemicalBook > CAS DataBase List > METHYL 3-CYANO-4-METHOXYBENZOATE

METHYL 3-CYANO-4-METHOXYBENZOATE

Uses

Product Name: METHYL 3-CYANO-4-METHOXYBENZOATE
CAS No.: 25978-74-9
Chemical Name: METHYL 3-CYANO-4-METHOXYBENZOATE
Synonyms: METHYL 3-CYANO-4-METHOXYBENZOATE;3-Cyano-4-methoxybenzoic acid methyl ester;methyl 3-cyano-4-methoxybenzoate - [M85982];Benzoic acid, 3-cyano-4-methoxy-, methyl ester
CBNumber: CB0144973
Molecular Formula: C10H9NO3
Formula Weight: 191.18
MOL File: 25978-74-9.mol

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METHYL 3-CYANO-4-METHOXYBENZOATE Property

Melting point:: 124 °C
Boiling point:: 339.7±27.0 °C(Predicted)
Density: 1.20±0.1 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
Appearance: White to yellow Solid
BRN: 2374769
InChI: InChI=1S/C10H9NO3/c1-13-9-4-3-7(10(12)14-2)5-8(9)6-11/h3-5H,1-2H3
InChIKey: RYJSFYBJYKFNCF-UHFFFAOYSA-N
SMILES: C(OC)(=O)C1=CC=C(OC)C(C#N)=C1
CAS DataBase Reference: 25978-74-9

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Safety

Risk Statements: 20/21/22-36/37/38
Safety Statements: 26-36/37/39
RIDADR: 3439
HazardClass: 6.1
PackingGroup: III
HS Code: 2926907090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Danger

Hazard statements

H302Harmful if swallowed

H331Toxic if inhaled

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P304+P340IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.

P405Store locked up.

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N-Bromosuccinimide Price

TRC

Product number: M338278
Product name: Methyl3-Cyano-4-methoxybenzoate
Packaging: 100mg
Price: $75
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC55139
Product name: 3-Cyano-4-methoxybenzoic acid methyl ester
Packaging: 5G
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC55139
Product name: 3-Cyano-4-methoxybenzoic acid methyl ester
Packaging: 10g
Price: $90
Updated: 2021/12/16

SynQuest Laboratories

Product number: 4637-1-U8
Product name: Methyl 3-cyano-4-methoxybenzoate
Packaging: 1g
Price: $96
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FC55139
Product name: 3-Cyano-4-methoxybenzoic acid methyl ester
Packaging: 25g
Price: $175
Updated: 2021/12/16

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METHYL 3-CYANO-4-METHOXYBENZOATE Chemical Properties,Usage,Production

Uses

Methyl 3-Cyano-4-methoxybenzoate is a useful research chemical.

Synthesis

35450-37-4

25978-74-9

General procedure for the synthesis of methyl 3-cyano-4-methoxybenzoate from methyl 3-bromo-4-methoxybenzoate: to a solution of methyl 3-bromo-4-methoxybenzoate (1.1 g, 4.4 mmol) in dimethylformamide (10 mL) was added cuprous cyanide (1.2 g, 13.2 mmol). The reaction mixture was heated to 140 °C and maintained for 6 hours. After the reaction was completed, it was cooled to room temperature and diluted by adding ethyl acetate (25 mL). The organic phase was washed with saturated sodium chloride solution, dried over anhydrous sodium sulfate and concentrated under reduced pressure. The crude product was purified by fast column chromatography (eluent: petroleum ether/ethyl acetate=10:1) to afford methyl 3-cyano-4-methoxybenzoate (662 mg, 79% yield) as a white solid.

References

[1] Patent: CN106146504, 2016, A. Location in patent: Paragraph 0219; 0220; 0221; 0224; 0225

METHYL 3-CYANO-4-METHOXYBENZOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from METHYL 3-CYANO-4-METHOXYBENZOATE manufacturers

Capot Chemical Co.,Ltd.

Product: Methyl 3-cyano-4-methoxybenzoate 25978-74-9
Price: US $0.00-0.00/kg
Min. Order: 1kg
Purity: 98%
Supply Ability: kgs
Release date: 2023-01-03

Career Henan Chemical Co

Product: METHYL 3-CYANO-4-METHOXYBENZOATE 25978-74-9
Price: US $3.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 100kg
Release date: 2019-07-10

25978-74-9, METHYL 3-CYANO-4-METHOXYBENZOATERelated Search:

Ethylparaben p-Toluic acid 3-Chlorobenzoic acid SODIUM LAURETH SULFATE Metaclazepam Benzoic acid Methylparaben Methyl anisate METHYL 3-CYANO-4-METHOXYBENZOATE Methyl 3-cyano-4-(2-fluorophenoxy)benzoate METHYL 3-CYANO-4-ISOPROPOXYBENZOATE Benzoic acid, 3-cyano-4-ethoxy-, methyl ester (9CI) AKOS 233-19

METHYL 3-CYANO-4-METHOXYBENZOATE

3-Cyano-4-methoxybenzoic acid methyl ester

Benzoic acid, 3-cyano-4-methoxy-, methyl ester

methyl 3-cyano-4-methoxybenzoate - [M85982]

25978-74-9

25987-74-9

Aromatic Esters