ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE

Product Name: ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE
CAS No.: 175278-02-1
Chemical Name: ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE
Synonyms: Ethylbistrifluoromethylbenzoylacetate;ETHYL [3,5-BIS(TRIFLUOROMETHYL)BENZOYL]ACETATE;Ethyl 2-[3,5-bis(trifluoromethyl)benzoyl]acetate;Ethyl β-oxo-3,5-bis(trifluoromethyl)benzenepropanoate;ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE;ETHYL 3-(3,5-BIS(TRIFLUOROMETHYL)PHENYL)-3-OXOPROPANOATE;Ethyl 3-[3,5-di(trifluoromethyl)phenyl]-3-oxopropanoate, tech;Benzenepropanoic acid, β-oxo-3,5-bis(trifluoromethyl)-, ethyl ester;Ethyl 3-[3,5-bis(trifluoromethyl)phenyl]-3-oxopropionate, Ethyl [3,5-bis(trifluoromethyl)benzoyl]acetate
CBNumber: CB0228969
Molecular Formula: C13H10F6O3
Formula Weight: 328.21
MOL File: 175278-02-1.mol

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ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE Property

Boiling point:: 80 °C
CAS DataBase Reference: 175278-02-1

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Safety

Risk Statements: 20/21/22
Safety Statements: 23-36/37/39
HS Code: 2916399090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P280Wear protective gloves/protective clothing/eye protection/face protection.

P302+P352IF ON SKIN: wash with plenty of soap and water.

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N-Bromosuccinimide Price

AK Scientific

Product number: 9170AA
Product name: Ethyl3-(3,5-bis(trifluoromethyl)phenyl)-3-oxopropanoate
Packaging: 1g
Price: $162
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2829-3-Y2
Product name: Ethyl 3-[3,5-bis(trifluoromethyl)phenyl]-3-oxopropanoate
Packaging: 5G
Price: $240
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0025848
Product name: ETHYL [3,5-BIS(TRIFLUOROMETHYL)BENZOYL]-ACETATE
Purity: 95.00%
Packaging: 1G
Price: $310.8
Updated: 2021/12/16

SynQuest Laboratories

Product number: 2829-3-Y2
Product name: Ethyl 3-[3,5-bis(trifluoromethyl)phenyl]-3-oxopropanoate
Packaging: 1g
Price: $64
Updated: 2021/12/16

Matrix Scientific

Product number: 002680
Product name: Ethyl [3,5-bis(trifluoromethyl)benzoyl]-acetate
Purity: tech
Packaging: 1g
Price: $83
Updated: 2021/12/16

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ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE Chemical Properties,Usage,Production

Synthesis

A mixture of 3,5-bis(trifluoromethyl)bromobenzene (0.5 mmol) and potassium monoethyl malonate (0.75 mmol) was added to a 30 mL microwaveable tubular flask with THF (10 mL) with stirring, followed by Pd(OAc)2 (5 mol%), Xantphos (5 mol%), MgCl2 (0.75), Et3N (0.75), imidazole (1 mmol). mmol), imidazole (1 mmol), then Co2(CO)8 (0.15 mmol) was added and the tubular vial was immediately sealed and microwaved at 90??C for 30 min. The mixture was diluted with ethyl acetate and water. The ethyl acetate layer was separated, dried with sodium sulfate and concentrated. The crude product obtained was purified by column chromatography and the pure compound was obtained using 0 to 5% hexane solution of ethyl acetate.

ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE Preparation Products And Raw materials

Raw materials

Preparation Products

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ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE Suppliers

Belgium 1 China 14 Germany 2 India 2 United Kingdom 3 United States 11 Global 33

J & K SCIENTIFIC LTD.

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Thermo Fisher Scientific

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CONIER CHEM AND PHARMA LIMITED

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Nanjing Shizhou Biology Technology Co.,Ltd

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175278-02-1, ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATERelated Search:

3-(3-Trifluoromethylphenyl)propionic acid 3-(3-TRIFLUOROMETHYL-PHENYL)-PROPIONALDEHYDE 3-(3'-TRIFLUOROMETHYL PHENYL) PROPANOL 3'-(Trifluoromethyl)acetophenone 3-(Trifluoromethyl)benzaldehyde 3-OXO-3-(3-TRIFLUOROMETHYLPHENYL)PROPIONIC ACID ETHYL ESTER 3',5'-BIS(TRIFLUOROMETHYL)PROPIOPHENONE 3',5'-Bis(trifluoromethyl)acetophenone METHYL 3-(TRIFLUOROMETHYL)BENZOYLACETATE 3-(3-METHYLPHENYL)PROPIONIC ACID 3,5-Bis(trifluoromethyl)benzaldehyde ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE 3'-(TRIFLUOROMETHYL)PROPIOPHENONE Ethyl benzoylacetate 1,3-Bis(trifluoromethyl)-benzene 3,5-BIS(TRIFLUOROMETHYL)TOLUENE 3-M-TOLYL-PROPIONIC ACID ETHYL ESTER 3-(3-METHYLPHENYL)PROPIONALDEHYDE

ETHYL [3,5-BIS(TRIFLUOROMETHYL)BENZOYL]ACETATE

ETHYL 3-(3,5-BIS(TRIFLUOROMETHYL)PHENYL)-3-OXOPROPANOATE

ETHYL 3-[3,5-DI(TRIFLUOROMETHYL)PHENYL]-3-OXOPROPANOATE

Ethylbistrifluoromethylbenzoylacetate

Ethyl 3-[3,5-di(trifluoromethyl)phenyl]-3-oxopropanoate, tech

Ethyl 3-[3,5-bis(trifluoromethyl)phenyl]-3-oxopropionate, Ethyl [3,5-bis(trifluoromethyl)benzoyl]acetate

Ethyl 2-[3,5-bis(trifluoromethyl)benzoyl]acetate

Benzenepropanoic acid, β-oxo-3,5-bis(trifluoromethyl)-, ethyl ester

Ethyl β-oxo-3,5-bis(trifluoromethyl)benzenepropanoate

175278-02-1