ChemicalBook > CAS DataBase List > 4-IODO-3-NITROTOLUENE

4-IODO-3-NITROTOLUENE

Product Name
4-IODO-3-NITROTOLUENE
CAS No.
5326-39-6
Chemical Name
4-IODO-3-NITROTOLUENE
Synonyms
3-nitro-4-iodotoluol;4-IODO-3-NITROTOLUENE;3-nitro-4-iodotoluene;4-Iodo-3-nitrotoluene,97%;4-IODO-3-NITROTOLUENE 97%;4-Iodo-3-nitrotoluene, 98.5%;4-METHYL-2-NITRO IODO BENZENE;1-Iodo-2-nitro-4-methylbenzene;1-IODO-4-METHYL-2-NITROBENZENE;Benzene, 1-iodo-4-methyl-2-nitro-
CBNumber
CB0190703
Molecular Formula
C7H6INO2
Formula Weight
263.03
MOL File
5326-39-6.mol
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4-IODO-3-NITROTOLUENE Property

Melting point:
53-56 °C(lit.)
Boiling point:
111°C 1mm
Density 
1.8886 (estimate)
Flash point:
110 °C
storage temp. 
Keep in dark place,Sealed in dry,Room Temperature
solubility 
soluble in Methanol
form 
Glistening Powder
color 
Orange-brown
CAS DataBase Reference
5326-39-6(CAS DataBase Reference)
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Safety

Hazard Codes 
Xi,Xn
Risk Statements 
36/37/38-20/21/22
Safety Statements 
26-36-36/37/39-22
WGK Germany 
3
HazardClass 
IRRITANT
HS Code 
29049090
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Hazard and Precautionary Statements (GHS)

Symbol(GHS)
Signal word
Warning
Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P264Wash hands thoroughly after handling.

P264Wash skin thouroughly after handling.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.

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N-Bromosuccinimide Price

Sigma-Aldrich
Product number
540447
Product name
4-Iodo-3-nitrotoluene
Purity
98%
Packaging
5g
Price
$60.2
Updated
2023/06/20
TCI Chemical
Product number
I1022
Product name
4-Iodo-3-nitrotoluene
Packaging
1G
Price
$27
Updated
2025/07/31
TCI Chemical
Product number
I1022
Product name
4-Iodo-3-nitrotoluene
Packaging
5G
Price
$105
Updated
2025/07/31
TRC
Product number
B448778
Product name
1-Iodo-4-methyl-2-nitrobenzene
Packaging
50mg
Price
$60
Updated
2021/12/16
AK Scientific
Product number
V1874
Product name
4-Iodo-3-nitrotoluene
Packaging
5g
Price
$19
Updated
2021/12/16
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4-IODO-3-NITROTOLUENE Chemical Properties,Usage,Production

Chemical Properties

orange-brown glistening powder

Uses

4-Iodo-3-nitrotoluene may be used in the preparation of:

  • 3-cyano-4-iodotoluene
  • 4,6′-dimethyl-2 ,2′-dinitrobiphenyl
  • bis(2-nitro-4-methylphenyl) sulfide

General Description

4-Iodo-3-nitrotoluene can be prepared from 4-amino-3-nitrotoluene according to the procedure described by Carlin and Foltz.

Synthesis

27329-27-7

5326-39-6

General procedure for the synthesis of 4-iodo-3-nitrotoluene from 4-methyl-2-nitrobenzoic acid: To a Silak reaction tube equipped with a magnetic stirrer, 6.2 mg of silver sulfate (Ag2SO4), 21.8 mg of copper acetate (Cu(OAc)2), 12.5 mg of 2,9-dimethyl-1,10-o-phenanthroline (as a ligand), 36.2 mg 4 -methyl-2-nitrobenzoic acid (as raw material) and 45 mg of sodium iodide (NaI), dissolved in 4 mL of dimethyl sulfoxide (DMSO). The reaction mixture was heated to 160°C under oxygen atmosphere and the reaction was stirred for 24 hours. Upon completion of the reaction, the reaction was quenched by the addition of distilled water and extracted three times with ethyl acetate (10 mL each time). The organic phases were combined and concentrated under reduced pressure to give 27.9 mg of 4-iodo-3-nitrotoluene (target product) in 53% yield.

References

[1] Journal of Organic Chemistry, 2016, vol. 81, # 7, p. 2794 - 2803
[2] Patent: CN107325002, 2017, A. Location in patent: Paragraph 0091
[3] Organic and Biomolecular Chemistry, 2018, vol. 16, # 30, p. 5416 - 5421

4-IODO-3-NITROTOLUENE Preparation Products And Raw materials

Raw materials

Preparation Products

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4-IODO-3-NITROTOLUENE Suppliers

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View Lastest Price from 4-IODO-3-NITROTOLUENE manufacturers

Shaanxi Dideu New Materials Co. Ltd
Product
4-IODO-3-NITROTOLUENE 5326-39-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
98.0%
Supply Ability
10000KGS
Release date
2025-07-04
Hebei Chuanghai Biotechnology Co., Ltd
Product
4-IODO-3-NITROTOLUENE 5326-39-6
Price
US $0.00-0.00/KG
Min. Order
1KG
Purity
99%
Supply Ability
20 mt
Release date
2025-03-14
Hangzhou ICH Biofarm Co., Ltd
Product
4-IODO-3-NITROTOLUENE 5326-39-6
Price
US $0.00-0.00/g
Min. Order
1g
Purity
98%
Supply Ability
2000kg
Release date
2023-07-12

5326-39-6, 4-IODO-3-NITROTOLUENERelated Search:

4-IODO-2-NITROTOLUENE 2-IODO-5-NITROTOLUENE 4-IODO-3-NITROTOLUENE N,N'-Bis(2,3-dihydroxypropyl)-5-nitro-1,3-benzenedicarboxamide 4-Iodo-3-nitrobenzoic acid METHYL 4-IODO-3-NITROBENZOATE 2-IODO-4-NITROTOLUENE 4-iodo-3-nitrobenzamide 4-IODO-3-NITRO-BENZOIC ACID ETHYL ESTER 2-AMINO-3-IODO-5-NITROTOLUENE 4-IODO-3-NITROBENZOTRIFLUORIDE 2-IODO-6-NITROTOLUENE 4-CHLORO-2-IODO-6-NITROTOLUENE 3-IODO-4-NITROTOLUENE 2-BROMO-4-IODO-6-NITROTOLUENE ALPHA-BROMO-3-IODO-4-NITROTOLUENE 2-IODO-3-NITROTOLUENE 4-BROMO-2-IODO-6-NITROTOLUENE

  • 1-(2-hydroxy-5-methoxyphenyl)-N,N,N-trimethylmethanaminium iodide
  • 4-IODO-3-NITROTOLUENE
  • 4-Iodo-3-nitrotoluene, 98.5%
  • 4-IODO-3-NITROTOLUENE 97%
  • 1-IODO-4-METHYL-2-NITROBENZENE
  • 1-Iodo-2-nitro-4-methylbenzene
  • 3-nitro-4-iodotoluene
  • 4-Iodo-3-nitrotoluene,97%
  • 3-nitro-4-iodotoluol
  • Benzene, 1-iodo-4-methyl-2-nitro-
  • 4-METHYL-2-NITRO IODO BENZENE
  • 5326-39-6
  • O2NC6H3ICH3
  • IC6H3CH3NO2
  • Nitrogen Compounds
  • Organic Building Blocks
  • Nitro Compounds
  • Building Blocks
  • Aromatic Hydrocarbons (substituted) & Derivatives
  • Halogen toluene
  • Nitro Compounds
  • Nitrogen Compounds
  • Organic Building Blocks