5-Aminoisophthalic acid monomethyl ester
- Product Name
- 5-Aminoisophthalic acid monomethyl ester
- CAS No.
- 28179-47-7
- Chemical Name
- 5-Aminoisophthalic acid monomethyl ester
- Synonyms
- CHEMPACIFIC 41247;Monomethyl 5-aminoisophthalate;3-amino-5-methoxycarbonylbenzoicaci;5-aminoisophthalate monomethyl ester;3-AMINO-5-(METHOXYCARBONYL)BENZOIC ACID;5-AMINOISOPHTHALIC ACID MONOMETHYL ESTER;1,3-Benzenedicarboxylicacid,5-amino-,1-methylester;Methyl 3-amino-5-carboxybenzoate, 5-Aminoisophthalic acid monomethyl ester;5-AMINOISOPHTHALIC ACID MONOMETHYLESTER3-AMINO-5-(METHOXYCARBONYL)BENZOIC ACID
- CBNumber
- CB0241991
- Molecular Formula
- C9H9NO4
- Formula Weight
- 195.17
- MOL File
- 28179-47-7.mol
5-Aminoisophthalic acid monomethyl ester Property
- storage temp.
- 2-8°C(protect from light)
- Appearance
- Light yellow to yellow Solid
- CAS DataBase Reference
- 28179-47-7(CAS DataBase Reference)
Safety
- HS Code
- 2922290090
Hazard and Precautionary Statements (GHS)
- Symbol(GHS)
-
- Signal word
- Warning
- Hazard statements
-
H315Causes skin irritation
H319Causes serious eye irritation
H335May cause respiratory irritation
- Precautionary statements
-
P261Avoid breathing dust/fume/gas/mist/vapours/spray.
P305+P351+P338IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continuerinsing.
N-Bromosuccinimide Price
- Product number
- A612805
- Product name
- 5-AminoisophthalicAcidMonomethylEster
- Packaging
- 250mg
- Price
- $140
- Updated
- 2021/12/16
- Product number
- FA00457
- Product name
- 5-Amino isophthalic methylester
- Packaging
- 1g
- Price
- $275
- Updated
- 2021/12/16
- Product number
- 126366
- Product name
- 3-Amino-5-(methoxycarbonyl)benzoicacid
- Purity
- >95%
- Packaging
- 1g
- Price
- $324
- Updated
- 2021/12/16
- Product number
- API0005065
- Product name
- MONOMETHYL 5-AMINOISOPHTHALATE
- Purity
- 95.00%
- Packaging
- 1G
- Price
- $327.6
- Updated
- 2021/12/16
- Product number
- U804
- Product name
- Monomethyl5-aminoisophthalate
- Packaging
- 5g
- Price
- $395
- Updated
- 2021/12/16
5-Aminoisophthalic acid monomethyl ester Chemical Properties,Usage,Production
Synthesis
1955-46-0
28179-47-7
Example 14: Synthesis of methyl 5-((1R,2S)-2-((S)-4-(4-chlorophenyl)-4-hydroxy-3,3-dimethylpiperidine-1-carbonyl)cyclohexylcarbamoyl)biphenyl-3-carboxylate Step 1: Preparation of 3-amino-5-(methoxycarbonyl)benzoic acid Under argon protection, 20% Pd(OH)2 (0.50 g) was carefully wetted with methanol (5 mL), followed by addition of a methanol (20 mL) solution of 3-(methoxycarbonyl)-5-nitrobenzoic acid (5.00 g, 22.2 mmol). The mixture was placed in a Parr shaker and hydrogenated under 50 psi hydrogen pressure for 5 hours. Upon completion of the reaction, the reaction mixture was carefully filtered through glass fiber filter paper under argon protection. The filtrate was concentrated to give the off-white solid product 3-amino-5-(methoxycarbonyl)benzoic acid (4.0 g, 20.5 mmol, 92% yield). Mass spectrometry analysis resulted in (M-H)+ = 194.
References
[1] Patent: WO2009/15166, 2009, A1. Location in patent: Page/Page column 87
[2] Chemical Communications, 2012, vol. 48, # 40, p. 4809 - 4811
[3] Bioorganic and Medicinal Chemistry Letters, 2009, vol. 19, # 10, p. 2654 - 2660
[4] Patent: US2007/32470, 2007, A1. Location in patent: Page/Page column 8-9
[5] Patent: US2006/223759, 2006, A1. Location in patent: Page/Page column 193
5-Aminoisophthalic acid monomethyl ester Preparation Products And Raw materials
Raw materials
Preparation Products
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View Lastest Price from 5-Aminoisophthalic acid monomethyl ester manufacturers
- Product
- Monomethyl 5-aminoisophthalate 28179-47-7
- Price
- US $30.00/Kg/Drum
- Min. Order
- 10Kg/Drum
- Purity
- 98.00%HPLC
- Supply Ability
- 6tons/month
- Release date
- 2021-09-14
- Product
- 5-Aminoisophthalic acid monomethyl ester 28179-47-7
- Price
- US $15.00-10.00/KG
- Min. Order
- 1KG
- Purity
- 99%+ HPLC
- Supply Ability
- Monthly supply of 1 ton
- Release date
- 2021-08-11
- Product
- 5-Aminoisophthalic acid monomethyl ester 28179-47-7
- Price
- US $3.00/KG
- Min. Order
- 1KG
- Purity
- 98%
- Supply Ability
- 100KG
- Release date
- 2020-02-04