ChemicalBook > CAS DataBase List > 2-BROMO-5-HYDROXYMETHYL-ANISOLE

2-BROMO-5-HYDROXYMETHYL-ANISOLE

Product Name: 2-BROMO-5-HYDROXYMETHYL-ANISOLE
CAS No.: 17100-64-0
Chemical Name: 2-BROMO-5-HYDROXYMETHYL-ANISOLE
Synonyms: (4-broMo-3-Methoxyphenyl)Methanol;4-Bromo-3-methoxybenzyl alcohol;2-BROMO-5-HYDROXYMETHYL-ANISOLE;Benzyl alcohol, 4-bromo-3-methoxy-;Benzenemethanol, 4-bromo-3-methoxy-
CBNumber: CB01519637
Molecular Formula: C8H9BrO2
Formula Weight: 217.06
MOL File: 17100-64-0.mol

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2-BROMO-5-HYDROXYMETHYL-ANISOLE Property

Boiling point:: 306.8±27.0 °C(Predicted)
Density: 1.513±0.06 g/cm3(Predicted)
storage temp.: Sealed in dry,Room Temperature
pka: 14.04±0.10(Predicted)
form: solid
color: Faint orange/brown

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Safety

HS Code: 2909498090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

TRC

Product number: B711230
Product name: (4-Bromo-3-methoxyphenyl)methanol
Packaging: 100mg
Price: $60
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142805
Product name: (4-Bromo-3-methoxyphenyl)methanol
Packaging: 250mg
Price: $70
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142805
Product name: (4-Bromo-3-methoxyphenyl)methanol
Packaging: 500mg
Price: $125
Updated: 2021/12/16

Biosynth Carbosynth

Product number: FB142805
Product name: (4-Bromo-3-methoxyphenyl)methanol
Packaging: 1g
Price: $216
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2607-9-22
Product name: 4-Bromo-3-methoxybenzyl alcohol
Packaging: 1g
Price: $248
Updated: 2021/12/16

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2-BROMO-5-HYDROXYMETHYL-ANISOLE Chemical Properties,Usage,Production

Synthesis

6971-51-3

17100-64-0

The general procedure for the synthesis of 2-bromo-5-hydroxymethyl anisole from m-methoxybenzyl alcohol was as follows: to a solution of 3-methoxybenzyl alcohol (20.0 g, 145 mmol) in tetrahydrofuran (THF, 400 mL) was added N-bromosuccinimide (NBS, 26 g, 146 mmol). The reaction mixture was stirred at room temperature for 8 hours. After the reaction was completed, ether (500 mL) was added to dilute and the mixture was washed with deionized water (3 x 100 mL). The organic phase was dried with anhydrous magnesium sulfate, filtered and concentrated under reduced pressure to afford 2-bromo-5-hydroxymethyl anisole (31.2 g, 99% yield), and the product was used directly in the next reaction without further purification.

References

[1] Patent: US9725406, 2017, B1. Location in patent: Page/Page column 7-8
[2] Tetrahedron, 2005, vol. 61, # 49, p. 11692 - 11696
[3] Patent: US2018/208604, 2018, A1. Location in patent: Paragraph 0201-0203
[4] Patent: US2010/4159, 2010, A1. Location in patent: Page/Page column 59; 64
[5] Bioorganic and Medicinal Chemistry Letters, 2011, vol. 21, # 3, p. 1010 - 1014

2-BROMO-5-HYDROXYMETHYL-ANISOLE Preparation Products And Raw materials

Raw materials

Preparation Products

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2-BROMO-5-HYDROXYMETHYL-ANISOLE Suppliers

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17100-64-0, 2-BROMO-5-HYDROXYMETHYL-ANISOLERelated Search:

2,4-DIBROMO-3-(DIFLUOROMETHOXY)BENZOIC ACID TERT-BUTYL 3-BENZYLOXY-4-BROMOBENZOATE METHYL 3-(BENZYLOXY)-4-BROMOBENZOATE 98 TERT-BUTYL 4-BROMO-3-METHOXYBENZOATE 98 METHYL 4-BROMO-3-METHOXYBENZOATE 2-BROMO-5-HYDROXYMETHYL-ANISOLE 4-BROMO-3,5-DIMETHOXYBENZOIC ACID 3-(BENZYLOXY)-4-BROMOBENZOIC ACID 98 4-Bromo-3-methoxybenzoic acid 4-BROMO-3,5-DIMETHOXYBENZYL ALCOHOL TERT-BUTYL 4-BROMO-3,5-DIMETHOXYBENZOATE 4-BROMO-2,5-DIMETHOXYBENZOIC ACID [3-(BENZYLOXY)-4-BROMOPHENYL]METHANOL 4-BROMO-2-FLUORO-3-METHOXY-BENZOIC ACID (4-BROMO-2,5-DIMETHOXYPHENYL)METHANOL 4-BROMO-3,5-DIMETHOXYBENZOIC ACID METHYL ESTER 5-(4-BROMO-3,5-DIMETHOXYPHENYL)-1,3,4-OXADIAZOL-2(3H)-ONE AKOS 212-39

2-BROMO-5-HYDROXYMETHYL-ANISOLE

4-Bromo-3-methoxybenzyl alcohol

Benzyl alcohol, 4-bromo-3-methoxy-

(4-broMo-3-Methoxyphenyl)Methanol

Benzenemethanol, 4-bromo-3-methoxy-

17100-64-0