(3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER
- Product Name
- (3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER
- CAS No.
- 610302-03-9
- Chemical Name
- (3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER
- Synonyms
- 3-(Boc-aMino)cyclohexanol;3-N-BOC-AMINO-CYCLOHEXANOL;1-N-Boc aminocyclohexan-3-ol;TERT-BUTYL 3-HYDROXYCYCLOHEXYL CARBAMATE;5-amino-2-methylpyridine-3-carboxylic acid;tert-butyl N-(3-hydroxycyclohexyl)carbaMate;cis-1-N-Boc-3-hydroxy-cyclohexylamine(racemic);1,1-DiMethylethyl (3-hydroxycyclohexyl)carbaMate;trans-1-N-Boc-3-hydroxy-cyclohexylamine (racemic);1,1-Dimethylethyl N-(3-hydroxycyclohexyl)carbamate
- CBNumber
- CB0214074
- Molecular Formula
- C11H21NO3
- Formula Weight
- 215.29
- MOL File
- 610302-03-9.mol
(3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER Property
- Boiling point:
- 337.7±31.0 °C(Predicted)
- Density
- 1.06
- storage temp.
- 2-8°C
- pka
- 12.32±0.40(Predicted)
- Appearance
- White to off-white Solid
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H302Harmful if swallowed
H410Very toxic to aquatic life with long lasting effects
- Precautionary statements
-
P264Wash hands thoroughly after handling.
P264Wash skin thouroughly after handling.
P270Do not eat, drink or smoke when using this product.
P273Avoid release to the environment.
P301+P312IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P330Rinse mouth.
P391Collect spillage. Hazardous to the aquatic environment
P501Dispose of contents/container to..…
N-Bromosuccinimide Price
- Product number
- H950098
- Product name
- (3-Hydroxy-cyclohexyl)-carbamicacidtert-butylester
- Packaging
- 250mg
- Price
- $50
- Updated
- 2021/12/16
- Product number
- CS-W003310
- Product name
- (3-Hydroxy-cyclohexyl)carbamicacidtert-butylester
- Purity
- 97.37%
- Packaging
- 10g
- Price
- $181
- Updated
- 2021/12/16
- Product number
- W7334
- Product name
- (3-Hydroxy-cyclohexyl)-carbamicacidtert-butylester
- Packaging
- 5g
- Price
- $228
- Updated
- 2021/12/16
- Product number
- W7334
- Product name
- (3-Hydroxy-cyclohexyl)-carbamicacidtert-butylester
- Packaging
- 250mg
- Price
- $89
- Updated
- 2021/12/16
- Product number
- W7334
- Product name
- (3-Hydroxy-cyclohexyl)-carbamicacidtert-butylester
- Packaging
- 1g
- Price
- $100
- Updated
- 2021/12/16
(3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER Chemical Properties,Usage,Production
Synthesis
885280-38-6
610302-03-9
The general procedure for the synthesis of tert-butyl 3-hydroxycyclohexylcarbamate from N-Boc-3-cyclohexanone amine was as follows: sodium borohydride (710 mg, 18.8 mmol, 2.0 eq.) was slowly added to a solution of tert-butyl 3-oxocyclohexylcarbamate (2.0 g, 9.38 mmol, 1.0 eq.) dissolved in methanol (20 mL) at 0 °C. The reaction mixture was stirred continuously for 14 hours at room temperature. Upon completion of the reaction, the reaction was quenched with deionized water (20 mL) followed by extraction with ethyl acetate (30 mL x 3). The organic phases were combined, dried with anhydrous sodium sulfate and concentrated under reduced pressure to afford the target product tert-butyl 3-hydroxycyclohexylcarbamate (2.0 g, yield: 100%).
References
[1] Patent: US2016/200730, 2016, A1. Location in patent: Paragraph 0484; 0485
[2] Patent: WO2015/39348, 2015, A1. Location in patent: Page/Page column 34
(3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from (3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER manufacturers
- Product
- (3-Hydroxycyclohexyl)carbamic acid tert-butyl ester 610302-03-9
- Price
- US $0.00/gm
- Min. Order
- 100gm
- Purity
- 99%min
- Supply Ability
- 100kgs
- Release date
- 2024-09-05
- Product
- (3-HYDROXY-CYCLOHEXYL)-CARBAMIC ACID TERT-BUTYL ESTER 610302-03-9
- Price
- US $2.00/KG
- Min. Order
- 1KG
- Purity
- 99%
- Supply Ability
- customise
- Release date
- 2018-08-09