ChemicalBook > CAS DataBase List > 5-bromo-4-methylthiazole

5-bromo-4-methylthiazole

Product Name: 5-bromo-4-methylthiazole
CAS No.: 111600-83-0
Chemical Name: 5-bromo-4-methylthiazole
Synonyms: 5-bromo-4-methylthiazole;4-methyl-5-bromothiazole;Thiazole, 5-broMo-4-Methyl;5-Bromo-4-methyl-1,3-thiazole
CBNumber: CB02500353
Molecular Formula: C4H4BrNS
Formula Weight: 178.05
MOL File: 111600-83-0.mol

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5-bromo-4-methylthiazole Property

Melting point:: 138 °C
Boiling point:: 207.3±20.0 °C(Predicted)
Density: 1.702±0.06 g/cm3(Predicted)
storage temp.: under inert gas (nitrogen or Argon) at 2-8°C
form: liquid
pka: 2.21±0.10(Predicted)
color: Brown
InChI: InChI=1S/C4H4BrNS/c1-3-4(5)7-2-6-3/h2H,1H3
InChIKey: IIMLZWMRQNCPTM-UHFFFAOYSA-N
SMILES: S1C(Br)=C(C)N=C1

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Safety

HS Code: 2934100090

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Hazard and Precautionary Statements (GHS)

Symbol(GHS)

Signal word

Warning

Hazard statements

H302Harmful if swallowed

H315Causes skin irritation

H319Causes serious eye irritation

H335May cause respiratory irritation

Precautionary statements

P261Avoid breathing dust/fume/gas/mist/vapours/spray.

P271Use only outdoors or in a well-ventilated area.

P280Wear protective gloves/protective clothing/eye protection/face protection.

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N-Bromosuccinimide Price

TRC

Product number: B697788
Product name: 5-Bromo-4-methylthiazole
Packaging: 250mg
Price: $55
Updated: 2021/12/16

TRC

Product number: B697788
Product name: 5-Bromo-4-methylthiazole
Packaging: 100mg
Price: $45
Updated: 2021/12/16

TRC

Product number: B697788
Product name: 5-Bromo-4-methylthiazole
Packaging: 5g
Price: $310
Updated: 2021/12/16

TRC

Product number: B697788
Product name: 5-Bromo-4-methylthiazole
Packaging: 10g
Price: $550
Updated: 2021/12/16

American Custom Chemicals Corporation

Product number: HCH0367019
Product name: 5-BROMO-4-METHYLTHIAZOLE
Purity: 95.00%
Packaging: 5MG
Price: $505.62
Updated: 2021/12/16

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5-bromo-4-methylthiazole Chemical Properties,Usage,Production

Synthesis

693-95-8

111600-83-0

General procedure for the synthesis of 4-methyl-5-bromothiazole from 4-methylthiazole: 4-methylthiazole (200 μL, 2.2 mmol) was mixed with bromine (112 μL, 2.2 mmol) in acetic acid (2 mL), and the reaction system needed to be protected from light, and the reaction was stirred for 16 hours at room temperature. Upon completion of the reaction, the reaction mixture was washed with 10% aqueous sodium carbonate solution and subsequently extracted with ethyl acetate. The organic phase was washed with saturated brine, dried over anhydrous sodium sulfate and concentrated under reduced pressure to afford the target product 4-methyl-5-bromothiazole (0.085 g, 22% yield). Its nuclear magnetic resonance hydrogen spectrum (1H NMR, 400 MHz, CDCl3) data were as follows: δ 2.45 (3H, s), 8.69 (1H, s).

References

[1] Patent: WO2008/36579, 2008, A1. Location in patent: Page/Page column 26
[2] Patent: WO2003/93252, 2003, A1. Location in patent: Page/Page column 85

5-bromo-4-methylthiazole Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 5-bromo-4-methylthiazole manufacturers

Hebei Fengqiang Trading Co., LTD

Product: 5-Bromo-4-methyl-thiazole 111600-83-0
Price: US $100.00/bag
Min. Order: 1bag
Purity: 99
Supply Ability: 5000
Release date: 2023-09-15

Career Henan Chemical Co

Product: 5-bromo-4-methylthiazole 111600-83-0
Price: US $1.00/KG
Min. Order: 1KG
Purity: 99%
Supply Ability: 10000KGS
Release date: 2019-12-25

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