ChemicalBook > CAS DataBase List > 1H-Indole, 4-broMo-5-Methyl-

1H-Indole, 4-broMo-5-Methyl-

Product Name
1H-Indole, 4-broMo-5-Methyl-
CAS No.
610794-15-5
Chemical Name
1H-Indole, 4-broMo-5-Methyl-
Synonyms
4-BroMo-5-Methylindole;4-BroMo-5-Methyl-1H-indole;1H-Indole, 4-broMo-5-Methyl-
CBNumber
CB02606480
Molecular Formula
C9H8BrN
Formula Weight
210.07
MOL File
610794-15-5.mol
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1H-Indole, 4-broMo-5-Methyl- Property

storage temp. 
Sealed in dry,Room Temperature
Appearance
Off-white to light yellow Solid
InChI
InChI=1S/C9H8BrN/c1-6-2-3-8-7(9(6)10)4-5-11-8/h2-5,11H,1H3
InChIKey
DVCLJDAZHYRZHZ-UHFFFAOYSA-N
SMILES
N1C2=C(C(Br)=C(C)C=C2)C=C1
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Hazard and Precautionary Statements (GHS)

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N-Bromosuccinimide Price

TRC
Product number
B814620
Product name
4-bromo-5-methyl-1H-indole
Packaging
10mg
Price
$45
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141531
Product name
4-Bromo-5-methyl-1H-indole
Packaging
10mg
Price
$50
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141531
Product name
4-Bromo-5-methyl-1H-indole
Packaging
25mg
Price
$100
Updated
2021/12/16
AK Scientific
Product number
9141AB
Product name
4-Bromo-5-methyl-1H-indole
Packaging
100mg
Price
$202.4
Updated
2021/12/16
Biosynth Carbosynth
Product number
FB141531
Product name
4-Bromo-5-methyl-1H-indole
Packaging
100mg
Price
$226
Updated
2021/12/16
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1H-Indole, 4-broMo-5-Methyl- Chemical Properties,Usage,Production

Synthesis

60956-25-4

4637-24-5

610794-15-5

Under nitrogen protection, 2-bromo-1,3-dimethyl-4-nitrobenzene (3.0 g, 13.04 mmol), pyrrolidine (926 mg, 13.04 mmol), and N,N-dimethylformamide dimethyl acetal (7.76 g, 65.22 mmol) were dissolved in 1,4-dioxane (20 mL) and the reaction was carried out for 18 hr at 100 °C. After completion of the reaction, the mixture was concentrated to dryness under reduced pressure. To the residue was added iron powder (3.65 g, 65.22 mmol) and acetic acid (40 mL) and heated at 110°C for 4 hours. The reaction solution was cooled to room temperature and filtered, and the filtrate was concentrated under reduced pressure. The crude product was purified by silica gel column chromatography using petroleum ether/ethyl acetate (10:1) as eluent to afford 4-bromo-5-methyl-1H-indole (150 mg, 5.5% yield) as a yellow solid. Mass spectrum (ESI) m/z = 210.1 ([M+H]+).

References

[1] Patent: WO2013/26914, 2013, A1. Location in patent: Page/Page column 170

1H-Indole, 4-broMo-5-Methyl- Preparation Products And Raw materials

Raw materials

Preparation Products

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View Lastest Price from 1H-Indole, 4-broMo-5-Methyl- manufacturers

Career Henan Chemical Co
Product
1H-Indole, 4-broMo-5-Methyl- 610794-15-5
Price
US $9.80/KG
Min. Order
1g
Purity
≥99%
Supply Ability
100kg
Release date
2020-01-14

610794-15-5, 1H-Indole, 4-broMo-5-Methyl-Related Search:

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